{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"采用普通直流电沉积和超声直流电沉积制备Cu/<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>/<span style=\"color:red\">Ti</span><span style=\"color:red\">基</span><span style=\"color:red\">复合</span><span style=\"color:red\">薄膜</span>,而后在NaOH溶液中用电氧化的方法将Cu单质氧化成<span style=\"color:red\">CuO</span>,制备了<span style=\"color:red\">CuO</span>/<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>/<span style=\"color:red\">Ti</span><span style=\"color:red\">基</span><span style=\"color:red\">复合</span><span style=\"color:red\">薄膜</span>.利用扫描电子显微镜(SEM)和X射线衍射仪(XRD)对两种<span style=\"color:red\">复合</span><span style=\"color:red\">薄膜</span>电极的形貌和结构进行了表征,详细考察了电镀工艺参数(电流密度)和超声波对<span style=\"color:red\">复合</span><span style=\"color:red\">薄膜</span>形貌的影响.同时通过稳态光电响应技术对<span style=\"color:red\">复合</span><span style=\"color:red\">薄膜</span>电极组成的染料敏华太阳能电池(DSSC)的光电性能进行了研究,结果表明:通过普通直流电沉积在工艺参数(3 mA/cm<span style=\"color:red\">2</span>、5min)处制备的<span style=\"color:red\">复合</span><span style=\"color:red\">薄膜</span>组装的DSSC具有该体系下的最佳光电性能(Jsc=9.00mA/cm<span style=\"color:red\">2</span>、Voc=0.664V、FF =0.512、η=3.06％);在同等条件下通过超声辅助直流电沉积制备的<span style=\"color:red\">复合</span><span style=\"color:red\">薄膜</span>组装的DSSC的最佳光电性能(Jse=15.50mA/cm<span style=\"color:red\">2</span>、Woc =0.688V、FF=0.505、η=5.39％)出现在工艺参数为(6mA/cm<span style=\"color:red\">2</span>、5min)处.对比可知超声条件下的光电性能较好,且最佳光电性能工艺参数发生了后移.","authors":[{"authorName":"聂洋洲","id":"4437bc09-b19e-4b71-823b-9cbfd2b9b6ca","originalAuthorName":"聂洋洲"},{"authorName":"杨国华","id":"22b53e3d-57ed-41b8-9960-4e4779f4006a","originalAuthorName":"杨国华"},{"authorName":"顾玉宗","id":"ad85175a-1eca-42c8-976e-e417bc270f44","originalAuthorName":"顾玉宗"}],"doi":"10.3969/j.issn.1007-4252.2012.03.013","fpage":"247","id":"1b5a18e0-f172-4d16-b57a-1dc0f7bd085f","issue":"3","journal":{"abbrevTitle":"GNCLYQJXB","coverImgSrc":"journal/img/cover/GNCLYQJXB.jpg","id":"34","issnPpub":"1007-4252","publisherId":"GNCLYQJXB","title":"功能材料与器件学报   "},"keywords":[{"id":"71140017-65de-432b-9845-d9479a8d7491","keyword":"<span style=\"color:red\">CuO</span>/<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>/<span style=\"color:red\">Ti</span><span style=\"color:red\">基</span><span style=\"color:red\">复合</span><span style=\"color:red\">薄膜</span>","originalKeyword":"CuO/TiO2纳米管阵列/Ti基复合薄膜"},{"id":"a9ddd15c-4b8f-4a18-a44c-0d657ce30b11","keyword":"超声辅助","originalKeyword":"超声辅助"},{"id":"a217e9de-c8a5-482a-bf9a-b3cb7889abf1","keyword":"工艺参数","originalKeyword":"工艺参数"},{"id":"b0523c7f-6073-4f1b-a67e-955dbc01b90d","keyword":"染料敏化太阳能电池","originalKeyword":"染料敏化太阳能电池"}],"language":"zh","publisherId":"gnclyqjxb201203013","title":"染料敏化太阳能电池中<span style=\"color:red\">CuO</span>/<span style=\"color:red\">TiO2</span><span style=\"color:red\">薄膜</span>制备及应用","volume":"18","year":"2012"},{"abstractinfo":"<FONT face=Verdana>使用阳极氧化法制备了<span style=\"color:red\">TiO</span><SUB><span style=\"color:red\">2</span></SUB>/<span style=\"color:red\">Ti</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span><span style=\"color:red\">薄膜</span>材料. <span style=\"color:red\">TiO</span><SUB><span style=\"color:red\">2</span></SUB><span style=\"color:red\">纳米管</span>管孔分布均匀，<span style=\"color:red\">管</span>径约为80~90nm，平均<span style=\"color:red\">管</span>长约为1.8μm. 