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陶瓷微器件的软刻蚀成形研究进展

苏博 , 吴有智 , 孟军虎 , 吕晋军

材料科学与工程学报

软刻蚀技术是基于传统光刻蚀技术提出的一系列技术,包括微模塑、转移微模塑和毛细微模塑等,其共同特点是利用弹性模作为微结构转移元件,复制其他方法制备的原始模板的微结构,再用此弹性模进行微结构的成形.因其成本低廉、操作过程简单,为陶瓷微器件的制备提供了一种先进的净成形加工技术.其工艺步骤主要包括:弹性模的制备、浆料或陶瓷预聚体的制备、注模、干燥(交联固化)、脱模和烧结.本文按照制备工艺综述了软刻蚀技术成形陶瓷微器件的研究进展,着重讨论了影响微成形的关键因素,并对将来的研究方向进行了展望.

关键词: 软刻蚀 , 陶瓷微器件 , 弹性模

Sol-Gel Based Soft Lithography and Piezoresponse Force Microscopy of Patterned Pb(Zr0:52Ti0:48)O3 Microstructures

Lining Lan Shuhong Xie Li Tan Jiangyu Li

材料科学技术(英文)

Sol-gel based soft lithography technique has been developed to pattern a variety of ferroelectric Pb(Zr0:52Ti0:48)O3 (PZT) microstructures, with feature size approaching 180 nm and good pattern transfer between the master mold and patterned films. X-ray diffraction and high-resolution transmission electron microscopy confirm the perovskite structure of the patterned PZT. Piezoresponse force microscopy (PFM) and switching spectroscopy piezoresponse force microscopy (SSPFM) confirm their piezoelectricity and ferroelec-
tricity. Piezoresponse as high as 2.75 nm has been observed, comparable to typical PZT films. The patterned PZT microstructures are promising for a wide range of device applications.

关键词: Soft lithography , Piezoresponse force microscopy , PZT

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