{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"本研究提供了一种简易、低成本的工艺和方法,进行神经<span style=\"color:red\">微电极</span>的性能改进,来改善神经<span style=\"color:red\">电极</span>/神经组织的界面特性.首先采用光敏型聚酰亚胺(Durimide 7510)作为<span style=\"color:red\">微电极</span>基质材料制备了一种<span style=\"color:red\">柔性</span>神经<span style=\"color:red\">微电极</span>;然后电化学合成导电聚合物聚噻吩PEDOT/LiClO4,进行神经<span style=\"color:red\">微电极</span>位点的表面修饰;最后测试和评价了神经<span style=\"color:red\">微电极</span>的表面形貌、电学性能及其生物相容性.结果表明导电聚合物粗糙的菜花状表面形貌提供了更大的界面表面积,因此<span style=\"color:red\">电极</span>阻抗降低到原来的1/20,<span style=\"color:red\">微电极</span>的电荷注入能力也增加了约100倍.细胞生物学实验也表明,导电聚合物修饰的<span style=\"color:red\">柔性</span><span style=\"color:red\">微电极</span>上,细胞生长状态良好,与未修饰的<span style=\"color:red\">柔性</span><span style=\"color:red\">微电极</span>下相比,粘附率与存活率均有明显改善,粘附率较修饰前增加了92.5%,存活率也由69.2%提高到85.4%.","authors":[{"authorName":"张华","id":"c3fb6c7b-c109-4b21-87ca-d5ad0d18c134","originalAuthorName":"张华"},{"authorName":"朱壮晖","id":"c50c79e8-bbd7-4d51-8d89-a46ba8db7461","originalAuthorName":"朱壮晖"},{"authorName":"吴蕾","id":"12af10fe-b0d3-489f-930c-d3b771f560a4","originalAuthorName":"吴蕾"},{"authorName":"周洪波","id":"2b100f83-cea5-4f64-b7e4-e289ef777d3a","originalAuthorName":"周洪波"},{"authorName":"孙晓娜","id":"023ef6db-122b-478a-951f-486e537a7b2c","originalAuthorName":"孙晓娜"},{"authorName":"周亮","id":"727d61b3-5f73-4a25-b831-2bab3468f849","originalAuthorName":"周亮"},{"authorName":"李刚","id":"5b526d54-f636-4c4f-9d7c-0fc126ae2392","originalAuthorName":"李刚"},{"authorName":"金庆辉","id":"07d1dec1-f574-4237-8910-dd6b304da33e","originalAuthorName":"金庆辉"},{"authorName":"赵建龙","id":"8a0d3b74-c10e-4913-aefe-1ab3805c8862","originalAuthorName":"赵建龙"}],"doi":"10.3969/j.issn.1007-4252.2010.05.009","fpage":"457","id":"0fdb4168-56a2-4aae-b4b3-57312d0bd479","issue":"5","journal":{"abbrevTitle":"GNCLYQJXB","coverImgSrc":"journal/img/cover/GNCLYQJXB.jpg","id":"34","issnPpub":"1007-4252","publisherId":"GNCLYQJXB","title":"功能材料与器件学报   "},"keywords":[{"id":"21707757-1b6a-4b8a-bc3d-5df30385c7a0","keyword":"<span style=\"color:red\">柔性</span><span style=\"color:red\">微电极</span>","originalKeyword":"柔性微电极"},{"id":"57149c80-661e-47d1-bb1d-ed70cb901ffb","keyword":"导电聚合物","originalKeyword":"导电聚合物"},{"id":"dec15cb3-5730-4ba6-8e38-acf5f60fef7e","keyword":"表面修饰","originalKeyword":"表面修饰"},{"id":"02bbf1c7-dace-4ea9-ab0b-20afaf213d0d","keyword":"生物相容性","originalKeyword":"生物相容性"}],"language":"zh","publisherId":"gnclyqjxb201005009","title":"导电聚合物修饰的<span style=\"color:red\">柔性</span>神经<span style=\"color:red\">微电极</span>的制备与界面性质","volume":"16","year":"2010"},{"abstractinfo":"为了实现植入式<span style=\"color:red\">柔性</span>神经<span style=\"color:red\">微电极</span>与外部记录或刺激装置的有效、可靠连接,本文提出了一种基于通孔电镀的植入式<span style=\"color:red\">柔性</span>神经<span style=\"color:red\">微电极</span>互连方法.