在400℃下</FONT><FONT face=Verdana>煅烧<span style=\"color:red\">2</span>h后，<span style=\"color:red\">TiO</span><SUB><span style=\"color:red\">2</span></SUB><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>为锐钛矿型，并且结构保持良好，没有出现变形、剥落的现象. 以<span style=\"color:red\">TiO</span><SUB><span style=\"color:red\">2</span></SUB>/<span style=\"color:red\">Ti</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span><span style=\"color:red\">薄膜</span>材料为光催化剂，同时施</FONT><FONT face=Verdana>加0~+3.0V范围内变化的电场，考察了外加电压对降解亚甲基蓝光电协同效率的影响. 结果表明在外加+1.4V电压的条件下，光电协同效率达到</FONT><FONT face=Verdana>124%. <span style=\"color:red\">TiO</span><SUB><span style=\"color:red\">2</span></SUB><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>与基底<span style=\"color:red\">Ti</span>板结合牢固，多次重复使用后没有发现降解率的明显变化. </FONT>","authors":[{"authorName":"陈怡","id":"53986319-9f54-40d2-bf43-dd0042290694","originalAuthorName":"陈怡"},{"authorName":"施利毅","id":"4b96d1eb-0862-487c-90a5-6a146e3d4a33","originalAuthorName":"施利毅"},{"authorName":"袁帅","id":"58b2ba29-dcc9-478d-b4f7-7596d8886fc0","originalAuthorName":"袁帅"},{"authorName":"吴钧","id":"e98f6337-8f49-4362-ac55-2f8fb561dd32","originalAuthorName":"吴钧"},{"authorName":"张美红","id":"8a83a6fc-0169-4c1d-b06a-c51c4b6abe37","originalAuthorName":"张美红"},{"authorName":"方建慧","id":"a26aa881-ce3f-4c9e-8b42-0c6cf81b8ee0","originalAuthorName":"方建慧"}],"categoryName":"|","doi":"10.3724/SP.J.1077.2009.00680","fpage":"680","id":"b242a794-b58a-4138-8fa7-3469568de794","issue":"4","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"b78869e3-5298-4e1f-beff-f08b1797d1fc","keyword":"阳极氧化","originalKeyword":"阳极氧化"},{"id":"030cec34-6baa-485e-afde-47c1948e75c8","keyword":" <span style=\"color:red\">TiO</span><SUB><span style=\"color:red\">2</span></SUB> nanotube array","originalKeyword":" TiO<SUB>2</SUB> nanotube array"},{"id":"d87e23a5-1097-4273-9a2f-5c74fa329fae","keyword":" synergetic effect of UV light and electric field","originalKeyword":" synergetic effect of UV light and electric field"},{"id":"38528a8c-4852-430c-86b1-0fef343ae3bf","keyword":" methylene blue","originalKeyword":" methylene blue"}],"language":"zh","publisherId":"1000-324X_2009_4_24","title":"<span style=\"color:red\">TiO</span><SUB><span style=\"color:red\">2</span></SUB><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span><span style=\"color:red\">薄膜</span>光电协同降解亚甲基蓝的研究","volume":"24","year":"2009"},{"abstractinfo":"使用阳极氧化法制备了<span style=\"color:red\">TiO2</span>/<span style=\"color:red\">Ti</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span><span style=\"color:red\">薄膜</span>材料.