{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"基于沸石咪唑骨架材料在离子液体和低共熔溶剂中冷却结晶的析出方式,开发了一种离子热法合成沸石咪唑骨架材料的新途径,采用X射线衍射、扫描电镜、核磁共振光谱、红外光谱以及热重分析等方法对制备的产物进行了表征,研究了合成条件对产物结晶度、尺寸和形貌的影响,探讨了沸石咪唑骨架材料在离子热合成体系中的溶解-结晶析出机理。研究发现,冷却速率能够影响产物形貌,急速冷却时, sod (RCSR代码)型产物的形貌为球形, zni (RCSR代码)型产物为棒状或平板状;程序控制冷却时, sod型产物的形貌为多面体, zni型产物呈团簇状。","authors":[{"authorName":"王亚松","id":"19ab8fd4-9e13-4734-a835-55b9051a5469","originalAuthorName":"王亚松"},{"authorName":"徐云鹏","id":"14822bc4-3a2b-423f-a0e9-5acda8bdb864","originalAuthorName":"徐云鹏"},{"authorName":"李大伟","id":"95bf0a96-9742-4422-a582-bf669e89d247","originalAuthorName":"李大伟"},{"authorName":"刘浩","id":"1c61e9ec-4938-4463-924c-a2eb7e6e1cc8","originalAuthorName":"刘浩"},{"authorName":"厉晓蕾","id":"83490ace-3457-4f7b-a1c6-f01f38b901b8","originalAuthorName":"厉晓蕾"},{"authorName":"陶硕","id":"13998f87-29d0-4215-b549-9beb88abae8e","originalAuthorName":"陶硕"},{"authorName":"田志坚","id":"fac96653-360c-413c-bd6d-af7c34c41621","originalAuthorName":"田志坚"}],"doi":"10.1016/S1872-2067(14)60278-3","fpage":"855","id":"769f1f3c-53f4-4222-9a07-e0210d5228bd","issue":"6","journal":{"abbrevTitle":"CHXB","coverImgSrc":"journal/img/cover/CHXB.jpg","id":"18","issnPpub":"0253-9837","publisherId":"CHXB","title":"催化学报 "},"keywords":[{"id":"fc55df3f-49e9-4039-8162-375b06aa3726","keyword":"离子热合成","originalKeyword":"离子热合成"},{"id":"90079d82-4515-4a5b-8273-b7ce5f0835d0","keyword":"沸石咪唑骨架材料","originalKeyword":"沸石咪唑骨架材料"},{"id":"4612cedd-a08c-4eee-af33-993958cb9a2e","keyword":"溶解-结晶机理","originalKeyword":"溶解-结晶机理"},{"id":"d44f4bf7-1e6e-432e-b9d8-4c4a9dfcae96","keyword":"溶解度","originalKeyword":"溶解度"},{"id":"d2ef21bd-be31-46cc-bcc7-7d287e89be48","keyword":"冷却析出","originalKeyword":"冷却析出"}],"language":"zh","publisherId":"cuihuaxb201506011","title":"离子热法合成沸石咪唑骨架材料及其溶解-结晶机理研究","volume":"","year":"2015"},{"abstractinfo":"采用溶胶-凝胶法和在Ar气氛下热分解技术,制得了MgB2超导晶态纳米线.利用XRD对样品进行物相分析,表明有MgB2生成.通过扫描电子显微镜(SEM)对样品进行形貌分析,证实制备出了MgB2纳米线.样品的超导特性通过电阻随温度变化的测量得以证实,其超导临界转变温度Tc为19.4K.