{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"以不同锌盐为原料,以NaOH、NH3·H2O为沉淀剂,以三乙醇胺和十二烷基硫酸钠为分散剂,采用沸腾回流、微波加热、恒温陈化等温和条件方法制备出了不同形貌的纳微氧化锌;采用X射线衍射仪、透射电镜和扫描电镜等对产物进行了表征.结果表明:产物均为纯氧化锌,具有六方纤锌矿结构;以NH3·H2O为沉淀剂,可制备出纺锤形氧化锌;以NaOH为沉淀剂、硫酸锌为原料可制备出片状氧化锌;而以硝酸锌、醋酸锌、氯化锌为原料制备的氧化锌为针形和棒状;微波加热可得到长0.5 μm、宽0.1μm的短棒,100℃恒温陈化可得到针形超细颗粒.","authors":[{"authorName":"程敬泉","id":"5d2bb546-f8bf-4c2b-9a1e-dc646ece5bd8","originalAuthorName":"程敬泉"},{"authorName":"<span style=\"color:red\">高</span><span style=\"color:red\">焕</span><span style=\"color:red\">君</span>","id":"b9919aa5-911c-49cd-9625-5582a2e11d41","originalAuthorName":"高焕君"}],"doi":"","fpage":"67","id":"5a88ed40-267a-40ff-a7c1-28742e36c583","issue":"2","journal":{"abbrevTitle":"JXGCCL","coverImgSrc":"journal/img/cover/JXGCCL.jpg","id":"45","issnPpub":"1000-3738","publisherId":"JXGCCL","title":"机械工程材料"},"keywords":[{"id":"bd22408f-f2d5-4615-affa-96537e84cf0c","keyword":"氧化锌","originalKeyword":"氧化锌"},{"id":"646c05a0-6bfc-4c40-a3e9-db03098c97c0","keyword":"温和条件","originalKeyword":"温和条件"},{"id":"3b4701a3-8af4-4fc5-84d1-46c6d234605e","keyword":"形貌","originalKeyword":"形貌"},{"id":"19155ecd-694a-4086-ace5-a3cd5e77f5b4","keyword":"尺寸","originalKeyword":"尺寸"}],"language":"zh","publisherId":"jxgccl201102018","title":"不同温和条件下制备纳微氧化锌的形貌及尺寸","volume":"35","year":"2011"},{"abstractinfo":"","authors":[],"doi":"","fpage":"25","id":"0bf08538-745e-4be6-a77a-e73f8449dda8","issue":"2","journal":{"abbrevTitle":"SHJS","coverImgSrc":"journal/img/cover/SHJS.jpg","id":"59","issnPpub":"1001-7208","publisherId":"SHJS","title":"上海金属"},"keywords":[{"id":"109e7d2e-ad21-4dae-bd81-f25b506d6827","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"shjs200402018","title":"新日铁<span style=\"color:red\">君</span>津厂4号高炉重新点火","volume":"26","year":"2004"},{"abstractinfo":"","authors":[{"authorName":"崔红","id":"15e3f532-3724-445f-9e18-5342678c1a44","originalAuthorName":"崔红"},{"authorName":"肖志超","id":"9c8a5db7-68d1-4844-85b9-a33341e5d258","originalAuthorName":"肖志超"}],"doi":"10.3969/j.issn.1007-8827.2004.03.014","fpage":"239","id":"b9219767-2bea-4cc0-bea2-0829bcae187d","issue":"3","journal":{"abbrevTitle":"XXTCL","coverImgSrc":"journal/img/cover/XXTCL.jpg","id":"70","issnPpub":"1007-8827","publisherId":"XXTCL","title":"新型炭材料"},"keywords":[{"id":"a4c6240f-f26b-44ea-aa78-1605d33acf79","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"xxtcl200403014","title":"苏<span style=\"color:red\">君</span>明高工和他的研究活动","volume":"19","year":"2004"},{"abstractinfo":"改变常规镀锌钝化液成膜剂和pH值调整剂,研制出了一种新型<span style=\"color:red\">高</span>耐蚀性钝化工艺.此工艺形成的钝化膜铬含量:Cr(Ⅲ) 0.10 mg/dm2 Cr(Ⅳ) 2.277 mg/dm2 膜重 10.8 mg/dm2.