<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span>管孔分布均匀,<span style=\"color:red\">管</span>径约为80～90nm,平均<span style=\"color:red\">管</span>长约为1.8μm.在400℃下煅烧<span style=\"color:red\">2</span>h后,<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>为锐钛矿型,并且结构保持良好,没有出现变形、剥落的现象.以<span style=\"color:red\">TiO2</span>/<span style=\"color:red\">Ti</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span><span style=\"color:red\">薄膜</span>材料为光催化剂,同时施加0～+3.0V范围内变化的电场,考察了外加电压对降解亚甲基蓝光电协同效率的影响.结果表明在外加+1.4V电压的条件下,光电协同效率达到124%.<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>与基底<span style=\"color:red\">Ti</span>板结合牢固,多次重复使用后没有发现降解率的明显变化.","authors":[{"authorName":"陈怡","id":"35357326-f12e-47b4-9c53-9e29875d5c90","originalAuthorName":"陈怡"},{"authorName":"施利毅","id":"f5edfea3-2192-4aef-ae7f-d78b61442d99","originalAuthorName":"施利毅"},{"authorName":"袁帅","id":"7caa77ba-602f-42d8-95b5-ab0ffa7a4a40","originalAuthorName":"袁帅"},{"authorName":"吴钧","id":"dbd9e361-8fd2-4c64-9f4a-9a139ea9af8c","originalAuthorName":"吴钧"},{"authorName":"张美红","id":"edffa7eb-d50b-4d27-b3fb-f5becfee10d1","originalAuthorName":"张美红"},{"authorName":"方建慧","id":"a81ccfed-5311-4bc2-9e6a-06c56b34781b","originalAuthorName":"方建慧"}],"doi":"10.3724/SP.J.1077.2009.00680","fpage":"680","id":"d9dac6e7-90bd-4aa6-8017-39c911724fa1","issue":"4","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"46e5f9a4-4c50-40cb-bfe8-7f37d9ac3f75","keyword":"阳极氧化","originalKeyword":"阳极氧化"},{"id":"4af5abac-8c01-4786-8bba-89b133ccdd2a","keyword":"<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>","originalKeyword":"TiO2纳米管阵列"},{"id":"bca92c74-7e35-477c-bc47-7521924ae782","keyword":"光电协同","originalKeyword":"光电协同"},{"id":"9169a928-e994-4900-afd1-01987a77315d","keyword":"亚甲基蓝","originalKeyword":"亚甲基蓝"}],"language":"zh","publisherId":"wjclxb200904007","title":"<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span><span style=\"color:red\">薄膜</span>光电协同降解亚甲基蓝的研究","volume":"24","year":"2009"},{"abstractinfo":"采用液相沉积法,将铝基多孔阳极氧化铝(AAO)模板浸入到(MH4)<span style=\"color:red\">2</span>TiF6溶液中,制备出高度有序的<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span><span style=\"color:red\">薄膜</span>,并在不同的温度下进行了热处理.用场发射扫描电子显微镜、透射电子显微镜和X射线衍射仪等手段对试样的微观形貌、结构及物相进行了表征.结果表明,<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span>的形貌依赖于AAO的特征,<span style=\"color:red\">薄膜</span>是由外径大约200 nm,壁厚约40 nm的<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>组成,<span style=\"color:red\">薄膜</span>厚度约25μm.原位模板法制备的<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span><span style=\"color:red\">薄膜</span>为非晶态,在400℃空气中焙烧<span style=\"color:red\">2</span> h转变为锐钛矿相<span style=\"color:red\">TiO2</span>.