此外,对比分析了溶胶-凝胶法粉末和传统固相烧结粉末的异同.","authors":[{"authorName":"杨超伟","id":"9cf1f5e9-f605-48f7-b62b-f2005c4c30de","originalAuthorName":"杨超伟"},{"authorName":"陶硕","id":"e66fb5f2-e8ba-48d5-b2ab-7f388d0859e8","originalAuthorName":"陶硕"},{"authorName":"张志伟","id":"9eaba521-53af-4317-8a21-fea2e72df7ce","originalAuthorName":"张志伟"},{"authorName":"赵晓鹏","id":"80a98993-c7e9-4f25-9714-6bfcffb37a7c","originalAuthorName":"赵晓鹏"}],"doi":"","fpage":"5","id":"9467b78c-d69a-483c-b893-9dc0d29e7fae","issue":"6","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"b95b8300-2880-4c36-be08-5c3f804a43a0","keyword":"溶胶-凝胶法","originalKeyword":"溶胶-凝胶法"},{"id":"71ae3c5d-07c9-4934-9a64-2a0319c9b65e","keyword":"MgB2","originalKeyword":"MgB2"},{"id":"3fc1cd12-c415-4d5b-ad12-7aea566b66e8","keyword":"纳米线","originalKeyword":"纳米线"},{"id":"a8eab8d9-46db-4537-ab96-142d9351104b","keyword":"超导","originalKeyword":"超导"}],"language":"zh","publisherId":"cldb201406002","title":"溶胶-凝胶法制备MgB2超导纳米线","volume":"28","year":"2014"},{"abstractinfo":"采用水冷-强度法测试表征了锂辉石/SiCp紫砂陶试样抗热震性能,结合SEM、XRD等测试分析手段进行物相、微观组织形貌方面分析,在SiCp含量为9%条件下,重点研究锂辉石含量(0 ~32%)对紫砂陶试样力学和热学性质的影响.结果表明,锂辉石含量为16%时,紫砂陶试样抗折强度达到最大值83.37 MPa;含量为24%时,平均热膨胀系数最低,强度保持率达到53.07%最高值,抗热震性能最好;莫来石和β-锂辉石固溶体晶相含量随锂辉石含量增大而增多;试样热震后断口出现裂纹,沿晶断裂是试样断裂的主要方式.","authors":[{"authorName":"王俊","id":"b2065036-a7a1-48ed-b860-964bac5f6da2","originalAuthorName":"王俊"},{"authorName":"王平","id":"ac7c9e29-3030-4649-986e-e42c6e064efb","originalAuthorName":"王平"},{"authorName":"简觉非","id":"de9bb966-9752-4a5a-b1b3-662310f2ac2b","originalAuthorName":"简觉非"},{"authorName":"邓义群","id":"080b5ac0-bcf4-40ae-9cab-d8ddf4c7a58c","originalAuthorName":"邓义群"},{"authorName":"漆小鹏","id":"fabcac37-8993-4a70-9064-84255054e533","originalAuthorName":"漆小鹏"},{"authorName":"李之锋","id":"72ace446-d4f1-41ca-8244-481c30312fb8","originalAuthorName":"李之锋"},{"authorName":"刘斌","id":"27cc64c5-f5cd-4a10-b86b-133059f117d3","originalAuthorName":"刘斌"}],"doi":"","fpage":"28","id":"c35a0944-5153-4dc0-89d1-9e05fdba5b68","issue":"1","journal":{"abbrevTitle":"CLRCLXB","coverImgSrc":"journal/img/cover/CLRCLXB.jpg","id":"15","issnPpub":"1009-6264","publisherId":"CLRCLXB","title":"材料热处理学报"},"keywords":[{"id":"fe1204e4-ec4d-4330-90f3-31c13c476177","keyword":"紫砂陶","originalKeyword":"紫砂陶"},{"id":"3a98193e-dcc7-466c-b199-be1e7b076063","keyword":"锂辉石","originalKeyword":"锂辉石"},{"id":"5f98a863-8bf9-4261-8d99-d0a97627df5c","keyword":"抗折强度","originalKeyword":"抗折强度"},{"id":"a668df5f-f83c-4dbf-9c5b-85f75915b78f","keyword":"抗热震性","originalKeyword":"抗热震性"}],"language":"zh","publisherId":"jsrclxb201401006","title":"锂辉石/SiCp紫砂陶的抗热震性能","volume":"35","year":"2014"},{"abstractinfo":"选取膨润土作为陶瓷基体,以鳞片石墨、预处理石墨及炭黑作为导电原料,碳化硅作为增强原料,经球磨混合、50MPa模压成型和1000℃热处理3h后制备出炭/陶复合电热材料。