该方法首先制作具有通孔结构的<span style=\"color:red\">柔性</span>互连膜,并将其通孔与待连接的植入式<span style=\"color:red\">微电极</span>焊接位点对准贴合,然后电镀生长导通金属,从而实现与待连接的植入武器件的<span style=\"color:red\">柔性</span>连接.最后本文通过SEM观察、电学性能测试、机械强度测试以及生物兼容性测试等手段对此互连方法的焊接效果进行了评价.测试结果表明本文提出的<span style=\"color:red\">柔性</span><span style=\"color:red\">微电极</span>互连方法具有很好的可靠性和稳定性.","authors":[{"authorName":"周亮","id":"fcff4b9f-e5be-4ae8-a132-831548685e21","originalAuthorName":"周亮"},{"authorName":"朱壮晖","id":"84428c05-4ac4-4fa9-a745-73155aeb932a","originalAuthorName":"朱壮晖"},{"authorName":"张华","id":"f85c9d95-b49a-46fa-849a-e93bb663f467","originalAuthorName":"张华"},{"authorName":"周洪波","id":"0155074e-bac2-4f81-a632-70294a13723c","originalAuthorName":"周洪波"},{"authorName":"孙晓娜","id":"e509e949-a751-487a-9651-970d007f4a4b","originalAuthorName":"孙晓娜"},{"authorName":"李刚","id":"3af2619e-1e70-48d1-8e64-dbbcd8186029","originalAuthorName":"李刚"},{"authorName":"赵建龙","id":"51de79ec-2dcc-470b-946d-61794c31c4ff","originalAuthorName":"赵建龙"}],"doi":"10.3969/j.issn.1007-4252.2010.05.011","fpage":"471","id":"1ef72bc2-8e58-47b8-8bc6-9ed1c46bcd93","issue":"5","journal":{"abbrevTitle":"GNCLYQJXB","coverImgSrc":"journal/img/cover/GNCLYQJXB.jpg","id":"34","issnPpub":"1007-4252","publisherId":"GNCLYQJXB","title":"功能材料与器件学报   "},"keywords":[{"id":"16e08c4c-728a-4db2-b5b4-56479a16a7e2","keyword":"<span style=\"color:red\">柔性</span>基底","originalKeyword":"柔性基底"},{"id":"e45be6e4-0dea-4cd5-8f70-1d94bc8eeb1d","keyword":"神经<span style=\"color:red\">微电极</span>","originalKeyword":"神经微电极"},{"id":"4537c294-be25-4188-9e43-a1af92c2cbe5","keyword":"电镀","originalKeyword":"电镀"},{"id":"1c440214-42e6-42fd-bf4d-a5d44c48c07d","keyword":"互连","originalKeyword":"互连"}],"language":"zh","publisherId":"gnclyqjxb201005011","title":"植入式<span style=\"color:red\">柔性</span>神经<span style=\"color:red\">微电极</span>的互连方法","volume":"16","year":"2010"},{"abstractinfo":"介绍了近十年来各种组合式<span style=\"color:red\">微电极</span>的最新发展,总结了组合式<span style=\"color:red\">微电极</span>的类型、制作材料和方法,组合式<span