经过650℃焙烧仍保持<span style=\"color:red\">纳米管</span>结构,表现出较好的热稳定性.","authors":[{"authorName":"蒋武锋","id":"89dc847d-6540-4487-a112-422d496a4372","originalAuthorName":"蒋武锋"},{"authorName":"凌云汉","id":"6203cbb8-1ea3-45ec-a8a5-ad03666241ee","originalAuthorName":"凌云汉"},{"authorName":"白新德","id":"d377b3b4-4804-4852-ac08-d636748e0a1d","originalAuthorName":"白新德"},{"authorName":"李洪义","id":"3214931e-9a71-426e-881b-26cab6e3fcdf","originalAuthorName":"李洪义"},{"authorName":"苍大强","id":"0e90e29a-f892-49b0-ac18-155e1b79f2f3","originalAuthorName":"苍大强"}],"doi":"","fpage":"1178","id":"4eb087e1-a24c-49b9-af3a-1a63e97fb213","issue":"7","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"f59f7d0f-2051-4e9d-92a7-067683551137","keyword":"二氧化钛","originalKeyword":"二氧化钛"},{"id":"189cb382-c601-45fc-8027-cc931c1dc2a2","keyword":"<span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span><span style=\"color:red\">薄膜</span>","originalKeyword":"纳米管阵列薄膜"},{"id":"f3397c19-5168-4259-9175-a555ba47b5d8","keyword":"液相沉积","originalKeyword":"液相沉积"},{"id":"239c47b4-8763-45b6-a4d3-2a6765c9faf8","keyword":"阳极氧化铝(AAO)","originalKeyword":"阳极氧化铝(AAO)"}],"language":"zh","publisherId":"xyjsclygc200707011","title":"原位模板法在铝基底上制备<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span><span style=\"color:red\">薄膜</span>","volume":"36","year":"2007"},{"abstractinfo":"阳极氧化<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>由于具有高度有序的独特<span style=\"color:red\">纳米</span>结构和优异的物理化学性能,已成为<span style=\"color:red\">纳米</span>材料以及太阳能光转化利用等研究领域的热点之一.国内外围绕<span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>的制备、改性及应用等方面开展了大量研究,取得了显著成果.最近,<span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>改性方面的研究受到人们的特别关注,相关研究已经为这种高度有序<span style=\"color:red\">纳米</span>材料的应用打下良好基础.本文较详细地介绍了<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>的改性研究进展,分析了存在的主要问题,提出了今后的发展建议.","authors":[{"authorName":"刘世凯","id":"c6e80729-4ea9-45a7-a796-b5453676c218","originalAuthorName":"刘世凯"},{"authorName":"杨海滨","id":"843625cf-7dd6-4c4f-8e82-95398f0765ad","originalAuthorName":"杨海滨"},{"authorName":"付乌有","id":"8667d119-dabc-4bfc-847f-7eb0a32c4bde","originalAuthorName":"付乌有"}],"doi":"","fpage":"597","id":"6215370a-1530-4c82-a99a-0cada89ecaa9","issue":"3","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报   "},"keywords":[{"id":"012cca8d-4023-4404-99c0-6ea6a0822ab6","keyword":"二氧化钛","originalKeyword":"二氧化钛"},{"id":"05581339-4667-46d6-a042-69230960e653","keyword":"<span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>","originalKeyword":"纳米管阵列"},{"id":"00f1d5e6-f9ad-4468-8662-53acce87eeb1","keyword":"阳极氧化","originalKeyword":"阳极氧化"},{"id":"93c51b97-e526-4ef4-abd2-9021ad906b81","keyword":"改性","originalKeyword":"改性"}],"language":"zh","publisherId":"gsytb201103022","title":"阳极氧化<span style=\"color:red\">TiO2</span><span style=\"color:red\">基</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>改性的研究进展","volume":"30","year":"2011"},{"abstractinfo":"采用阳极氧化法在<span style=\"color:red\">Ti</span>-6Al-4V合金表面制备了<span style=\"color:red\">TiO2</span><span style=\"color:red\">基</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>.所用电解液为0.3 mol/L.H3PO4与0.14 mol/L NH4F的混合溶液,使用电压10～50 V.用冷场发射扫描电子显微镜(FESEM)、能量色散X射线荧光光谱仪(EDX)和X射线衍射仪(XRD)表征了所制备<span style=\"color:red\">薄膜</span>的形貌、元素组成和晶型结构.用紫外-可见光分光光度计分析了<span style=\"color:red\">薄膜</span>的光吸收特性,用电化学工作站测试了其光电特性.