{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"利用透射<span style=\"color:red\">电镜</span>(TEM)和扫描<span style=\"color:red\">电镜</span>(SEM)研究了不同耐磨堆焊层的显微组织特征.通过与实际工况磨损状态和堆焊层硬度测试数据对比分析,发现高铬铸铁耐磨堆焊层的显微组织,如硬质相的形态、尺寸和分布、基体相的性质等是决定其耐磨性的主要因素,而不是一般认为的硬度因素.","authors":[{"authorName":"潘春旭","id":"472b83cd-c517-42fd-af80-11e9609b7f02","originalAuthorName":"潘春旭"},{"authorName":"陈俐","id":"6c512a2a-8711-450c-9527-8b186af9307e","originalAuthorName":"陈俐"}],"doi":"10.3969/j.issn.1004-244X.2000.02.002","fpage":"8","id":"8b97aa1a-30f1-4ddc-9d24-17cbd0c97d5e","issue":"2","journal":{"abbrevTitle":"BQCLKXYGC","coverImgSrc":"journal/img/cover/BQCLKXYGC.jpg","id":"4","issnPpub":"1004-244X","publisherId":"BQCLKXYGC","title":"兵器材料科学与工程   "},"keywords":[{"id":"a31207ee-0dbf-4463-a557-9850ee44722f","keyword":"耐磨堆焊","originalKeyword":"耐磨堆焊"},{"id":"99126fb4-f56c-4e71-8646-91479703534d","keyword":"耐磨性","originalKeyword":"耐磨性"},{"id":"1133a92c-f26e-4276-ba66-736deed19d30","keyword":"显微组织","originalKeyword":"显微组织"},{"id":"dbaa1060-1b51-4b5c-a125-228e43891f86","keyword":"<span style=\"color:red\">电镜</span>","originalKeyword":"电镜"}],"language":"zh","publisherId":"bqclkxygc200002002","title":"耐磨堆焊层显微组织特征及其与耐磨性关系的研究","volume":"23","year":"2000"},{"abstractinfo":"利用等离子喷涂技术制备了ZrO2陶瓷和NiCrAl金属的梯度热障涂层,利用扫描<span style=\"color:red\">电镜</span>(SEM)、能谱仪(EDS)和电子探针(EPMA)研究了涂层的显微结构和化学成分分布特征.实验发现:梯度过渡层的显微结构明显不同,以金属为主要组分的过渡层主要为层状结构,以陶瓷为主要组分的过渡层层状特征不明显;过渡层化学元素分布不均匀,其中Zr与Mg分布特征相同,Zr与Ni分布位置互补,Cr、Al主要以氧化物形式位于晶粒边界处.","authors":[{"authorName":"徐小荣","id":"54c968a4-3f88-4e62-acd3-c578da2bea59","originalAuthorName":"徐小荣"},{"authorName":"潘春旭","id":"e3a70e21-5c22-432f-a037-488a45840b12","originalAuthorName":"潘春旭"}],"doi":"10.3969/j.issn.1005-0299.2003.01.015","fpage":"68","id":"4deb1d21-a5b5-40cd-93e6-934b4a1e172e","issue":"1","journal":{"abbrevTitle":"CLKXYGY","coverImgSrc":"journal/img/cover/CLKXYGY.jpg","id":"14","issnPpub":"1005-0299","publisherId":"CLKXYGY","title":"材料科学与工艺"},"keywords":[{"id":"ce6f1f3a-e1da-4f1f-a315-1ea037a55cb6","keyword":"梯度热障涂层","originalKeyword":"梯度热障涂层"},{"id":"b16e61e6-2bbc-4a1f-b1b7-e5e09eb45033","keyword":"ZrO2陶瓷","originalKeyword":"ZrO2陶瓷"},{"id":"b4348010-97cc-49dc-a82a-435c6f7bd12b","keyword":"显微结构","originalKeyword":"显微结构"},{"id":"43a7f690-da9b-403b-bc6b-debc42775343","keyword":"<span style=\"color:red\">电镜</span>","originalKeyword":"电镜"}],"language":"zh","publisherId":"clkxygy200301015","title":"ZrO2陶瓷-金属梯度热障涂层的显微结构特征","volume":"11","year":"2003"},{"abstractinfo":"介绍了四种常用分析方法在自组装功能膜结构及其界面层表征中的新进展.