在钝化膜形成后即使未干燥也有较高的抗摩擦性能,同时该膜也具有优异的耐酸碱性能,耐中性盐雾试验可达200 h不出现白锈.","authors":[{"authorName":"刘立炳","id":"6f39ce0a-32c8-4c07-83fd-1d41ca1d33de","originalAuthorName":"刘立炳"},{"authorName":"孙贺民","id":"6e955ca2-f25f-42c9-b50b-a10346d8d73b","originalAuthorName":"孙贺民"},{"authorName":"赵常就","id":"ce60c7fb-f3c5-4443-ad47-ebdeecafe34a","originalAuthorName":"赵常就"},{"authorName":"陈范才","id":"09557497-9030-47c0-9b1f-f8c3e6522a25","originalAuthorName":"陈范才"}],"doi":"10.3969/j.issn.1001-1560.1999.05.006","fpage":"10","id":"1c23cca2-a79b-4fe7-afe4-36967d43cfc6","issue":"5","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"3d1a4044-ff78-4c4d-973d-b1a87c9f5a06","keyword":"镀锌","originalKeyword":"镀锌"},{"id":"9d4b7f9a-2865-4012-8249-aff12b754ea5","keyword":"钝化","originalKeyword":"钝化"},{"id":"c0250205-4b68-4147-ba99-12652fdeb02f","keyword":"耐腐蚀性","originalKeyword":"耐腐蚀性"}],"language":"zh","publisherId":"clbh199905006","title":"<span style=\"color:red\">高</span>耐蚀镀锌钝化","volume":"32","year":"1999"},{"abstractinfo":"介绍了<span style=\"color:red\">高</span>铬<span style=\"color:red\">高</span>钴耐热钢成分设计的理论,研究了耐热钢的微观组织、热处理工艺和力学性能;根据裂纹产生的机制,通过实验的方法建立了恰当的热处理工艺,有效地防止了淬火裂纹的产生.研究表明,通过科学的成分设计和热处理的<span style=\"color:red\">高</span>铬<span style=\"color:red\">高</span>钴耐热钢具有良好的综合力学性能.","authors":[{"authorName":"郭存宝","id":"25e5eeec-0064-4274-b043-4b39bc1d752a","originalAuthorName":"郭存宝"},{"authorName":"龙思远","id":"d80a87e2-90b4-4609-b029-62ec588a2e13","originalAuthorName":"龙思远"},{"authorName":"廖慧敏","id":"b1b0df7f-b01b-40a4-9064-4e66458b284d","originalAuthorName":"廖慧敏"}],"doi":"","fpage":"423","id":"c8a3e764-a7f1-4913-b6d8-c929c225585a","issue":"z1","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"82810b10-af73-459c-b409-41356af934bb","keyword":"耐热钢","originalKeyword":"耐热钢"},{"id":"8ac141bb-5575-48ea-a535-f1a6e5f87911","keyword":"强化理论","originalKeyword":"强化理论"},{"id":"7ed2a4ef-7ff0-4559-b3dd-40be80c98b22","keyword":"DV-Xa分子轨道法","originalKeyword":"DV-Xa分子轨道法"},{"id":"ad505c41-f4b8-461d-af29-5a3b7fbe24f4","keyword":"热处理工艺","originalKeyword":"热处理工艺"}],"language":"zh","publisherId":"cldb2008z1129","title":"<span style=\"color:red\">高</span>铬<span style=\"color:red\">高</span>钴耐热钢的研究","volume":"22","year":"2008"},{"abstractinfo":"本文介绍了新型矿物添加材料赛<span style=\"color:red\">高</span>岭(Metakolin)的物理性能,化学成分,采用ASTM C39,ASTM C1202,稳态迁移等方法着重研究了赛<span style=\"color:red\">高</span>岭混凝土的抗压强度和抗氯离子性能,并与硅粉混凝土及对比波特兰水泥混凝土的有关性能作了比较,探讨了赛<span style=\"color:red\">高</span>岭作为硅粉替代材料生产<span style=\"color:red\">高</span>功能混凝土的可能性.","authors":[{"authorName":"蒋林华","id":"dd749bf4-6ec1-434d-8ebc-1acb0be0b7d4","originalAuthorName":"蒋林华"}],"doi":"10.3969/j.issn.1001-1625.2001.05.011","fpage":"51","id":"0d3fb318-d7bf-498b-a4ed-923c8549c9aa","issue":"5","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报   "},"keywords":[{"id":"f91221d9-da38-4299-a79c-ad5d348463fb","keyword":"赛<span style=\"color:red\">高</span>岭","originalKeyword":"赛高岭"},{"id":"24ccce66-2bba-47d1-bd5b-06c25a9810bc","keyword":"硅粉","originalKeyword":"硅粉"},{"id":"aa5bb8eb-5846-405e-bf9a-b5dfa40c4e30","keyword":"混凝土","originalKeyword":"混凝土"},{"id":"7656cc44-ccf7-419b-89a2-cb8e3b98d53a","keyword":"性能","originalKeyword":"性能"}],"language":"zh","publisherId":"gsytb200105011","title":"赛<span style=\"color:red\">高</span>岭混凝土研究","volume":"20","year":"2001"},{"abstractinfo":"<span style=\"color:red\">高</span>纯钴主要应用于磁记录材料、磁传感器材料、光电材料等高技术领域.其制备方法有萃取法、离子交换法、电解法、真空熔炼法等.萃取法和离子交换法能够制备<span style=\"color:red\">高</span>纯盐, 这是制备<span style=\"color:red\">高</span>纯钴的重要环节.<span style=\"color:red\">高</span>纯钴盐通过沉淀、氢还原或电解能获得<span style=\"color:red\">高</span>纯金属原料, 该过程也将金属进一步提纯.真空熔炼法能够进一步提纯金属, 并得到性能优异的金属锭.采用几种方法结合的工艺路线可以制备出品质优良的<span style=\"color:red\">高</span>纯材料.","authors":[{"authorName":"陈蓉","id":"98ce9af8-9406-4938-922c-18ecde6bed5f","originalAuthorName":"陈蓉"},{"authorName":"王力军","id":"cf76c8fe-17ca-4520-8621-e2c05b9b174c","originalAuthorName":"王力军"},{"authorName":"罗远辉","id":"1b53adc4-cbda-42b6-aca0-68a6dd0e2d44","originalAuthorName":"罗远辉"},{"authorName":"张力","id":"fbfb43b4-a869-40d9-99bb-c9c878849c28","originalAuthorName":"张力"},{"authorName":"陈松","id":"833018c9-94d0-4ca8-8e3f-85f6c3836d61","originalAuthorName":"陈松"},{"authorName":"韩林","id":"c2971562-454c-4a36-b2a9-61821e47fc32","originalAuthorName":"韩林"}],"doi":"10.3969/j.issn.0258-7076.2005.05.043","fpage":"797","id":"3956c55f-58ec-4703-afd1-9a523af04a52","issue":"5","journal":{"abbrevTitle":"XYJS","coverImgSrc":"journal/img/cover/XYJS.jpg","id":"67","issnPpub":"0258-7076","publisherId":"XYJS","title":"稀有金属"},"keywords":[{"id":"69952c2c-6965-4ad8-92c7-450421ec9087","keyword":"<span style=\"color:red\">高</span>纯钴","originalKeyword":"高纯钴"},{"id":"d31fc244-f68b-4e76-b2e7-70069c919ea3","keyword":"萃取","originalKeyword":"萃取"},{"id":"4ac104a9-eb8c-469f-b537-493a100251c4","keyword":"离子交换","originalKeyword":"离子交换"},{"id":"194ef3cf-12c1-424b-b15d-9bc6aa1c49a9","keyword":"电解","originalKeyword":"电解"},{"id":"7e1c90f2-8949-452f-be43-5aa40155e141","keyword":"真空熔炼","originalKeyword":"真空熔炼"}],"language":"zh","publisherId":"xyjs200505043","title":"<span style=\"color:red\">高</span>纯钴制备技术","volume":"29","year":"2005"},{"abstractinfo":"紫金黄金冶炼厂以湿法萃取工艺作为<span style=\"color:red\">高</span>纯金的生产工艺,利用电解粗金泥、湿法金泥和合质金为原料分别进行了试验研究. 其结果表明:以电解粗金泥作为原料可以生产出总成色Au>99 . 