胡本芙
,
高桥平七郎
,
竹山太郎
金属学报
本文用超高压电镜(HVEM)作为电子束源,研究了Fe-15％Cr-30％Ni合金电子辐照后,合金空洞体胀和诱起晶界偏析.实验结果证明:723K,最大剂量15dpa条件下,体胀量为0.62％.在晶界发生Cr贫化、Ni富化.随着辐照温度提高,晶界偏析程度增加,723K时Cr,Ni在晶界出现最大偏析峰,相应空洞体胀量也最大.结果表明,空洞形成和晶界偏析密切相关,本文提出了辐照诱起晶界偏析模型.
关键词:
电子辐照
,
Fe-Cr-Ni alloy
,
void swelling
,
grain boundary segregation
胡本芙
,
高桥平七郎
,
伊藤久敏
,
竹山太郎
金属学报
本文采用电子束辐照,研究了Fe-15Cr-xMn合金以及添加W,V合金的孔洞体胀和诱起晶界偏析行为,并对包含晶界在内的辐照区进行成分分析。 结果表明,在Fe-Cr-Mn系合金中孔洞体胀孕育期可以被强烈抑制,晶界偏析也减少。特别是,合金中添加W,V效果更加明显。用Mn代替Ni,通常要发生体胀和相的不稳定性,由于反Kirkendall效应导致Ni和Mn的扩散行为不同,使Fe富集在尾闾处,局部地区形成铁素体,有利于减少体胀和晶界偏析。
关键词:
诱起偏析
,
inverse-Kirkendall effect
,
void swelling
,
electron irradiation
HU Benfu University of Science and Technology Beijing
,
Beijing
,
ChinaTAKAHASHI Heishichiro
,
ITOH Hisatoshi
,
TAKEYAMA Taro Hokkaido University
,
Sapporo
,
060
,
Japan Associate Professor
,
Dept of Materials Science and Engineering
,
University of Science and Technology Beijing
,
Beijing 100083
,
China
金属学报(英文版)
The behavior of void swelling and segregation in Fe-15Cr-xMn alloys and an alloy con- taining small amount of W and V was investigated by electron-irradiation.The compositional analysis in the irradiated regions including grain boundaries was performed.The resultdts show that there are many common features of irradiuation tehavior in the Fe-Cr-Mn and Fe-Cr-Ni systems while there are some significant differences,In the Fe-Cr-Mn alloy sys- tems void swelling was rematrkably suppressed and at the same time the radiation-induced segregation was also retarded,furthermore,the segregation was strongly retarded in an Fe-15Cr-15Mn alloy containing small amount of W and V.The results also show that Ni re- placed by Mn does not in general confer immunity from either swelling or phase instabilities. The phase instability is due to the different diffusion behavior of Ni and Mn in reponse to the operation of the inverse-Kirkendall effecr.Fe segregates to the microstructural sinks in the Fe-Cr-Mn alloys.The segregation of Fe often leads to the formation of ferrite.This fact is beneficial to reducing the swelling rate and segregation on the grain boundaries.
关键词:
electron irradiation
,
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