{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"从样品制备评价和校准曲线的建立两方面开展对火花源原子发射光谱法测定海绵钛中Si、Fe、Mn、Mg等元素的实验研究.主要考察了样品表面的均匀性、车削纹和车削深度对测定结果的影响.研究表明,保持激发表面平整、光洁、无明显车削纹(表面粗糙度Ra≤1.6μm)、车削深度控制在12 mm以内,可获得相对稳定的测定结果.利用电感耦合等离子体原子发射光谱法(ICP-AES)测定并经化学分析法确认后定值的样品绘制校准曲线避免了绘制曲线的标样与实际样品存在基体不匹配的问题,拓展了火花源原子发射光谱仪中内置的Si、Fe、Mn等曲线的测定范围,并建立了Mg的校准曲线,各曲线相关系数R2≥0.995.采用实验方法对海绵钛样品中Si、Fe、Mn、Mg进行测定,并与ICP-AES法进行对照,结果吻合性良好.t检验结果表明,实验方法与ICP-AES法无显著性差异.","authors":[{"authorName":"俞超","id":"0eae46fe-d661-4f5d-8bd5-8f596c6ce24a","originalAuthorName":"俞超"},{"authorName":"<span style=\"color:red\">汪</span><span style=\"color:red\">永</span><span style=\"color:red\">喜</span>","id":"9b587f3b-7027-4d61-a7e8-6856bd89c323","originalAuthorName":"汪永喜"},{"authorName":"蒋增辉","id":"79cc9ad2-09a9-4130-b933-f1afd8c122b9","originalAuthorName":"蒋增辉"},{"authorName":"曾次元","id":"88abef19-0f73-43e7-bd0f-b460f52490d7","originalAuthorName":"曾次元"}],"doi":"10.13228/j.boyuan.issn1000-7571.009570","fpage":"46","id":"332b4944-3c2b-4ca8-998a-785ed01cb0d6","issue":"6","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"c4185617-1eeb-492a-bbda-b78c3158f55c","keyword":"火花源原子发射光谱法","originalKeyword":"火花源原子发射光谱法"},{"id":"1dd6e52f-f59b-4822-bcfd-aaf5e14f6836","keyword":"海绵钛","originalKeyword":"海绵钛"},{"id":"00474caf-8133-429b-9abd-bff20b79ebe5","keyword":"硅","originalKeyword":"硅"},{"id":"e30cb552-6ce1-4440-a112-0ffeae1ea274","keyword":"铁","originalKeyword":"铁"},{"id":"3e89e6b6-a2ff-4d23-9220-a9c28397c042","keyword":"锰","originalKeyword":"锰"},{"id":"54af533c-eba9-4ef3-9e9a-b7f773211ac2","keyword":"镁","originalKeyword":"镁"},{"id":"b38fe5d5-2f65-41f4-a392-a6ba4ff9bc7c","keyword":"样品制备评价","originalKeyword":"样品制备评价"},{"id":"3cc85098-560f-41f7-b076-26618987b94f","keyword":"校准曲线建立","originalKeyword":"校准曲线建立"}],"language":"zh","publisherId":"yjfx201606009","title":"火花源原子发射光谱法测定海绵钛样品及样品制备方法的影响","volume":"36","year":"2016"},{"abstractinfo":"氧化亚铁微螺菌和<span style=\"color:red\">喜</span>温嗜酸硫杆菌是浸矿细菌的一种两种常见的浸矿细菌,为了测定重金属镍离子对它们活性的影响,设置了不同浓度镍离子的摇瓶实验,在温度为45℃,转速为150 r/min的条件下开展实验.