结果表明,在20～40V电压下可以做出不同<span style=\"color:red\">管</span>径的<span style=\"color:red\">纳米管</span>,经600℃热处理的样品在可见光区有较好的吸收和光电特性.","authors":[{"authorName":"罗保民","id":"ad90619b-72bf-4890-8e4e-668c259995dc","originalAuthorName":"罗保民"},{"authorName":"杨海滨","id":"b7f3b5fa-8ddb-43ed-95e2-1e23babbde46","originalAuthorName":"杨海滨"},{"authorName":"刘世凯","id":"2673d6cf-9754-40ee-be89-6f8093b3ba7c","originalAuthorName":"刘世凯"}],"doi":"","fpage":"19","id":"1e81e602-c5fa-4029-b93e-5e9199036c68","issue":"10","journal":{"abbrevTitle":"ZGCLJZ","coverImgSrc":"journal/img/cover/中国材料进展.jpg","id":"80","issnPpub":"1674-3962","publisherId":"ZGCLJZ","title":"中国材料进展"},"keywords":[{"id":"30618a03-4a65-4825-adc0-2003583da1c4","keyword":"阳极氧化","originalKeyword":"阳极氧化"},{"id":"1b7a7910-c238-472a-92b1-a85ebe66309f","keyword":"<span style=\"color:red\">TiO2</span>","originalKeyword":"TiO2"},{"id":"4a8b6d17-da7e-446d-af61-9a24e3e9bb26","keyword":"<span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>","originalKeyword":"纳米管阵列"},{"id":"d2b09df0-6858-4140-9d21-bad40d03609c","keyword":"Tj-6Al-4V","originalKeyword":"Tj-6Al-4V"}],"language":"zh","publisherId":"zgcljz200810005","title":"<span style=\"color:red\">Ti</span>-6Al-4V合金表面<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span><span style=\"color:red\">薄膜</span>的制备与光电特性研究","volume":"27","year":"2008"},{"abstractinfo":"采用电化学阳极氧化法在HF酸水溶液中使纯钛表面生成结构致密有序的<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span><span style=\"color:red\">薄膜</span>,考察了阳极氧化电压和阳极氧化时间对<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>形貌的影响,讨论了<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span>的形成机理.采用复阻抗谱方法,测量了获得的<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span><span style=\"color:red\">薄膜</span>在不同湿度下的电阻-电抗曲线和相位角-频率曲线,由此分析得到,试样的等效电路由<span style=\"color:red\">2</span>个RC并联回路串联而成,并拟合出等效电路各元件的参数值,说明<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span><span style=\"color:red\">薄膜</span>表面对湿度变化有较好的响应.","authors":[{"authorName":"王红","id":"ff98310c-3c98-49fa-8dbe-48df9dfd25b0","originalAuthorName":"王红"},{"authorName":"傅刚","id":"7e6f028b-dcc3-4519-99b0-b1d38c241ffa","originalAuthorName":"傅刚"},{"authorName":"陈环","id":"96cef0cb-12c2-45c6-bfcc-9380ae9fd4e6","originalAuthorName":"陈环"},{"authorName":"刘志宇","id":"77242276-0cda-4826-adab-b97b35a84248","originalAuthorName":"刘志宇"}],"doi":"","fpage":"100","id":"d6c89ddb-0775-4670-a944-174a0271ea49","issue":"z1","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"93cdfde8-4462-40e8-a777-99c149d85116","keyword":"阳极氧化","originalKeyword":"阳极氧化"},{"id":"0630a096-6e03-4b90-ad9f-9c6a8a582dc1","keyword":"<span style=\"color:red\">TiO2</span>","originalKeyword":"TiO2"},{"id":"208d560b-06db-493b-abe9-2e49e437681d","keyword":"<span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>","originalKeyword":"纳米管阵列"},{"id":"da96282d-2f44-42c4-aed2-d4243a5cda62","keyword":"湿度","originalKeyword":"湿度"},{"id":"b00ffea0-98ca-49a7-9bcd-5e125549a79c","keyword":"复阻抗分析","originalKeyword":"复阻抗分析"}],"language":"zh","publisherId":"cldb2008z1032","title":"<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>的制备及复阻抗分析","volume":"22","year":"2008"},{"abstractinfo":"在(NH4)<span style=\"color:red\">2</span>TiF6的水溶液中,以铝<span style=\"color:red\">基</span>阳极氧化铝为模板,采用水热法制备了<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>. 