style=\"color:red\">微电极</span>的性质及研究方法,重点介绍其应用领域.","authors":[{"authorName":"郑金","id":"bd1e2729-fc65-4854-8ec0-06fbd341de43","originalAuthorName":"郑金"},{"authorName":"印仁和","id":"dbd3d29a-fb12-4b36-a6c4-ebe88d9a502c","originalAuthorName":"印仁和"},{"authorName":"钟庆东","id":"80d2869d-f862-4042-806b-1c7b72dd75c8","originalAuthorName":"钟庆东"},{"authorName":"周国定","id":"502cc2f0-875b-4167-9e8d-22175b9aeb57","originalAuthorName":"周国定"}],"doi":"10.3969/j.issn.1005-748X.2003.08.002","fpage":"327","id":"2e9d2c22-979c-4f2b-bffd-b8a736583779","issue":"8","journal":{"abbrevTitle":"FSYFH","coverImgSrc":"journal/img/cover/FSYFH.jpg","id":"25","issnPpub":"1005-748X","publisherId":"FSYFH","title":"腐蚀与防护"},"keywords":[{"id":"89250287-8c55-4b7a-8dc9-e920ff6190eb","keyword":"<span style=\"color:red\">微电极</span>","originalKeyword":"微电极"},{"id":"4f44f91e-b57e-436f-8024-6612702ced10","keyword":"组合式<span style=\"color:red\">微电极</span>","originalKeyword":"组合式微电极"},{"id":"d492e09c-ef1c-4a27-8097-34e4dc32bfb3","keyword":"发展","originalKeyword":"发展"}],"language":"zh","publisherId":"fsyfh200308002","title":"组合式<span style=\"color:red\">微电极</span>的研究进展","volume":"24","year":"2003"},{"abstractinfo":"本文提出了一种简易、低成本的钨丝<span style=\"color:red\">微电极</span>阵列制作工艺和方法.该方法采用MEMS工艺制作的玻璃模具实现钨丝阵列的精密有序排列,同时,在钨丝<span style=\"color:red\">电极</span>表面涂覆一层光敏性的聚酰亚胺作为绝缘层,结合\"双面光刻\"技术和电化学腐蚀技术实现<span style=\"color:red\">电极</span>位点大小和<span style=\"color:red\">电极</span>丝几何尺寸的精确控制.最后,通过注模、光刻制作SU-8固定座体完成钨丝<span style=\"color:red\">微电极</span>阵列的组装固定.整个制作工艺简单快速,且玻璃模具可重复使用,大大降低了制作成本.此外,本文还测试和评价了所制作<span style=\"color:red\">微电极</span>的表面形貌、电学性能以及生物相容性.","authors":[{"authorName":"姚源","id":"6ff0be43-158d-421f-8d31-23dc0f9f8edc","originalAuthorName":"姚源"},{"authorName":"李刚","id":"a3f5d1fc-7403-498b-b842-b50719b1a655","originalAuthorName":"李刚"},{"authorName":"张华","id":"32f60534-f4a2-45c6-bb33-7417815c2ceb","originalAuthorName":"张华"},{"authorName":"周洪波","id":"3d30a4bd-d59a-48b2-94a4-2716f574e928","originalAuthorName":"周洪波"},{"authorName":"孙晓娜","id":"e50b7190-9547-415e-bf8f-850fcc2ac463","originalAuthorName":"孙晓娜"},{"authorName":"朱壮晖","id":"6b0de3f1-45eb-4cd7-9da6-1f9fcf5cd99f","originalAuthorName":"朱壮晖"},{"authorName":"隋晓红","id":"df5981b4-aede-48d4-9c59-b2b2dc1542dc","originalAuthorName":"隋晓红"},{"authorName":"赵建龙","id":"47956295-0a80-4cca-b56f-eb3b195296aa","originalAuthorName":"赵建龙"}],"doi":"10.3969/j.issn.1007-4252.2009.01.004","fpage":"20","id":"560f4d30-ed25-4bb3-b0fd-44ef5f10de35","issue":"1","journal":{"abbrevTitle":"GNCLYQJXB","coverImgSrc":"journal/img/cover/GNCLYQJXB.jpg","id":"34","issnPpub":"1007-4252","publisherId":"GNCLYQJXB","title":"功能材料与器件学报   "},"keywords":[{"id":"af80953f-63f3-44d7-8839-99187f9f92ab","keyword":"微细加工","originalKeyword":"微细加工"},{"id":"e1e1a70d-197a-41f6-99a7-3c4641f19241","keyword":"钨丝","originalKeyword":"钨丝"},{"id":"ab2f2757-bfa1-487d-a047-b4a8e8cc1df0","keyword":"<span style=\"color:red\">微电极</span>阵列","originalKeyword":"微电极阵列"},{"id":"8fccc752-4416-4bcb-bcca-c612086d7485","keyword":"神经探针","originalKeyword":"神经探针"},{"id":"dcfe0666-993d-4a1e-bf74-5326c03b112f","keyword":"双面光刻","originalKeyword":"双面光刻"}],"language":"zh","publisherId":"gnclyqjxb200901004","title":"钨丝<span style=\"color:red\">微电极</span>阵列的简易制备方法","volume":"15","year":"2009"},{"abstractinfo":"采用动电位极化、交流阻抗(EIS)和电化学噪声(ECN)等电化学方法研究了304不锈钢<span style=\"color:red\">微电极</span>的腐蚀行为。实验结果表明：极限扩散电流密度与<span style=\"color:red\">电极</span>尺寸之间具有非线性关系，随着<span style=\"color:red\">电极</span>面积的减小，极限扩散电流密度增大，溶液阻抗减小，双电层电容增大，自腐蚀电位负移，腐蚀电流密度增大。电化学噪声谱表明，随着<span style=\"color:red\">电极</span>面积减小，亚稳态点蚀噪声峰的频度降低，亚稳态点蚀的发生存在一个临界尺寸。","authors":[{"authorName":"黄文静","id":"95ac34a1-3a7b-448d-a453-3b9c95504a3e","originalAuthorName":"黄文静"},{"authorName":"黄华良","id":"913a46f2-5874-4c3c-a8da-15f39fb1e872","originalAuthorName":"黄华良"},{"authorName":"邱于兵","id":"cbf53307-6c68-4d7b-9a6f-be80d629200e","originalAuthorName":"邱于兵"},{"authorName":"陈振宇","id":"244d9803-3032-4646-94d7-9d2a5316c9a4","originalAuthorName":"陈振宇"},{"authorName":"郭兴蓬","id":"ddcd4988-d9d8-4e99-b440-cc4fa3c34ad3","originalAuthorName":"郭兴蓬"}],"categoryName":"|","doi":"","fpage":"141","id":"07e93f86-7dea-4f4d-b0cb-3b4d367787cf","issue":"2","journal":{"abbrevTitle":"ZGFSYFHXB","coverImgSrc":"journal/img/cover/中国腐蚀封面19-3期-01.jpg","id":"81","issnPpub":"1005-4537","publisherId":"ZGFSYFHXB","title":"中国腐蚀与防护学报"},"keywords":[{"id":"4aa123c2-df01-4d13-9ce2-da5f30c814a8","keyword":"304不锈钢","originalKeyword":"304不锈钢"},{"id":"4b1fdf21-822e-4650-954a-4deec1cb38bd","keyword":"micro-electrode","originalKeyword":"micro-electrode"},{"id":"ce3319d6-1a90-4db6-a69f-367897bcc3a4","keyword":"size effect","originalKeyword":"size effect"},{"id":"2294ebfc-ea29-4a8f-82fa-855f47e77cad","keyword":"potentiodynamic polarization","originalKeyword":"potentiodynamic polarization"},{"id":"e9985bb7-6426-435c-bcad-4884ca608c09","keyword":"EIS","originalKeyword":"EIS"},{"id":"436911ba-e115-4208-97f0-110b8db34f3a","keyword":"ECN","originalKeyword":"ECN"}],"language":"zh","publisherId":"1005-4537_2010_2_7","title":"尺寸效应对<span style=\"color:red\">微电极</span>腐蚀行为的影响","volume":"30","year":"2010"},{"abstractinfo":"扫描<span style=\"color:red\">微电极</span>法测定金属微区腐蚀电位及电流密度分布是研究金属局部腐蚀的重要手段。