结果表明:镍离子浓度在小于2g/L时,氧化亚铁微螺菌和<span style=\"color:red\">喜</span>温嗜酸硫杆菌的活性不受影响;镍离子浓度在4 g/L时,细菌的活性受到影响,活性降低,但通过自身的调节作用,还可以继续生长;镍离子浓度大于8g/L时,细菌几乎不生长.","authors":[{"authorName":"赵雪淞","id":"c41990c4-9f7f-406a-a791-d585aedbe25a","originalAuthorName":"赵雪淞"},{"authorName":"石倩倩","id":"e8f25a97-a08d-46c1-a258-bfe74ae6a187","originalAuthorName":"石倩倩"},{"authorName":"李彩霞","id":"cab27d73-6c81-4e21-95f6-f9e51853c375","originalAuthorName":"李彩霞"},{"authorName":"张孝松","id":"1f12ce0f-f7f2-4ced-bd69-6b02a17c2f19","originalAuthorName":"张孝松"}],"doi":"","fpage":"306","id":"470e9a9b-52d5-4e26-9e5a-079455663906","issue":"1","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报   "},"keywords":[{"id":"93aede27-05cf-4136-850e-179716c38ae3","keyword":"氧化亚铁微螺菌","originalKeyword":"氧化亚铁微螺菌"},{"id":"483e3eb5-044d-48ce-9b18-5ff784877f77","keyword":"<span style=\"color:red\">喜</span>温嗜酸硫杆菌","originalKeyword":"喜温嗜酸硫杆菌"},{"id":"8d4e16fc-1eb5-48ec-9302-947f76d8d75e","keyword":"活性","originalKeyword":"活性"},{"id":"c4f5f4a7-c001-4af2-ae40-9e937e8ff225","keyword":"镍离子","originalKeyword":"镍离子"}],"language":"zh","publisherId":"gsytb201601054","title":"镍离子对氧化亚铁微螺菌和<span style=\"color:red\">喜</span>温嗜酸硫杆菌活性的影响","volume":"35","year":"2016"},{"abstractinfo":"自云南酸性热泉水样中分离出一株中度嗜热硫氧化菌YN12.对其形态特征和生理生化特性以及16S rDNA序列分析结果证明,该菌株归属于<span style=\"color:red\">喜</span>温嗜酸硫杆菌(Acidithiobacillus caldus).重金属抗性实验表明,YN12菌株对3CdSO4-8H2O具有超强抗性,其最高初始Cd2+耐受浓度达4.8 g/L.在此基础上,不断提升3CdSO4-8H2O浓度,其最终Cd2+耐受浓度可达31.5 g /L(相当于3CdSO4-8H2O 210 g/L).在该最终Cd2+耐受浓度下,经过连续3代的适应性生长,YN12菌株的生长速度和硫氧化活性均能得到较好的恢复.","authors":[{"authorName":"丁建南","id":"176e4ae4-0084-4c41-9f88-19e3eaba636e","originalAuthorName":"丁建南"},{"authorName":"朱若林","id":"e188e17e-7e7b-4041-858b-f85cd40dafe4","originalAuthorName":"朱若林"},{"authorName":"康健","id":"ef9888eb-1178-4ff2-aea6-466a2e1c4d4e","originalAuthorName":"康健"},{"authorName":"张成桂","id":"9d980e84-be2e-4902-8212-963ebc81be9f","originalAuthorName":"张成桂"},{"authorName":"吴学玲","id":"577995ab-02ac-40af-b479-144aaf1b0729","originalAuthorName":"吴学玲"},{"authorName":"邱冠周","id":"db912e11-9e9f-4a1b-a6df-670482e6a1f0","originalAuthorName":"邱冠周"}],"doi":"","fpage":"342","id":"bd276956-9b07-49a0-bdc9-c2de83f89b4e","issue":"2","journal":{"abbrevTitle":"ZGYSJSXB","coverImgSrc":"journal/img/cover/ZGYSJSXB.jpg","id":"88","issnPpub":"1004-0609","publisherId":"ZGYSJSXB","title":"中国有色金属学报"},"keywords":[{"id":"c6864f0d-91e7-4976-9ab8-c7b19a5b50ec","keyword":"<span style=\"color:red\">喜</span>温嗜酸硫杆菌","originalKeyword":"喜温嗜酸硫杆菌"},{"id":"33fef14d-6b3f-4b18-9ec6-b824a2645a29","keyword":"YN12菌株","originalKeyword":"YN12菌株"},{"id":"22e81fdd-94bb-45e7-8e8f-33e2238c6cce","keyword":"镉抗性","originalKeyword":"镉抗性"},{"id":"5681b107-a535-424e-8a39-4614ac6a6c7c","keyword":"最高耐受浓度","originalKeyword":"最高耐受浓度"}],"language":"zh","publisherId":"zgysjsxb200802026","title":"<span style=\"color:red\">喜</span>温嗜酸硫杆菌YN12菌株的鉴定及其镉抗性能","volume":"18","year":"2008"},{"abstractinfo":"采用十八胺对<span style=\"color:red\">永</span>固红F5R进行化学修饰,以Span-80为稳定剂,四氯乙烯为分散介质,制备了分散性和稳定性良好的电泳液.