采用XRD和SEM对其物相组成和微观形貌进行表征,并对其通电发热性能、力学性能和抗氧化性能进行了测试和分析。所制备的炭/陶复合材料具有优异的电热性能,在交流低电压(10V)下即可迅速升温,并在较高温度下保持相对稳定,研制的样品中最高发热温度可达643℃。通过调整碳化硅含量,复合材料抗弯强度可达14.3MPa。通过将炭材料和陶瓷材料复合,可有效改善炭材料的抗氧化性,使其明显氧化失重温度升高200℃左右。","authors":[{"authorName":"魏炜","id":"e731d603-e3de-4b01-8d36-f64dd22603e5","originalAuthorName":"魏炜"},{"authorName":"夏金童","id":"b9f78ac5-05f4-46ac-8f5d-9c3ffd441295","originalAuthorName":"夏金童"},{"authorName":"李劲","id":"65c0b651-b3f4-4a5d-9841-50e438b1ae99","originalAuthorName":"李劲"},{"authorName":"赵敬利","id":"052bb595-8885-4de4-b38e-730c25e7acb0","originalAuthorName":"赵敬利"},{"authorName":"赵庆才","id":"8eee1232-2339-4941-a5c2-e1de3381176c","originalAuthorName":"赵庆才"},{"authorName":"李允柱","id":"538b1f58-6600-4db5-879b-0fdf74a30e98","originalAuthorName":"李允柱"},{"authorName":"刘奉来","id":"daa1d445-05f6-4685-86df-0b180a2414c2","originalAuthorName":"刘奉来"}],"doi":"","fpage":"1619","id":"917e3b84-89ee-4a2d-ac2d-a0f8ba927a29","issue":"9","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"2f6359b2-a032-4147-b962-44c166fc225c","keyword":"炭/陶复合电热材料","originalKeyword":"炭/陶复合电热材料"},{"id":"5c184812-e4a7-40d0-ab01-84dede3fe934","keyword":"电热性能","originalKeyword":"电热性能"},{"id":"ea03768c-adfa-47a8-aea3-3f1d082067c9","keyword":"力学性能","originalKeyword":"力学性能"},{"id":"a6a04b7c-a012-4059-a87b-6e76fa662329","keyword":"抗氧化性能","originalKeyword":"抗氧化性能"}],"language":"zh","publisherId":"gncl201109020","title":"新型炭/陶复合电热材料的研制","volume":"42","year":"2011"},{"abstractinfo":"通过在陶瓷基体原料(高岭土)中添加炭系导电原料(石墨、炭黑),经球磨混合、模压成形和烧结工艺制得炭/陶复合材料.采用X射线衍射(XRD)、扫描电镜(SEM)、数字测温仪等分析和测试了所研制试样的相组成、显微结构以及电热性能.结果表明,本实验的烧结条件下,炭系导电原料不会和陶瓷基体发生反应,其导电性不会受到影响.单一石墨和炭黑含量超过30和25wt%或石墨加炭黑混合(m石墨: m炭黑=1: 1)导电原料含量超过30wt%时,可在炭/陶复合材料内部形成良好的连续导电通道,且该材料具有优良的电发热性能.","authors":[{"authorName":"李焰","id":"c9736fc8-2e84-4b2a-90e7-d32362fd0e30","originalAuthorName":"李焰"},{"authorName":"夏金童","id":"9ab1d8d2-a8fd-456b-ab55-0cac8d048571","originalAuthorName":"夏金童"},{"authorName":"邵浩明","id":"e4f0dc3e-6d57-48a9-9cf4-511c43ed37c5","originalAuthorName":"邵浩明"},{"authorName