本文在评述了目前利用扫描<span style=\"color:red\">电极</span>测量金属表面电位分布的各种方法基础上,建立了新的实验系统。文中阐述了本方法的电化学理论基础,提出了获得外径低达数微米且具有良好电化学性能的 Ag/igCl参比<span style=\"color:red\">电极</span>,设计制造了微参比<span style=\"color:red\">电极</span>在样品表面附近自动扫描的机械装置,研制了具有高输入阻抗,强抗干扰能力的电位分布测定仪器,还介绍了测量电流密度分布等方法。本实验系统具有较高的测量精度,整套装置简易可行,能满足测量实际腐蚀体系的要求。","authors":[{"authorName":"田昭武","id":"b058a07c-f92b-4358-b954-c10438a5d25b","originalAuthorName":"田昭武"},{"authorName":"林昌健","id":"8687bd57-7051-47de-a566-cf407af31376","originalAuthorName":"林昌健"},{"authorName":"卓向东","id":"c87368bb-b177-4e05-985e-352b9692d107","originalAuthorName":"卓向东"}],"categoryName":"|","doi":"","fpage":"1","id":"c749a4f7-a06a-4b0a-b23c-7dab8e410299","issue":"4","journal":{"abbrevTitle":"ZGFSYFHXB","coverImgSrc":"journal/img/cover/中国腐蚀封面19-3期-01.jpg","id":"81","issnPpub":"1005-4537","publisherId":"ZGFSYFHXB","title":"中国腐蚀与防护学报"},"keywords":[],"language":"zh","publisherId":"1005-4537_1982_4_1","title":"扫描<span style=\"color:red\">微电极</span>法测量金属微区腐蚀电位电流分布——Ⅰ  扫描<span style=\"color:red\">微电极</span>测量系统","volume":"2","year":"1982"},{"abstractinfo":"用研磨抛光的方法制备了Pt研磨<span style=\"color:red\">微电极</span>(φ 0.1 mm),将其用于研究Bi2O3粉末在强碱性溶液中的循环伏安行为,结果表明,Pt研磨<span style=\"color:red\">微电极</span>可以大幅度提高测量速度. SEM研究表明,该<span style=\"color:red\">电极</span>上的Bi2O3粉末在9 mol/L溶液中连续浸泡15 h,并进行10周循环伏安扫描后<span style=\"color:red\">电极</span>上仍有Bi2O3粉末存在. 在研磨<span style=\"color:red\">微电极</span>和粉末<span style=\"color:red\">微电极</span>上所作的循环伏安曲线在Bi2O3的还原/氧化峰电位、峰电流变化规律等方面有较好的一致性,表明可以用研磨<span style=\"color:red\">微电极</span>代替粉末<span style=\"color:red\">微电极</span>进行电化学实验. OH- 浓度对Bi2O3的循环伏安行为有影响,说明KOH参与了Bi2O3的电化学反应,从而证明文献中使用粉末<span style=\"color:red\">微电极</span>所得循环伏安曲线出现的氧化平台是由于<span style=\"color:red\">电极</span>凹槽中OH-浓度持续变化造成的,而盘状研磨<span style=\"color:red\">微电极</span>上不存在凹槽,其循环伏安曲线上不出现平台.","authors":[{"authorName":"袁中直","id":"5fda7551-0ea4-4df9-af00-cf0b25647496","originalAuthorName":"袁中直"},{"authorName":"周震涛","id":"c0f7d8ac-36e1-415e-9feb-a2167138d8bb","originalAuthorName":"周震涛"},{"authorName":"李伟善","id":"bbf9bd01-0ff9-4a9c-8ad9-23529ad9e622","originalAuthorName":"李伟善"}],"doi":"10.3969/j.issn.1000-0518.2004.03.009","fpage":"251","id":"e3e23eab-06e7-4b34-acee-a15be52e274e","issue":"3","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"1c9d0cd5-1da6-46b1-8fae-b000360a8830","keyword":"<span