以此电泳液为囊芯,脲甲醛树脂为壁材,制备了一种红色电子墨水微胶囊,研究了投料比、合成温度、酸化时间和搅拌速度等对合成微胶囊的影响.结果表明,合成的微胶囊形貌呈规则球形,表面光滑,囊壁结构致密,强度较好,包覆率达到82%,囊芯含量达到76%.<span style=\"color:red\">永</span>固红F5R电泳液微胶囊具有明显的电场响应行为,可以作为柔板显示器的功能材料.","authors":[{"authorName":"倪卓","id":"e029822e-b1ed-424a-b43f-a3d2d95f646c","originalAuthorName":"倪卓"},{"authorName":"李丹","id":"f887ef04-3dc6-455f-86fc-9eaf77647b61","originalAuthorName":"李丹"},{"authorName":"钟玉莲","id":"6e3369c1-b82c-4882-b5ad-f92b613051e0","originalAuthorName":"钟玉莲"},{"authorName":"刘丽双","id":"d3c287ad-6acf-4232-8eae-a680e7e1a76f","originalAuthorName":"刘丽双"},{"authorName":"陈展明","id":"baa30c08-d528-444e-a1d0-a9e6d19f0be8","originalAuthorName":"陈展明"}],"doi":"","fpage":"101","id":"d12b9eff-6442-431e-95ec-d7cd2e3641e6","issue":"20","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"6e0a5c0b-b00d-482d-8087-7395d7978cd1","keyword":"电子墨水","originalKeyword":"电子墨水"},{"id":"992b930c-12f3-4576-8e3c-b39ae1c29e47","keyword":"微胶囊","originalKeyword":"微胶囊"},{"id":"e7f3811b-05f8-4d67-9e95-425b0fecdb1c","keyword":"<span style=\"color:red\">永</span>固红F5R","originalKeyword":"永固红F5R"},{"id":"aa0d839f-6344-4e50-88fd-9805b4855b0d","keyword":"电场响应","originalKeyword":"电场响应"}],"language":"zh","publisherId":"cldb200920030","title":"<span style=\"color:red\">永</span>固红F5R电泳液微胶囊的制备和表征","volume":"23","year":"2009"},{"abstractinfo":"本试验主要研究目的是SBS改性剂、相容剂、稳定剂、剪切速率、剪切时间、发育时间对<span style=\"color:red\">永</span>古高速公路SBS改性沥青性能的影响.查阅该地区沥青路面资料,初步确定在相容剂掺量1.5％,稳定剂掺量1.5‰的前提下,通过对沥青软化点、25℃的针入度、5℃的延度、离析软化点差进行试验,对试验结果进行分析,最终确定SBS改性沥青的SBS改性剂掺量3.8％、相容剂掺量1.5％、稳定剂掺量2‰.在此SBS改性沥青的前提下,研究剪切速率、剪切时间、发育时间对SBS改性沥青的影响,在剪切时间30 min,发育时间90 min的前提下,继续对沥青软化点、25℃的针入度、5℃的延度进行试验,整理分析数据,得到最终的制备工艺为:剪切速率5500 r·min-1、剪切时间35 min、发育时间为120 min.