":"卢学峰","id":"a39cb52d-2b23-4573-86a7-480708a8112f","originalAuthorName":"卢学峰"}],"doi":"10.3969/j.issn.1005-5053.2006.02.014","fpage":"57","id":"c2984658-4b1b-4cf7-a063-5c9b29c9ba6c","issue":"2","journal":{"abbrevTitle":"HKCLXB","coverImgSrc":"journal/img/cover/HKCLXB.jpg","id":"41","issnPpub":"1005-5053","publisherId":"HKCLXB","title":"航空材料学报"},"keywords":[{"id":"0e70cff4-4108-435f-bd6c-d7f37cb99d4d","keyword":"炭/陶复合材料","originalKeyword":"炭/陶复合材料"},{"id":"e5d12ff3-ca98-44c4-89ba-a5d77c2b3bfb","keyword":"石墨","originalKeyword":"石墨"},{"id":"6e0dd4ea-770f-45f4-b4bd-5c04fc871134","keyword":"炭黑","originalKeyword":"炭黑"},{"id":"37796487-c2a3-4f1f-9a96-ec3b2feb9210","keyword":"电热性能","originalKeyword":"电热性能"}],"language":"zh","publisherId":"hkclxb200602014","title":"炭/陶复合材料电热性能的研究","volume":"26","year":"2006"},{"abstractinfo":"本文研究了以Ag3PO4、CuO为杀菌剂制作杀菌陶质釉面砖的配方组成,同时研究了烧成温度对杀菌效果的影响.结果表明添加Ag3PO42%或Ag3PO42%、CuO1%,釉烧温度1050℃可获得良好的杀菌效果,样品性能达到或超过国家标准.对样品的杀菌耐久性进行了检验,经过3个月的酸、碱溶液浸泡,结果杀菌效果无变化.","authors":[{"authorName":"马铁成","id":"948de3d6-5659-49d3-afde-ebe312029db9","originalAuthorName":"马铁成"},{"authorName":"高文元","id":"76eeac8c-625b-4a1b-b3d5-930f1120586c","originalAuthorName":"高文元"},{"authorName":"刘贵伟","id":"d1cb7829-a349-4694-9127-e69240ce5ffd","originalAuthorName":"刘贵伟"},{"authorName":"蔡英骥","id":"47025da4-f9ab-4e06-9e68-fd8f78ad156f","originalAuthorName":"蔡英骥"}],"doi":"10.3969/j.issn.1001-1625.1999.04.009","fpage":"41","id":"e12995a7-53ab-462d-aea1-da78c849d1df","issue":"4","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报 "},"keywords":[{"id":"a9f3e682-1341-42fb-acea-230e04b8f6c4","keyword":"杀菌陶瓷","originalKeyword":"杀菌陶瓷"},{"id":"5727ff01-0a8b-4749-8810-73ba445fb995","keyword":"釉面砖","originalKeyword":"釉面砖"}],"language":"zh","publisherId":"gsytb199904009","title":"杀菌陶质釉面砖的研究","volume":"18","year":"1999"},{"abstractinfo":"用加固剂加固保护陶质文物是一种延长陶质文物寿命的有效方法.采用纳米SiO2改性的聚丙烯酸酯复合乳液对陶质文物进行加固保护处理.结果表明:复合乳液处理后的陶质文物具有优良的耐老化性、耐水性和力学性能,同时不影响陶质文物的外观.