style=\"color:red\">微电极</span>","originalKeyword":"微电极"},{"id":"67702bff-db11-41ea-bd0e-6b72aeda0950","keyword":"氧化铋","originalKeyword":"氧化铋"},{"id":"564fa813-e5fb-4e05-959d-513b2dad489d","keyword":"循环伏安","originalKeyword":"循环伏安"}],"language":"zh","publisherId":"yyhx200403009","title":"用研磨<span style=\"color:red\">微电极</span>研究Bi2O3的循环伏安行为","volume":"21","year":"2004"},{"abstractinfo":"采用电化学阳极氧化和高温碳酸盐氧化两种方法制备 IrO2-pH<span style=\"color:red\">微电极</span>，其特点是对氢离子响应快、线性范围宽、机械性能好、具有长期稳定性 .考察了该<span style=\"color:red\">电极</span>的pH响应特性、化学成分、机械性能等.结果表明，这种IrO2-pH<span style=\"color:red\">微电极</span> 适用于钢筋/混凝土界面pH值的原位测量.","authors":[{"authorName":"黄若双","id":"361780bf-6ab1-42d5-8a20-b8feb145dfd4","originalAuthorName":"黄若双"},{"authorName":"胡融刚","id":"ba9f133c-0aa0-4056-974a-76563a45c0a5","originalAuthorName":"胡融刚"},{"authorName":"杜荣归等","id":"911b95cf-55ba-4dd6-b312-791037676f79","originalAuthorName":"杜荣归等"}],"categoryName":"|","doi":"","fpage":"305","id":"d246b5e4-ae1c-4691-940c-dce46e7a2367","issue":"5","journal":{"abbrevTitle":"FSXB","coverImgSrc":"journal/img/cover/腐蚀学报封面.jpg","id":"24","issnPpub":"2667-2669","publisherId":"FSXB","title":"腐蚀学报（英文）"},"keywords":[{"id":"39fc24fb-c81d-4ec7-94df-b77a2f7bfd5c","keyword":"IrO2<span style=\"color:red\">电极</span>","originalKeyword":"IrO2电极"},{"id":"1421d3db-5ed5-45a6-a999-9692c2eae748","keyword":"pH","originalKeyword":"pH"},{"id":"b528e41e-8e9f-4897-8f29-44cbb2273afb","keyword":"steel/concrete","originalKeyword":"steel/concrete"},{"id":"6d1f9edb-dd74-4391-8845-9778c6fb2495","keyword":"interface","originalKeyword":"interface"}],"language":"zh","publisherId":"1002-6495_2002_5_1","title":"IrO2-pH<span style=\"color:red\">微电极</span>的研制及钢筋/混凝土界面pH的测量","volume":"14","year":"2002"},{"abstractinfo":"采用电化学阳极氧化和高温碳酸盐氧化两种方法制备IrO2-pH<span style=\"color:red\">微电极</span>,其特点是对氢离子响应快、线性范围宽、机械性能好、具有长期稳定性.考察了该<span style=\"color:red\">电极</span>的pH响应特性、化学成分、机械性能等.结果表明,这种IrO2-pH<span style=\"color:red\">微电极</span>适用于钢筋/混凝土界面pH值的原位测量.","authors":[{"authorName":"黄若双","id":"679cddb0-4d6d-4e9c-8866-7af7218f9232","originalAuthorName":"黄若双"},{"authorName":"胡融刚","id":"58c94dca-4dc0-48b9-ae85-9ca33f5d786f","originalAuthorName":"胡融刚"},{"authorName":"杜荣归","id":"54a81bd4-3a82-405f-91e8-94e4f58a3a45","originalAuthorName":"杜荣归"},{"authorName":"谭建光","id":"aee8f803-fa11-4f04-877c-b5bd34afa451","originalAuthorName":"谭建光"},