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纳米晶Fe85Si1Al6Cr8扁平状颗粒材料微波吸收特性

邓联文 , 冯则坤 , 江建军 , 何华辉 , 付祺伟 , 熊惟皓

金属学报

采用水雾化工艺和高能球磨处理技术制备纳米晶FeSiAlCr扁平状合金粉。重点研究了高能球磨处理工艺对材料微结构、形貌和微波电磁性能的影响,结果发现高能球磨处理可使球形雾化粉外形扁平化并可细化其晶粒,促使其纳米晶化;从而使FeSiAlCr微粉的微波磁导率得以显著提高,介电常数得以控制。还研究了后续热处理工艺的作用,发现热处理后可以进一步改善其微波电磁性能。采用该材料制作的涂层吸波性能测量结果表明,在4 GHz附近的微波段具有良好吸波性能,有望在抗电磁干扰和微波吸收领域获得广泛应用。

关键词: 纳米晶 , FeSiAlCr alloy , complex permeability , microwave absorber , high energy ball milling

Structure and magnetic properties of Fe-based powders prepared by mechanical alloying

Tingdong ZHOU

金属学报(英文版)

FeSiAlCr alloy powders were prepared by mechanical alloying, the milling time were 20 h, 40 h, 60 h and 80~h, respectively. Powders morphology was studied by SEM. Microstructure of powders milled for various times were analyzed by XRD. The complex permittivity and complex permeability of four powders were tested in the frequency range from 0.5 to 18 GHz, and their microwave absorption properties were analyzed. It was found that the particle size of powders milled for 80~h was less than 2μm. Silicon and aluminum atoms were dissolved into the crystal lattice of iron, and chromium atoms can form alloy with iron atoms. The minimum peak value of reflectivity can reach to -11.3 dB at the frequency of 4.3 GHz for 80 h milling powders, and the other one was -6 dB at 16.5 GHz.

关键词: FeSiAlCr alloy , 固溶体 , 电磁参数 , 反射率 , 机械合金化

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