纳米复合乳液有望在文物保护中得到广泛应用.","authors":[{"authorName":"董兵海","id":"8cffcc88-9bf7-4b1c-8e49-bdc37b4557a3","originalAuthorName":"董兵海"},{"authorName":"王世敏","id":"f9a9a907-3066-456e-8334-405a669867d4","originalAuthorName":"王世敏"},{"authorName":"许祖勋","id":"e292fcef-d74b-4730-826d-c68fb7b817b7","originalAuthorName":"许祖勋"},{"authorName":"夏璐","id":"68701ba6-18f9-477d-ad40-aa3e0cc5073a","originalAuthorName":"夏璐"},{"authorName":"谭白明","id":"484754be-d1e2-4d5d-a7f2-3aa92bceb567","originalAuthorName":"谭白明"}],"doi":"10.3969/j.issn.0253-4312.2005.12.003","fpage":"9","id":"5dcb654c-b6d5-4592-a1f4-cfe260019110","issue":"12","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业 "},"keywords":[{"id":"0b4dd8eb-624d-4db0-8074-3d76917da6b9","keyword":"陶质文物","originalKeyword":"陶质文物"},{"id":"5a08e6a0-c795-4579-9718-22a9f1c6b25b","keyword":"加固保护","originalKeyword":"加固保护"},{"id":"cbc952cc-9845-47dc-b931-a0779148d133","keyword":"纳米SiO2","originalKeyword":"纳米SiO2"},{"id":"71f72524-1f8d-4b50-8436-1561efce642b","keyword":"聚丙烯酸酯","originalKeyword":"聚丙烯酸酯"},{"id":"9b82d55e-cc1f-407f-b149-049f016ad54d","keyword":"复合乳液","originalKeyword":"复合乳液"}],"language":"zh","publisherId":"tlgy200512003","title":"纳米SiO2/聚丙烯酸酯复合乳液加固保护陶质文物的研究","volume":"35","year":"2005"},{"abstractinfo":"成都金沙遗址的年代覆盖了商代晚期至西周时期(公元前1200年-公元前650年),一般被认为是三星堆文化的延续.初步建立了质子激发X射线发射(PIXE)和卢瑟福背散射(RBS)实验装置,并采用PIXE和RBS方法研究了从金沙遗址出土的部分陶片的元素组成.通过因子分析,观察到来自不同地层的陶片的元素组成存在一定的差异,这可能意味着制作陶器的陶土在不同时期取自不同的地点.也观察到来自不同发掘坑的陶片的元素组成没有明显的聚类现象,这可能意味着制作不同使用用途的陶器所用的陶土是没有区别的.","authors":[{"authorName":"叶沥","id":"3220b7dd-fb4d-4873-9ac0-c23d47855287","originalAuthorName":"叶沥"},{"authorName":"刘慢天","id":"ed596516-5287-4d73-b0cb-95439327d009","originalAuthorName":"刘慢天"},{"authorName":"黄伟","id":"387cb63a-ed4c-4e82-8d52-e9076cf2387c","originalAuthorName":"黄伟"},{"authorName":"杨盛","id":"e5288c60-c57a-4cf4-b8c8-0709be3bb823","originalAuthorName":"杨盛"},{"authorName":"安竹","id":"ef202ea2-9e1c-4dcb-a426-d4511836ed90","originalAuthorName":"安竹"}],"doi":"","fpage":"493","id":"5cdbd0c7-8ad4-449f-a36d-fa2d3ec1ac48","issue":"4","journal":{"abbrevTitle":"YZHWLPL","coverImgSrc":"journal/img/cover/YZHWLPL.jpg","id":"78","issnPpub":"1007-4627","publisherId":"YZHWLPL","title":"原子核物理评论 "},"keywords":[{"id":"be02f80d-d85e-49bc-91c1-3c1cd51ab1e1","keyword":"PIXE","originalKeyword":"PIXE"},{"id":"e8aa8712-7a45-4b1c-9c4f-14c41676562b","keyword":"RBS","originalKeyword":"RBS"},{"id":"6c848d7a-7b9b-4d8c-80b0-f605f9ebb6d6","keyword":"陶器","originalKeyword":"陶器"},{"id":"247e37ad-d19c-4bea-b827-02849c20db0f","keyword":"金沙遗址","originalKeyword":"金沙遗址"}],"language":"zh","publisherId":"yzhwlpl201004020","title":"成都金沙遗址古代陶片的PIXE和RBS分析","volume":"27","year":"2010"},{"abstractinfo":"指出了金陶公司原选矿工艺存在的问题,介绍了对选矿厂碎矿、浸出、吸附、解吸、电解等工艺进行的一系列技术改造、增加\"水平衡工程\"及工艺改造前后的生产指标与取得的经济效益.","authors":[{"authorName":"贾洪杰","id":"85516e25-178a-4f50-a519-62527694bed8","originalAuthorName":"贾洪杰"},{"authorName":"张玉文","id":"f4ff7900-50d1-418c-91ac-02daaf14b022","originalAuthorName":"张玉文"},{"authorName":"杨云成","id":"4110ee94-44ee-434c-a663-72cfdc94959d","originalAuthorName":"杨云成"}],"doi":"10.3969/j.issn.1001-1277.2004.05.010","fpage":"31","id":"9351e6e8-ca3a-42de-9805-b2cd990f9c8d","issue":"5","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"d9cb8dc7-5349-4094-aba8-eff9a5ce50e8","keyword":"技术改造","originalKeyword":"技术改造"},{"id":"9caed097-5fda-4ef6-868a-e6551ba856fa","keyword":"水平衡工程","originalKeyword":"水平衡工程"},{"id":"0661f2d9-9ab3-4e5a-80bc-7921816c4f63","keyword":"选冶回收率","originalKeyword":"选冶回收率"},{"id":"b5efa7fa-d513-4d59-9faf-3a075c85d1fa","keyword":"经济效益","originalKeyword":"经济效益"}],"language":"zh","publisherId":"huangj200405010","title":"金陶公司选矿工艺技术改造与生产实践","volume":"25","year":"2004"},{"abstractinfo":"陕西省淳化县枣树沟脑遗址出土了大量的陶器.古代陶器的化学成分和微观结构能很好地反映陶器的种类和烧制工艺等信息.本文采用数码显微镜、扫描电子显微镜、X射线能谱仪、X射线衍射仪等多种仪器分析了陕西淳化枣树沟脑遗址出土的一件西周陶鬲的微观结构和化学成分.结果表明陶鬲陶土的成分中含有石英、白榴石、四氧化三铁、氧化亚铁、莫来石、白云母、硅线石和钙长石等.羼和料的主要成分是石英.","authors":[{"authorName":"严小琴","id":"3394a1cc-9a1c-4120-bdf0-423ad40896c7","originalAuthorName":"严小琴"},{"authorName":"凌雪","id":"097b09cb-2b77-4edb-bcca-a9970582a8f9","originalAuthorName":"凌雪"},{"authorName":"孙丽娟","id":"ff21b2f6-2971-4efc-898f-7ced8b0271d0","originalAuthorName":"孙丽娟"}],"doi":"","fpage":"646","id":"6e91e29c-dcde-4cac-8978-77d10eddd26d","issue":"3","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报 "},"keywords":[{"id":"8516ea71-f35a-4ced-b8e6-93b44d923ff8","keyword":"枣树沟脑遗址","originalKeyword":"枣树沟脑遗址"},{"id":"532db296-eaaf-45f4-b998-6aef14ff47df","keyword":"陶鬲","originalKeyword":"陶鬲"},{"id":"6ae49c96-ca1f-47a7-82b3-6257a366b76c","keyword":"X射线衍射","originalKeyword":"X射线衍射"}],"language":"zh","publisherId":"gsytb201403039","title":"陕西淳化枣树沟脑遗址出土西周陶鬲的科技分析","volume":"33","year":"2014"}],"totalpage":7,"totalrecord":68}