红外光谱是常用的结构分析方法,运用掠角反射红外光谱豆衰减全反射红外光谱可以分析自组装薄膜表面、界面结构以及分子链段的取向;XPS分析可以确定薄膜的化学组成;<span style=\"color:red\">电镜</span>的运用使直接观察体系的形态、形貌成为可能;ESR是研究聚合物在溶液中自组装成胶束过程的有力工具.","authors":[{"authorName":"何琳","id":"7a2b1387-b38a-468b-b374-35565557fd08","originalAuthorName":"何琳"},{"authorName":"张曦","id":"de386345-d4be-493a-ad71-542250cee981","originalAuthorName":"张曦"},{"authorName":"吕德水","id":"e8d38678-020c-4805-9865-2ddde65cf67e","originalAuthorName":"吕德水"},{"authorName":"陈志春","id":"2b4ebd41-bca9-4e4d-9705-e99ebe3c6f03","originalAuthorName":"陈志春"},{"authorName":"林贤福","id":"71d386f5-b113-440f-9352-7694c6b11267","originalAuthorName":"林贤福"}],"doi":"","fpage":"54","id":"ce73f2ea-ca94-4f07-98ee-a0bf468eb81d","issue":"3","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"95f7d730-192f-407d-87f9-dfe909c2abff","keyword":"红外光谱","originalKeyword":"红外光谱"},{"id":"a46864b4-1956-4da6-b524-aa1a03202450","keyword":"X光电子能潜","originalKeyword":"X光电子能潜"},{"id":"cc42a405-92c3-4933-9a8c-7c12d095e769","keyword":"<span style=\"color:red\">电镜</span>","originalKeyword":"电镜"},{"id":"b209292b-25e3-40a3-b903-e5518c7d9a6f","keyword":"顺磁共振","originalKeyword":"顺磁共振"},{"id":"4bfe92e8-c549-4c34-bf8f-e6620f3b0c2f","keyword":"大分子自组装","originalKeyword":"大分子自组装"}],"language":"zh","publisherId":"cldb200003021","title":"大分子自组装功能膜的结构及界面层表征","volume":"14","year":"2000"},{"abstractinfo":"采用浸泡试验结合电化学阻抗谱、扫描<span style=\"color:red\">电镜</span>等手段,对磷酸、单宁酸复合型转化液锈层转化效果进行了分析.结果表明,转化液中磷酸、单宁酸含量及其比例对锈层转化效果有影响,浸泡试验表明,当转化液中单宁酸含量为0.5％～1％,缓蚀剂含量为1％,渗透剂含量为3％～7％,且渗透剂与磷酸的质量比为0.4～0.6时,锈层的转化效果较佳;电化学阻抗结合显微形貌测试结果表明,锈层经不同转化液处理后,表面磷化膜致密性以及内部锈层的磷化程度不同,同时增加处理液中的渗透剂和缓蚀剂的用量可以提高磷化膜致密性以及内部锈层的磷化程度.","authors":[{"authorName":"易博","id":"cc645780-9980-4ffe-b662-52e26b30ef7e","originalAuthorName":"易博"},{"authorName":"董勇军","id":"b9911094-ac85-43f6-8c4c-f92c9e488a87","originalAuthorName":"董勇军"},{"authorName":"赵定义","id":"a15b444b-758a-4337-92e0-999596e47f05","originalAuthorName":"赵定义"},{"authorName":"高义斌","id":"48125b4a-ce6d-4597-8ed9-ef465b40ebc4","originalAuthorName":"高义斌"},{"authorName":"李启润","id":"31298486-71ca-4da1-a8e4-484b0a36222c","originalAuthorName":"李启润"},{"authorName":"张俊喜","id":"ab4e5bb3-41c2-4ebc-be8a-322d30251e78","originalAuthorName":"张俊喜"}],"doi":"10.11973/fsyfh-201509017","fpage":"873","id":"22fa7aa4-eb12-46cc-ab8d-6ff071711363","issue":"9","journal":{"abbrevTitle":"FSYFH","coverImgSrc":"journal/img/cover/FSYFH.jpg","id":"25","issnPpub":"1005-748X","publisherId":"FSYFH","title":"腐蚀与防护"},"keywords":[{"id":"ff4292f0-3400-4976-ac6a-17eed6f58c07","keyword":"带锈转化液","originalKeyword":"带锈转化液"},{"id":"4e0b74c7-f97d-455c-a9b8-f5595080340f","keyword":"转化效果","originalKeyword":"转化效果"},{"id":"e0ca1c3a-e01c-4eb0-b152-f906cf49ebc0","keyword":"浸泡试验","originalKeyword":"浸泡试验"},{"id":"1e2d1e84-009a-4396-927f-7bfeba5d1e3a","keyword":"电化学阻抗","originalKeyword":"电化学阻抗"},{"id":"dd0706cd-5c43-4e85-aeaa-dfa253b5167f","keyword":"<span