{"authorName":"林昌健","id":"fbaf3289-6f87-41e5-b6e3-d31698f6c230","originalAuthorName":"林昌健"}],"doi":"10.3969/j.issn.1002-6495.2002.05.016","fpage":"305","id":"88abe1ec-9654-489b-96ff-15ed27cc64be","issue":"5","journal":{"abbrevTitle":"FSXB","coverImgSrc":"journal/img/cover/腐蚀学报封面.jpg","id":"24","issnPpub":"2667-2669","publisherId":"FSXB","title":"腐蚀学报（英文）"},"keywords":[{"id":"e63a934e-17a4-4d5f-8c66-caf35537a4c0","keyword":"IrO2<span style=\"color:red\">电极</span>","originalKeyword":"IrO2电极"},{"id":"9ec26001-806c-44bc-a3f4-ad0333a69cd2","keyword":"pH","originalKeyword":"pH"},{"id":"d1a0f499-b3ac-43fb-bde8-c302fa97349a","keyword":"钢筋/混凝土","originalKeyword":"钢筋/混凝土"},{"id":"3fd2bd70-11c8-465a-8f1d-2d52e746e524","keyword":"原位测量","originalKeyword":"原位测量"},{"id":"de19548b-49f8-4d7f-a069-7dc4802f71a9","keyword":"腐蚀破坏","originalKeyword":"腐蚀破坏"}],"language":"zh","publisherId":"fskxyfhjs200205016","title":"IrO2-pH<span style=\"color:red\">微电极</span>的研制及钢筋/混凝土界面pH的测量","volume":"14","year":"2002"},{"abstractinfo":"用研磨<span style=\"color:red\">微电极</span>研究了尖晶石锂锰氧化物在1mol/L LiPF6/EC+DMC+EMC(1:1:1)电解液中的循环伏安行为,并用SEM分析了<span style=\"color:red\">电极</span>的表面形貌和锰元素分布.结果表明,尖晶石锂锰氧化物在研磨<span style=\"color:red\">微电极</span>上较在粉末<span style=\"color:red\">微电极</span>上稳定,嵌脱锂离子过程也更可逆.比较发现,固态法合成的尖晶石锂锰氧化物的循环稳定性较溶胶-凝胶法合成的要好,这一结果与XRD结晶度分析结果吻合,说明研磨<span style=\"color:red\">微电极</span>能够快速有效地评价尖晶石锂锰氧化物的循环稳定性及锂离子嵌脱过程的可逆性.","authors":[{"authorName":"周豪杰","id":"12b64686-86cb-45b0-b0c6-bba2d66214cd","originalAuthorName":"周豪杰"},{"authorName":"吕东生","id":"5e2bd93e-a0d9-4348-93d0-0e9bbd67c341","originalAuthorName":"吕东生"},{"authorName":"许梦清","id":"a390cc21-eadc-4e38-a1e8-bc79dfea5d44","originalAuthorName":"许梦清"},{"authorName":"李伟善","id":"b1917c4e-b64c-40ce-842a-88dc1573f42f","originalAuthorName":"李伟善"}],"doi":"10.3321/j.issn:1000-324X.2006.01.018","fpage":"109","id":"c4756c95-9b49-44b4-b864-d77db95e271d","issue":"1","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"9ffda055-4f8a-4963-bdb0-77cbe708ab0f","keyword":"研磨<span style=\"color:red\">微电极</span>","originalKeyword":"研磨微电极"},{"id":"cbc468ca-f0db-4647-a066-a722c4fd3bcf","keyword":"循环伏安","originalKeyword":"循环伏安"},{"id":"5bf6bd58-e1b3-40e2-b888-5b6335c40ae1","keyword":"尖晶石锂锰氧化物","originalKeyword":"尖晶石锂锰氧化物"}],"language":"zh","publisherId":"wjclxb200601018","title":"用研磨<span style=\"color:red\">微电极</span>研究LiMn2O4的循环伏安行为","volume":"21","year":"2006"}],"totalpage":619,"totalrecord":6188}