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TEM OBSERVATION OF NUCLEATION AND GROWTH OF BORIDE DURING BORONIZATION OF STEEL 20 AND INFLUENCE OF PRIOR DEFORMATION

JIANG Bailing LEI Tingquan LIU Wei CUI Yuexian Harbin Institute of Technology , Harbin , China Dept.of Metallic Materials and Technology , Harbin Institute of Technology , Harbin 150006 , China

金属学报(英文版)

The TEM observation on the single-side thinned specimens was made of the nucleation and growth of boride during boronization for steel 20 and the influence of prior room temperature deformation.The results of X-ray diffraction and electron probe microstructure analysis show that only Fe_2B formed in the surface layer of specimens at the beginning of boronization;the atomic concentration of B in the surface layer increased with the increase of deformation monotonously;and the segregation of B atoms in the dislocation cells hindered the recovery and recrystallization of the deformed structure of the matrix and accelerated the nucleation and growth of boride in the surface layer.

关键词: boronization , null , null , null , null , null

20钢渗硼过程中硼化物形核和生长的TEM观察及室温形变的影响

蒋百灵 , 雷廷权 , 刘威 , 崔约贤

金属学报

本文采用单向减薄制样法在透射电镜下直接观察了20钢渗硼初期硼化物的形核和生长特性及室温形变的影响。X射线及电子探针分析结果表明:渗硼初期试样表层仅有Fe_2B形成;表层硼原子浓度与形变量之间具有单调增长的关系;偏聚于位错胞壁之中的硼原子阻碍了形变组织的恢复和再结晶,加速了硼化物的形核和长大。

关键词: 渗硼 , boride , dislocation , nucleation

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