style=\"color:red\">电镜</span>","originalKeyword":"电镜"}],"language":"zh","publisherId":"fsyfh201509017","title":"磷酸、单宁酸混合型带锈转化液的转化效果","volume":"36","year":"2015"},{"abstractinfo":"利用电子探针、扫描<span style=\"color:red\">电镜</span>和X射线衍射仪对W-Mo-Ti系梯度飞片的化学成分分布、显微组织和组织结构特征进行了研究.研究表明:W-Mo-Ti系梯度飞片中主要元素W、Mo、Ti分布整体上具有梯度变化规律;以Ti为主的Mo-Ti混合区和高Ti区,Ti主要以多角形α相存在.","authors":[{"authorName":"李松","id":"d4910a50-7567-4498-a3ab-3f1533279b09","originalAuthorName":"李松"},{"authorName":"何小于","id":"207eac11-8604-4b86-9549-454f6c35400d","originalAuthorName":"何小于"},{"authorName":"张同俊","id":"916a4763-daf5-4efd-9846-8bb298155e0b","originalAuthorName":"张同俊"},{"authorName":"员文杰","id":"4add00e2-90f7-49f5-8773-ed1c59f2629b","originalAuthorName":"员文杰"}],"doi":"10.3969/j.issn.1673-2812.2004.01.006","fpage":"20","id":"dfd2beb7-a7fe-4a43-955c-24976bda61c0","issue":"1","journal":{"abbrevTitle":"CLKXYGCXB","coverImgSrc":"journal/img/cover/CLKXYGCXB.jpg","id":"13","issnPpub":"1673-2812","publisherId":"CLKXYGCXB","title":"材料科学与工程学报"},"keywords":[{"id":"f870ddfe-6066-43b9-9b94-b12be4b4d6b2","keyword":"W-Mo-Ti","originalKeyword":"W-Mo-Ti"},{"id":"82b77d45-eaf1-412b-9b26-94330e777a1f","keyword":"显微组织","originalKeyword":"显微组织"},{"id":"c603bf5d-1f79-492c-ba6b-85a9c23a1d42","keyword":"<span style=\"color:red\">电镜</span>","originalKeyword":"电镜"}],"language":"zh","publisherId":"clkxygc200401006","title":"W-Mo-Ti系梯度飞片的显微组织特征","volume":"22","year":"2004"},{"abstractinfo":"在英国和法国的很多高放核废料中都含有大量的钼。钼在核废料玻璃中的溶解度很低，过量的钼会导致玻璃产生钼酸盐分相从而影响核废料玻璃化的效率和安全。主要研究了钼酸盐在硼酸盐玻璃中的溶解度与玻璃中碱土金属元素的关系以及钼酸盐的溶解对玻璃的结构和性质的影响。在其它玻璃组分不变的情况下，对玻璃中的碱土金属（由镁至钡）进行等摩尔量替换。结果发现，当碱土金属为钙时钼酸盐的溶解度最高，为2.84 mol%。XRD结果显示除了明显分相的玻璃外其它均一玻璃均为无定形态。SEM结果显示玻璃基体内的分相大多为球状/水滴状并呈随机分布；其尺寸与钼酸盐的过量程度有关，但直径都小于1mm。对钙硼硅酸盐玻璃中析出相的 EDX 分析表明其中富含钼和钙，而 TEM 结果证明这些析出相为晶体相且符合钼酸钙的电子衍射特征。含钼玻璃有两个强烈的拉曼峰（分别位于320和910 cm–1附近）：其强度随玻璃中钼含量的增加而增加，其位置随玻璃中碱土金属元素的变化而偏移。此外，钼的加入也会导致玻璃的玻璃转变温度降低以及玻璃密度增加。","authors":[{"authorName":"谭盛恒","id":"9afe5480-5f1a-471a-b919-3e4e55d36930","originalAuthorName":"谭盛恒"},{"authorName":"Russell J HAND","id":"2bd12200-384c-46f2-a4ff-42c0b1619a1d","originalAuthorName":"Russell J