得到结论为<span style=\"color:red\">永</span>古高速SBS改性沥青为:SBS改性剂掺量3.8％、相容剂掺量1.5％、稳定剂掺量2‰、剪切速率5500 r·min-1、剪切时间35 min、发育时间120 min.","authors":[{"authorName":"杨成","id":"49e1bb34-385e-450e-b15a-d087702dd672","originalAuthorName":"杨成"},{"authorName":"刘德仁","id":"5e1cc12a-3310-4b99-987e-685849267cce","originalAuthorName":"刘德仁"},{"authorName":"王旭","id":"3f7ebb88-9706-4ed1-a295-874f3dd09b5e","originalAuthorName":"王旭"},{"authorName":"刘国太","id":"b788fc37-667e-45b2-84cf-868fbfcd442e","originalAuthorName":"刘国太"}],"doi":"","fpage":"1956","id":"f7099de0-276a-4990-90b1-bf620a4ab25c","issue":"8","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报   "},"keywords":[{"id":"e07d0294-fda5-4a30-ae4d-66ec36aeb26e","keyword":"改性沥青","originalKeyword":"改性沥青"},{"id":"54db9649-1e0d-4ed1-81e9-84b273668a97","keyword":"SBS改性剂","originalKeyword":"SBS改性剂"},{"id":"45690fb2-dbab-4f89-ab83-bed0ff385565","keyword":"相容剂","originalKeyword":"相容剂"},{"id":"13cee48f-5a15-4e51-a5a2-3315010837ac","keyword":"稳定剂","originalKeyword":"稳定剂"},{"id":"4084d161-2ce7-4acd-9e1d-3c8c5bdc64d4","keyword":"生产工艺","originalKeyword":"生产工艺"}],"language":"zh","publisherId":"gsytb201408018","title":"<span style=\"color:red\">永</span>古高速公路SBS改性沥青试验研究","volume":"33","year":"2014"},{"abstractinfo":"采用浓硫酸对5种不同来源的四氯苯醌和\"<span style=\"color:red\">永</span>固紫\"染料样品进行溶解分散,用甲苯提取和多层色谱柱纯化,利用同位素稀释法及高分辨气相色谱/质谱 (HRGC/HRMS)联用技术,测定了其中的多氯代二苯并二(口恶)(口英)/呋喃(PCDD/F)的质量比.结果表明\"<span style=\"color:red\">永</span>固紫\"染料及其原料中P CDD/F的质量比异常高,八氯代二苯并二(口恶)(口英)/呋喃(OCDD/F)已达到μg/g级甚至100 μg/g级,七氯代二苯并二(口恶)(口英)/呋喃(HpCDD/F)和六氯代二苯并二(口恶)(口英)/呋喃(HxCDD/F)质量比也达到 ng/g级.所有样品的毒性当量浓度(TEQ)均已超过10 pg/g的危险水平,是纺织品中PCDD/F的一类重要污染源.并进一步探讨了PCDD/F的来源.","authors":[{"authorName":"张庆华","id":"a0508650-85a5-4b40-bcd5-1fe36cc47da7","originalAuthorName":"张庆华"},{"authorName":"吴文忠","id":"277bbfc9-4c17-4304-bfe5-426d2212c8de","originalAuthorName":"吴文忠"},{"authorName":"占伟","id":"b14424b5-e4e7-49e5-8ede-37f906299bcf","originalAuthorName":"占伟"},{"authorName":"徐盈","id":"f7eddda3-96df-42eb-b756-b1d814f5ebb2","originalAuthorName":"徐盈"}],"doi":"10.3321/j.issn:1000-8713.2000.01.006","fpage":"21","id":"565f4845-690c-401a-aeb5-ef021b0ab222","issue":"1","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"9f06a77c-e98d-4780-a193-2c5f7014a9c7","keyword":"多氯代二苯并二(口恶)(口英)/呋喃","originalKeyword":"多氯代二苯并二(口恶)(口英)/呋喃"},{"id":"07b72d36-322a-4610-b4c6-a97b6d4e7c12","keyword":"染料","originalKeyword":"染料"},{"id":"853ea362-d40f-4c73-9f82-2cf868fd063c","keyword":"四氯苯醌","originalKeyword":"四氯苯醌"}],"language":"zh","publisherId":"sp200001006","title":"\"<span