999 %的<span style=\"color:red\">高</span>纯金,但Cu元素超出了<span style=\"color:red\">高</span>纯金的标准;而以湿法金泥和合质金( Au>99 %)作为生产原料能够生产出合格的<span style=\"color:red\">高</span>纯金,23种杂质元素全部达到<span style=\"color:red\">高</span>纯金的标准.","authors":[{"authorName":"孙根荣","id":"3cf40340-e731-45db-8072-579b6a8187d9","originalAuthorName":"孙根荣"}],"doi":"10.11792/hj20151114","fpage":"61","id":"f9190fe0-b8d3-4599-909d-a453ce0ea7d3","issue":"11","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"9f65b604-02c3-4b6f-a041-0ef84ea28ff2","keyword":"<span style=\"color:red\">高</span>纯金","originalKeyword":"高纯金"},{"id":"a9a8561c-879a-43f9-882a-03d54ca406a8","keyword":"合质金","originalKeyword":"合质金"},{"id":"a936bb52-9b79-43b7-9c5a-3ce47059c0f0","keyword":"湿法萃取","originalKeyword":"湿法萃取"},{"id":"86d7bcfd-b8f0-4c8e-835d-222dd1dfc6b2","keyword":"精炼工艺","originalKeyword":"精炼工艺"}],"language":"zh","publisherId":"huangj201511015","title":"<span style=\"color:red\">高</span>纯金精炼试验研究","volume":"36","year":"2015"},{"abstractinfo":"有关<span style=\"color:red\">高</span>酸度磷化的成膜机理目前有多种看法,作者用电离平衡和电化学原理分析了<span style=\"color:red\">高</span>酸度条件下磷化膜形成机理,讨论了磷酸的特性及其在成膜中所起的作用,分析表明,磷酸的缓冲作用和粘稠性有利于<span style=\"color:red\">高</span>酸度磷化.","authors":[{"authorName":"曾仁森","id":"9dda3891-1253-4404-878f-5ef8c5478a40","originalAuthorName":"曾仁森"}],"doi":"10.3969/j.issn.1001-1560.2000.05.019","fpage":"39","id":"d9c783e9-9c7a-4eac-8e44-35eaec2ced0f","issue":"5","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"71459f55-e451-446b-9bc4-dd68f145abab","keyword":"磷化","originalKeyword":"磷化"},{"id":"cb02d80e-5f9e-4628-b5a6-20c45008b3dc","keyword":"<span style=\"color:red\">高</span>酸度","originalKeyword":"高酸度"},{"id":"8890bb91-4161-4c05-ad0e-4247248ba55a","keyword":"氧化","originalKeyword":"氧化"},{"id":"c3f57e65-8828-4bf7-8335-f6e46efde4d7","keyword":"机理","originalKeyword":"机理"}],"language":"zh","publisherId":"clbh200005019","title":"<span style=\"color:red\">高</span>酸度磷化机理分析","volume":"33","year":"2000"},{"abstractinfo":"介绍了遂昌金矿有限公司的<span style=\"color:red\">高</span>纯金电解工艺。实践表明，采用该工艺，在金阳极板含金95%~99%下经过一次金电解，金纯度即可达到99.997%以上。经检测，杂质含量低于<span style=\"color:red\">高</span>纯金(99.999%)的杂质要求。","authors":[{"authorName":"叶跃威","id":"0c28e070-3642-409f-a88b-0140ca2cfeb0","originalAuthorName":"叶跃威"}],"doi":"","fpage":"23","id":"c8ed43b5-f16d-4f32-a771-f1e1d6fc2b94","issue":"1","journal":{"abbrevTitle":"GJS","coverImgSrc":"journal/img/cover/GJS.jpg","id":"38","issnPpub":"1004-0676","publisherId":"GJS","title":"贵金属"},"keywords":[{"id":"67518cf9-2307-4836-9b37-f232dd4d6925","keyword":"有色金属冶金","originalKeyword":"有色金属冶金"},{"id":"1df4d7d1-cf95-4426-9236-329cca956430","keyword":"<span style=\"color:red\">高</span>纯金","originalKeyword":"高纯金"},{"id":"dba6329a-2042-47dd-aff0-7791c476a7d0","keyword":"电解","originalKeyword":"电解"}],"language":"zh","publisherId":"gjs201401005","title":"<span style=\"color:red\">高</span>纯金的电解工艺","volume":"","year":"2014"}],"totalpage":2228,"totalrecord":22274}