HAND"}],"doi":"10.7502/j.issn.1674-3962.2016.07.03","fpage":"496","id":"80d44b55-9267-4b5a-8aca-aa6cf32b351f","issue":"7","journal":{"abbrevTitle":"ZGCLJZ","coverImgSrc":"journal/img/cover/中国材料进展.jpg","id":"80","issnPpub":"1674-3962","publisherId":"ZGCLJZ","title":"中国材料进展"},"keywords":[{"id":"688a24ab-a2c2-4064-b07e-691e5fb9b8b5","keyword":"核废料玻璃化","originalKeyword":"核废料玻璃化"},{"id":"879a2f57-603c-406c-ba20-72ed60d4ca77","keyword":"钼","originalKeyword":"钼"},{"id":"9ff66a8f-741e-4942-9ecd-943cb3ed354b","keyword":"碱土金属","originalKeyword":"碱土金属"},{"id":"31086a25-f246-43b0-8661-6b0fc0b23f9a","keyword":"拉曼光谱","originalKeyword":"拉曼光谱"},{"id":"c6febf87-e3d8-47f7-b8ea-dc51d58e1263","keyword":"<span style=\"color:red\">电镜</span>","originalKeyword":"电镜"}],"language":"zh","publisherId":"zgcljz201607003","title":"钼酸盐在硼硅酸盐玻璃体系中的溶解","volume":"35","year":"2016"},{"abstractinfo":"针对<span style=\"color:red\">电镜</span>室安装环境的振动和磁场测试超标的问题，分析了振动、磁场干扰的原因和特性，采用增大<span style=\"color:red\">电镜</span>基础结合缓冲垫层的方法来隔振，通过低碳钢板和纯铁板双层材料磁屏蔽技术来防磁，实践结果满足了<span style=\"color:red\">电镜</span>安装的要求。","authors":[{"authorName":"廉晓洁","id":"794f9cfd-952f-4ba9-88c2-734ae0a7954e","originalAuthorName":"廉晓洁"}],"categoryName":"|","doi":"","fpage":"25","id":"7ddd7654-a73a-4c10-95c5-6b69552fd014","issue":"1","journal":{"abbrevTitle":"WLCS","coverImgSrc":"journal/img/cover/WLCS.jpg","id":"64","issnPpub":"1001-0777","publisherId":"WLCS","title":"物理测试"},"keywords":[{"id":"9657c168-1f5e-42e3-84b8-9274cc7a750e","keyword":"电子显微镜 ","originalKeyword":"电子显微镜 "},{"id":"b1a8a5f6-e22d-4d0f-9952-e1bb8388bc5a","keyword":" anti-vibration ","originalKeyword":" anti-vibration "},{"id":"c99566f8-57c2-487d-b02f-5461ed7e87ff","keyword":" magnetic shielding","originalKeyword":" magnetic shielding"}],"language":"zh","publisherId":"1001-0777_2012_1_7","title":"<span style=\"color:red\">电镜</span>实验室磁屏蔽和防振措施","volume":"30","year":"2012"},{"abstractinfo":"针对<span style=\"color:red\">电镜</span>室安装环境的振动和磁场测试超标的问题,分析了振动、磁场干扰的原因和特性,采用增大<span style=\"color:red\">电镜</span>基础结合缓冲垫层的方法来隔振,通过低碳钢板和纯铁板双层材料磁屏蔽技术来防磁,实践结果满足了<span style=\"color:red\">电镜</span>安装的要求。","authors":[{"authorName":"廉晓洁","id":"57ca0b6d-7687-4ebb-85db-0efd25cb0c40","originalAuthorName":"廉晓洁"}],"doi":"","fpage":"25","id":"ea2a47fb-147e-4d3f-bd6b-bf75b05b60af","issue":"1","journal":{"abbrevTitle":"WLCS","coverImgSrc":"journal/img/cover/WLCS.jpg","id":"64","issnPpub":"1001-0777","publisherId":"WLCS","title":"物理测试"},"keywords":[{"id":"3d3bf7ae-d305-4fde-a4ed-a7cb5685a8ef","keyword":"电子显微镜","originalKeyword":"电子显微镜"},{"id":"30552669-b18a-45b7-8bdd-dd898f0785f4","keyword":"防振","originalKeyword":"防振"},{"id":"02ae7516-f400-4238-b806-46cea2d6054d","keyword":"磁屏蔽","originalKeyword":"磁屏蔽"}],"language":"zh","publisherId":"wlcs201201007","title":"<span style=\"color:red\">电镜</span>实验室磁屏蔽和防振措施","volume":"","year":"2012"},{"abstractinfo":"介绍了扫描<span style=\"color:red\">电镜</span>粉末样品的几种制备方法,并通过试验将各种制备方法进行比较.