{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"采用熔盐电脱氧法,以熔融的CaCl2-NaCl为电解质,经粉末压制烧结后的Nb2O5为阴极,石墨为阳极,电解制备了金属.并研究了压制压力、烧结温度、电解时间等因素对Nb2O5阴极电脱氧的影响.实验分析表明:阴极脱氧过程是由Nb2O5→NbO2→NbO→Nb且由阴极表面到内部逐步进行的,在适宜条件下可以得到纯度为99.5%以上的金属.","authors":[{"authorName":"谢大海","id":"9f842047-7306-44c9-966c-5dcdae033b1d","originalAuthorName":"谢大海"},{"authorName":"王兴庆","id":"e1f3e939-c4eb-46d9-b636-c42af39d5ed5","originalAuthorName":"王兴庆"},{"authorName":"陈发允","id":"374bbfc6-2968-4ea5-938c-c5032963cf1b","originalAuthorName":"陈发允"}],"doi":"10.3969/j.issn.1001-7208.2011.02.006","fpage":"23","id":"dd843846-6e1e-4093-bd07-ac81977e6bbe","issue":"2","journal":{"abbrevTitle":"SHJS","coverImgSrc":"journal/img/cover/SHJS.jpg","id":"59","issnPpub":"1001-7208","publisherId":"SHJS","title":"上海金属"},"keywords":[{"id":"7cc5aa7d-55f6-4dac-b31f-3aac3ae7a8ba","keyword":"熔盐电脱氧制备","originalKeyword":"熔盐电脱氧制备"},{"id":"4ab0a2e4-aae1-41ad-83fd-fbaa533f0287","keyword":"金属","originalKeyword":"金属铌"},{"id":"521240a0-7218-4e33-9c66-a14bd637278b","keyword":"Nb2O5","originalKeyword":"Nb2O5"},{"id":"736f08cb-6cb0-4af5-9490-fd851ff8322c","keyword":"压制烧结","originalKeyword":"压制烧结"}],"language":"zh","publisherId":"shjs201102006","title":"熔盐电脱氧制备金属的研究","volume":"33","year":"2011"},{"abstractinfo":"利用X射线衍射、TEM、EPMA、SEM等研究了含Nb堆焊金属中的碳化物分布形态及基体组织,分析了碳化物形成过程.结果表明,Nb的加入有利于形成大量碳化物硬质相,但Nb含量过多时,会形成铁素体基体及大量共晶碳化物,导致堆焊金属硬度过低;适量Ti、Nb、V共同作用时,能获得大量均匀分布的颗粒碳化物及马氏体或贝氏体基体,颗粒碳化物是以氧化物为核心的复合碳化物,内层Ti含量高于Nb,外层Nb含量高于Ti.","authors":[{"authorName":"张元彬","id":"7071086b-2ebc-4ed2-9339-23bddcf32498","originalAuthorName":"张元彬"},{"authorName":"史耀武","id":"ad187e0a-c20a-4425-a49d-0ab7f6a45a58","originalAuthorName":"史耀武"}],"doi":"","fpage":"408","id":"8dee0929-538b-40e4-9e4f-11a268886e67","issue":"z1","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"a598da9c-3895-4000-a849-1e07bde28e54","keyword":"","originalKeyword":"铌"},{"id":"65782618-deda-4ac5-8fad-17a8d0e930ba","keyword":"堆焊","originalKeyword":"堆焊"},{"id":"4be5af1e-aa26-41a4-8196-f5873ef4b189","keyword":"碳化物","originalKeyword":"碳化物"}],"language":"zh","publisherId":"cldb2006z1129","title":"在堆焊金属中的应用","volume":"20","year":"2006"},{"abstractinfo":"综述了LiNbO3、NaNbO3和KNbO3系无铅铁电陶瓷的最新研究进展及应用.对碱金属酸盐体系的掺杂和改性作了总结.介绍了目前制备酸盐陶瓷粉体所用方法,重点说明了水热法在碱金属酸盐陶瓷材料制备中的研究和应用现状.并展望了酸盐系无铅铁电陶瓷的发展趋势.","authors":[{"authorName":"王世平","id":"f51a4e2e-30e6-4f4d-9239-37a05dc8bd83","originalAuthorName":"王世平"},{"authorName":"苗鸿雁","id":"8f87d5d1-4e93-4c86-8113-49acf42f5b7d","originalAuthorName":"苗鸿雁"},{"authorName":"谈国强","id":"e15c1a74-d5f3-44c4-b02b-635c655c3d60","originalAuthorName":"谈国强"}],"doi":"10.3969/j.issn.1673-2812.2007.03.039","fpage":"486","id":"f8df66c2-0b30-4091-912a-5923397b2e8e","issue":"3","journal":{"abbrevTitle":"CLKXYGCXB","coverImgSrc":"journal/img/cover/CLKXYGCXB.jpg","id":"13","issnPpub":"1673-2812","publisherId":"CLKXYGCXB","title":"材料科学与工程学报"},"keywords":[{"id":"e28450fa-ee9b-4435-aea5-a7e49eea528e","keyword":"酸锂","originalKeyword":"铌酸锂"},{"id":"61bd8681-5434-4cec-bbc1-52b7111538e1","keyword":"酸钠","originalKeyword":"铌酸钠"},{"id":"63cacc7d-49e0-4ef0-acdf-743af47a75b3","keyword":"酸钾","originalKeyword":"铌酸钾"},{"id":"626f196d-2ab2-4286-8104-c2f29f8e2b38","keyword":"水热法","originalKeyword":"水热法"},{"id":"f8f025d9-368c-4e64-80bf-9197741d8ff2","keyword":"无铅铁电陶瓷","originalKeyword":"无铅铁电陶瓷"}],"language":"zh","publisherId":"clkxygc200703039","title":"碱金属酸盐铁电陶瓷的研究进展","volume":"25","year":"2007"},{"abstractinfo":"采用固体透氧膜(SOM)法直接电解还原Nb2O5制备金属Nb.在CaCl2熔盐体系中,电解电压控制为3.2V,以经过1 200℃预烧4 h成型的Nb2O5为阴极,氧化锆管内碳饱和的液态铜合金为阳极.研究电解时间分别为0.5、1、2和4 h以及不同温度下电解的特征规律和不同电解温度对阴极产物微结构的影响.结果表明:随着电解的进行,Nb2O5首先转变为Nb的一系列低价氧化物,进而才被还原成金属Nb;且随着实验温度的升高,电解速度相应加快,金属颗粒尺寸增大.与FFC法相比,SOM法具有更高的电解效率,1 150℃下的电解效率可达81.7%.","authors":[{"authorName":"何理","id":"d6256d8d-ccb4-4f9c-bdbf-589daa5546cd","originalAuthorName":"何理"},{"authorName":"","id":"d3a4ff7f-c72c-4538-81c7-fa56278e4887","originalAuthorName":""},{"authorName":"陈朝轶","id":"465f464a-477f-4517-b682-58b4e29b87fe","originalAuthorName":"陈朝轶"},{"authorName":"","id":"81b2b3da-e9fd-4c90-9c8d-3d6d03159633","originalAuthorName":""},{"authorName":"李重和","id":"3a382c96-2f29-4834-b12a-ed39ae7c19ea","originalAuthorName":"李重和"},{"authorName":"","id":"5bde2aec-eba6-4aca-953d-536820b3f8e6","originalAuthorName":""}],"doi":"","fpage":"1336","id":"d22d9b38-7a18-46b3-a167-9c915aecd428","issue":"7","journal":{"abbrevTitle":"ZGYSJSXB","coverImgSrc":"journal/img/cover/ZGYSJSXB.jpg","id":"88","issnPpub":"1004-0609","publisherId":"ZGYSJSXB","title":"中国有色金属学报"},"keywords":[{"id":"627845e7-9104-4c44-ac87-7b1df8fd9925","keyword":"固体透氧膜","originalKeyword":"固体透氧膜"},{"id":"07b5abc9-8771-4b9a-b9f7-98f271c0ce1d","keyword":"Nb2O5","originalKeyword":"Nb2O5"},{"id":"38ef3b1e-384b-4391-8549-e5a0d10f0777","keyword":"Nb","originalKeyword":"Nb"},{"id":"65e391c7-1f08-4771-8577-30803ea51471","keyword":"电化学","originalKeyword":"电化学"},{"id":"b6436f2c-3382-44fc-9b19-55b2e4587d02","keyword":"还原","originalKeyword":"还原"}],"language":"zh","publisherId":"zgysjsxb200807027","title":"固体透氧膜法制备金属","volume":"18","year":"2008"},{"abstractinfo":"采用粉末压片制样,使用X射线荧光光谱仪对含金属矿样中的进行测定.由于含的多金属矿标样极少且含量较低,实验选取钽矿石标准样品、矿区具有代表性的化学法定值多个样品,及其他土壤、岩石、多金属矿物标准样品、矿区定值样品混合配制的校准样品,制成一套含量5.9~2 700 μg/g、梯度适当的校准样品系列,绘制的校准曲线相关系数为0.998 6.采用经验系数和康普顿散射线内标法校正了基体效应,用Omnian近似定量软件、化学分析法与岩矿鉴定分析,确定了矿区矿物中主要成分SiO2、Al2O3、CaO、MgO、K2O、Pb、Zn、Cu、Fe、Zr、Mo、Rb、Hf、Th、U、Ti、Ga及稀土的最高允许量.综合考虑样品基体对检出限的影响,实验选取8个标准样品计算出检出限的平均值为1.62 μg/g.对岩石标样进行精密度考察,结果的相对标准偏差(RSD,n=12)为2.2% .