使用场发射扫描电镜和X射线衍射对水热合成产物进行了表征. 实验结果表明,水热处理所得<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>具有特殊的形貌,其表面为连续的多孔状,断面为不连续、相互分离的管状;管口和管壁分别由平均粒度约45和25 nm的微细<span style=\"color:red\">TiO2</span>颗粒紧密堆积而成. 采用本方法制备的<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>无需热处理便已具有明显的锐钛矿型晶相特征.","authors":[{"authorName":"李纲","id":"ee1ba906-5be6-4a3a-8f0a-43ed8304d490","originalAuthorName":"李纲"},{"authorName":"刘中清","id":"afe0a98f-f9bf-490a-931a-56499b5d15a1","originalAuthorName":"刘中清"},{"authorName":"颜欣","id":"584dc337-292f-4088-ad99-98aa662483d3","originalAuthorName":"颜欣"},{"authorName":"张昭","id":"27574680-82c1-404b-b8df-9f6023d52d25","originalAuthorName":"张昭"}],"doi":"","fpage":"680","id":"a045937e-b402-474e-945f-3e687c08fee7","issue":"8","journal":{"abbrevTitle":"CHXB","coverImgSrc":"journal/img/cover/CHXB.jpg","id":"18","issnPpub":"0253-9837","publisherId":"CHXB","title":"催化学报   "},"keywords":[{"id":"6ee38a2a-b510-42a7-bc28-e7e497462c68","keyword":"二氧化钛","originalKeyword":"二氧化钛"},{"id":"937bac42-8eab-460c-b01d-548c1274ec44","keyword":"<span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>","originalKeyword":"纳米管阵列"},{"id":"07df76eb-67a5-400a-94cb-889ff4880fdf","keyword":"铝<span style=\"color:red\">基</span>","originalKeyword":"铝基"},{"id":"4bc8c8e1-0cc4-498d-b093-4aca842ef8a9","keyword":"阳极氧化铝模板","originalKeyword":"阳极氧化铝模板"},{"id":"4c4c1ea7-84cf-4027-a27d-2cb7f6180f1a","keyword":"水热合成","originalKeyword":"水热合成"}],"language":"zh","publisherId":"cuihuaxb200808002","title":"铝<span style=\"color:red\">基</span>阳极氧化铝模板水热法制备<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>","volume":"29","year":"2008"},{"abstractinfo":"综述了近年来有序<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span><span style=\"color:red\">薄膜</span>的制备、性质及其在能源、环境、生物组织工程等领域应用的研究进展.","authors":[{"authorName":"张文彦","id":"455390d9-b0fc-4810-82d7-1228dc947236","originalAuthorName":"张文彦"},{"authorName":"奚正平","id":"da0e8654-ab4a-430e-a8d5-99115261fdec","originalAuthorName":"奚正平"},{"authorName":"李广忠","id":"42208a1e-b805-496b-9311-36b239eb6753","originalAuthorName":"李广忠"},{"authorName":"李亚宁","id":"fa08dd5f-8959-4a99-9cbf-27b6a35d3717","originalAuthorName":"李亚宁"},{"authorName":"张健","id":"1e4e0b0d-de0f-45cf-908b-7c39ffbb401d","originalAuthorName":"张健"},{"authorName":"汤慧萍","id":"8b68c9ff-7094-4579-a5b7-1b9db7e7bded","originalAuthorName":"汤慧萍"}],"doi":"","fpage":"1876","id":"a1ef0086-a9ad-432c-b664-cf5ebfe56926","issue":"10","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"88edfcc1-83a9-4f9f-ae11-6c80ea1b6039","keyword":"钛","originalKeyword":"钛"},{"id":"814db403-f21d-4496-9adb-57ebeea93fbf","keyword":"阳极氧化","originalKeyword":"阳极氧化"},{"id":"8d37c203-8697-49d1-9ec1-bc5155f6f612","keyword":"<span