结果表明:不同性质的粉末样品应采用合适的制样方法.","authors":[{"authorName":"苗壮","id":"73c1f911-02fd-4b18-a91a-471af94f920a","originalAuthorName":"苗壮"},{"authorName":"刘竞艳","id":"f011ef01-f769-48da-b909-2d88abb010b1","originalAuthorName":"刘竞艳"},{"authorName":"常璐","id":"e57794fb-7b04-4eea-9bf3-1ea20ab83cbb","originalAuthorName":"常璐"},{"authorName":"田弋纬","id":"4c37a53e-ed17-4e9d-97e1-aff907823709","originalAuthorName":"田弋纬"}],"doi":"10.3969/j.issn.1009-9964.2008.04.008","fpage":"31","id":"610b0a72-1f86-4f14-b872-deca1ea8ccbb","issue":"4","journal":{"abbrevTitle":"TGYJZ","coverImgSrc":"journal/img/cover/TGYJZ.jpg","id":"60","issnPpub":"1009-9964","publisherId":"TGYJZ","title":"钛工业进展"},"keywords":[{"id":"abeae97c-19ba-4194-a5ed-482b82bc4d11","keyword":"扫描<span style=\"color:red\">电镜</span>","originalKeyword":"扫描电镜"},{"id":"e9f7b74f-849f-4a8c-8b09-5732c825a89f","keyword":"粉末样品","originalKeyword":"粉末样品"},{"id":"75ba6461-c77b-45d1-9b4f-8a430958bf69","keyword":"制各方法","originalKeyword":"制各方法"}],"language":"zh","publisherId":"tgyjz200804008","title":"扫描<span style=\"color:red\">电镜</span>粉末样品的制备方法","volume":"25","year":"2008"},{"abstractinfo":"用透射<span style=\"color:red\">电镜</span>(TEM)观察粉末产品,当粉末样品颗粒直径(即厚度)大于0.5μm时,由于电子束不能穿透,是不能进行电子显微结构分析的,把复合电镀技术引入到粉末颗粒<span style=\"color:red\">电镜</span>试样制备的方法中,在减薄镀层的同时实现了粉末颗粒的减薄.以平均粒径8μm的氧化钴锂LiCoO2(二次锂离子电池正极材料)为例,将其散布到CuSO4电镀液中进行复合电镀.将悬浮在电镀液中的颗粒连同镀金层金属离子共同沉积在电极上,通过选择合理的电镀工艺参数,形成厚度适宜、颗粒分布密度高、包埋紧实且易于剥离的复合镀层,然后将其电解双喷和离子减薄形成颗粒薄区,使电子束可以穿透.对用此方法制备的试样所做的透射<span style=\"color:red\">电镜</span>电子像和电子衍射谱分析表明,通过复合电镀包埋颗粒再减薄颗粒的方法对于<span style=\"color:red\">电镜</span>粉末大颗粒样品制备有实用价值.还探讨了复合电沉积时粉末颗粒的运动特点.","authors":[{"authorName":"闫时建","id":"2de9b4b7-b28c-4a86-b924-0c1fa7b5f940","originalAuthorName":"闫时建"},{"authorName":"田文怀","id":"a38558cf-30a3-42bd-aefa-04a2788bf201","originalAuthorName":"田文怀"},{"authorName":"周永令","id":"be97172f-7be1-454b-bcc9-00dcf217495e","originalAuthorName":"周永令"}],"doi":"10.3969/j.issn.1001-1560.2004.05.002","fpage":"4","id":"ea47bdd5-b845-4241-8263-400621d8f5a3","issue":"5","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"e9fb11b0-bac0-4f36-aa48-ad8fbe4b46d1","keyword":"复合电镀","originalKeyword":"复合电镀"},{"id":"025a2060-f73d-4443-a84d-19fcf18eb4f3","keyword":"LiCoO2颗粒","originalKeyword":"LiCoO2颗粒"},{"id":"90bb3c87-1709-443a-b13a-ec3d5eea7a57","keyword":"<span style=\"color:red\">电镜</span>试样","originalKeyword":"电镜试样"}],"language":"zh","publisherId":"clbh200405002","title":"复合电镀制备透射<span style=\"color:red\">电镜</span>试样","volume":"37","year":"2004"}],"totalpage":1783,"totalrecord":17821}