style=\"color:red\">永</span>固紫\"染料和四氯苯醌中多氯代二苯并二(口恶)(口英)/呋喃的分析","volume":"18","year":"2000"},{"abstractinfo":"","authors":[{"authorName":"王祝堂","id":"ae804cc4-cf2b-46f8-a76d-2194971a6727","originalAuthorName":"王祝堂"}],"doi":"10.3969/j.issn.1000-6826.2005.01.018","fpage":"40","id":"213c49f8-5c64-423c-8742-a6cadf61f42b","issue":"1","journal":{"abbrevTitle":"JSSJ","coverImgSrc":"journal/img/cover/3abe017a-2574-4821-8152-4ae974ef0471.jpg","id":"47","issnPpub":"1000-6826","publisherId":"JSSJ","title":"金属世界"},"keywords":[{"id":"ff41c7fc-a2f6-4522-a3a4-81db0d00395a","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"jssj200501018","title":"铝材状态家庭<span style=\"color:red\">喜</span>添新丁","volume":"","year":"2005"},{"abstractinfo":"","authors":[],"doi":"","fpage":"594","id":"a8f95271-0568-4acd-865c-8218cdeb0825","issue":"9","journal":{"abbrevTitle":"ZGCLJZ","coverImgSrc":"journal/img/cover/中国材料进展.jpg","id":"80","issnPpub":"1674-3962","publisherId":"ZGCLJZ","title":"中国材料进展"},"keywords":[{"id":"64725150-046a-4256-8cf4-c812b9b26e4d","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"zgcljz201409011","title":"专栏特约编辑赵<span style=\"color:red\">永</span>庆","volume":"","year":"2014"},{"abstractinfo":"","authors":[],"doi":"","fpage":"319","id":"88754d16-be8c-4fd1-9277-a7f03b1cc610","issue":"6","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰   "},"keywords":[{"id":"a57dd2aa-ab71-45c4-bafa-cba21325a5f2","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"ddyts201506006","title":"《丙烯酸涂料生产实用技术问答》（<span style=\"color:red\">汪</span>盛藻编著）等","volume":"","year":"2015"},{"abstractinfo":"钢铁工业的飞跃发展及其弊端,对工矿摩擦学提出了相应要求.润滑工程前沿技术的发展,要求与钢铁工业发展相适应,以求技术与管理的最大效应.","authors":[{"authorName":"陈祥斌","id":"cb14f6e8-f946-4c27-bea0-88e7c287ea24","originalAuthorName":"陈祥斌"},{"authorName":"于东","id":"968cae39-eefa-490c-84ff-185928cbd477","originalAuthorName":"于东"}],"doi":"10.3969/j.issn.1001-1560.2004.z1.005","fpage":"12","id":"e12f0091-69cc-4587-9a7c-68b12a41ab79","issue":"z1","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"46e725b4-8a1c-4e76-b2d9-af8660cdbea8","keyword":"钢铁工业","originalKeyword":"钢铁工业"},{"id":"18ffb71e-2b8d-4fd7-bd6c-d7bd92971940","keyword":"润滑技术","originalKeyword":"润滑技术"},{"id":"a3f08ae2-7201-4774-8aa3-5b5972637de4","keyword":"配伍","originalKeyword":"配伍"}],"language":"zh","publisherId":"clbh2004z1005","title":"钢铁行业的<span style=\"color:red\">喜</span>和忧及对工矿摩擦学的思考","volume":"37","year":"2004"}],"totalpage":5,"totalrecord":44}