style=\"color:red\">TiO2</span>","originalKeyword":"TiO2"},{"id":"3026533c-6b21-4409-b99e-45cddfbb7622","keyword":"<span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>","originalKeyword":"纳米管阵列"}],"language":"zh","publisherId":"xyjsclygc200910042","title":"有序<span style=\"color:red\">TiO2</span><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>膜材料的研究进展","volume":"38","year":"2009"},{"abstractinfo":"采用阳极氧化法在钛片上制备了<span style=\"color:red\">TiO</span><SUB><span style=\"color:red\">2</span></SUB><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>光电极, 利用扫描电子显微镜(SEM)和X射线衍射仪(XRD) 对<span style=\"color:red\">TiO</span><SUB><span style=\"color:red\">2</span></SUB><span style=\"color:red\">纳米管</span>的形貌和结构进行了表征, 详细考察了氧化工艺参数对<span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>形貌的影响, 并通过稳态光电响应技术对<span style=\"color:red\">TiO</span><SUB><span style=\"color:red\">2</span></SUB><span style=\"color:red\">纳米管</span>电极的光电化学性能进行了研究. 结果表明, 在1wt HF电解液中, 控制氧化电压为20V, 反应30min后, 在<span style=\"color:red\">Ti</span>表面获得了垂直导向的<span style=\"color:red\">TiO</span><SUB><span style=\"color:red\">2</span></SUB><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>, 孔径约为90nm, 管壁厚度约为10nm. 经600℃退火处理后, <span style=\"color:red\">TiO</span><SUB><span style=\"color:red\">2</span></SUB><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>为锐钛矿型与金 红石型的混晶结构, 此时电极的光电性能最佳, 与<span style=\"color:red\">TiO</span><SUB><span style=\"color:red\">2</span></SUB><span style=\"color:red\">纳米</span>多孔膜电极相比, 光电性能大幅提高.","authors":[{"authorName":"李贺","id":"c1dd1d35-c7eb-45c6-9855-32dfaa4969b6","originalAuthorName":"李贺"},{"authorName":"姚素薇","id":"4a5bd892-7af6-4289-b0b6-e2690e9711d2","originalAuthorName":"姚素薇"},{"authorName":"张卫国","id":"f19d9143-378d-4331-93bd-e3e257ecf863","originalAuthorName":"张卫国"},{"authorName":"王宏智","id":"244fd233-c0db-4c57-ac1e-aeb94bbb294a","originalAuthorName":"王宏智"},{"authorName":"贲宇恒","id":"01df1568-46d9-4ed4-9e42-8889eadc48f0","originalAuthorName":"贲宇恒"}],"categoryName":"|","doi":"10.3724/SP.J.1077.2007.00349","fpage":"349","id":"a39bf1f8-5191-4a9a-8e2d-220a53cca17a","issue":"2","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"ff4cd619-26e3-4048-8184-6988841f994c","keyword":"阳极氧化","originalKeyword":"阳极氧化"},{"id":"1c24497a-746e-4c0e-bfcb-c1ef4d7ed769","keyword":" <span style=\"color:red\">TiO2</span> nanotubes","originalKeyword":" TiO2 nanotubes"},{"id":"e1b28cef-37aa-4d08-b033-076fb04315ed","keyword":" array","originalKeyword":" array"},{"id":"252f043f-cd33-4b73-93c3-dc5efe6b63e5","keyword":" photoelectrochemistry","originalKeyword":" photoelectrochemistry"}],"language":"zh","publisherId":"1000-324X_2007_2_16","title":"阳极氧化法制备<span style=\"color:red\">TiO</span><SUB><span style=\"color:red\">2</span></SUB><span style=\"color:red\">纳米管</span><span style=\"color:red\">阵列</span>及其光电性能研究","volume":"22","year":"2007"}],"totalpage":12587,"totalrecord":125866}