对标准样品及矿区实际样品进行分析,测定值与认定值、实验室内其他方法的测定值及其他实验室的测定值吻合,满足《地质矿产实验室测试质量管理规范》的要求.","authors":[{"authorName":"梁祖顺","id":"2a4130da-0f99-4612-b30e-140790ea3435","originalAuthorName":"梁祖顺"},{"authorName":"李小莉","id":"3c583084-f714-481a-ab76-f009981274f2","originalAuthorName":"李小莉"},{"authorName":"刘峰","id":"40ea3fae-fc65-4b90-b72f-73dfb0404f45","originalAuthorName":"刘峰"},{"authorName":"李国会","id":"b31b96e7-4cd4-4445-8daa-ffe89d0eda4d","originalAuthorName":"李国会"}],"doi":"10.13228/j.issn.1000-7571.2014.10.013","fpage":"65","id":"0514aa4c-8da3-41df-970f-9e06d0c22cae","issue":"10","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析 "},"keywords":[{"id":"e1354d3d-48e9-4c6d-8e84-3f70ebf1f1f9","keyword":"X射线荧光光谱法","originalKeyword":"X射线荧光光谱法"},{"id":"4d335fbc-36c1-4d47-84f9-a0476ff35c74","keyword":"","originalKeyword":"铌"},{"id":"9d4f4b7f-18de-4fc7-869f-43db0f44d477","keyword":"粉末压片","originalKeyword":"粉末压片"},{"id":"f9100ff1-e014-42a3-bb2a-9b1ed85cba8f","keyword":"含金属矿样","originalKeyword":"含铌多金属矿样"}],"language":"zh","publisherId":"yjfx201410013","title":"粉末压片-X射线荧光光谱法测定含金属矿样中","volume":"34","year":"2014"},{"abstractinfo":"采用实际堆焊、Gleeble焊接热模拟、透射电镜及光学显微镜和硬度仪等分析了添加不同含量的铜和时,对多层焊焊缝金属显微组织和硬度的影响,探讨了铜和的作用机制.结果表明:在普通碳-锰焊缝金属的基础上添加质量分数约3.0%的铜和0.03%的时,在模拟多层焊各再热区域均可形成均匀的贝氏体组织,且产生大量均匀、热稳定性良好的沉淀析出相,使多层焊高强度焊缝具有均匀的硬度.","authors":[{"authorName":"陈大伟","id":"3947b98c-a721-4bc8-81ee-505dc9a5286f","originalAuthorName":"陈大伟"},{"authorName":"王青峰","id":"fbb938cb-d003-4ec4-a918-36be571007b4","originalAuthorName":"王青峰"},{"authorName":"苏航","id":"94c3369e-102c-4fb8-9699-186757a4df41","originalAuthorName":"苏航"}],"doi":"10.3969/j.issn.1000-3738.2007.01.025","fpage":"82","id":"5afeefca-634c-4d30-8882-a2103098a8cd","issue":"1","journal":{"abbrevTitle":"JXGCCL","coverImgSrc":"journal/img/cover/JXGCCL.jpg","id":"45","issnPpub":"1000-3738","publisherId":"JXGCCL","title":"机械工程材料"},"keywords":[{"id":"ca4dd47d-98b3-4f5c-a317-7121f8bf61f5","keyword":"焊缝金属","originalKeyword":"焊缝金属"},{"id":"9daf4868-f62a-4577-9e07-8c8f03895575","keyword":"铜","originalKeyword":"铜"},{"id":"a383225f-5f9c-4849-80fb-fe6cd8d16eb0","keyword":"","originalKeyword":"铌"},{"id":"8cdbed28-d6fb-44de-9d53-b3ca370321e7","keyword":"沉淀强化","originalKeyword":"沉淀强化"}],"language":"zh","publisherId":"jxgccl200701025","title":"铜和对多层焊焊缝金属显微组织和硬度的影响","volume":"31","year":"2007"},{"abstractinfo":"针对试样特点拟定了加大称样量以减轻偏析,以浓硝酸溶解样品破坏碳化物,加入氢氟酸助溶,分离稀土基体同时络合钛、钼、钨、和钽的方法,无须基底匹配,采用工作曲线法成功地测定了金属镧、铈、镨、钕、钐、铕、钆、铽、镝、钇中的钛、钼、钨、和钽量,测定范围:0.0050%~0.50%.","authors":[{"authorName":"崔爱端","id":"1cf81d7a-f18a-4d3c-a9d4-36e0668e1e2e","originalAuthorName":"崔爱端"},{"authorName":"杜梅","id":"63a899e4-1400-4f40-b23e-39ca57f30221","originalAuthorName":"杜梅"},{"authorName":"刘晓杰","id":"dbad6f82-fc9f-4d90-be7d-ca1fb6e8a2bf","originalAuthorName":"刘晓杰"}],"doi":"10.3969/j.issn.1004-0277.2005.01.015","fpage":"57","id":"927f401e-601c-4354-9478-963fda31ed21","issue":"1","journal":{"abbrevTitle":"XT","coverImgSrc":"journal/img/cover/XT.jpg","id":"65","issnPpub":"1004-0277","publisherId":"XT","title":"稀土"},"keywords":[{"id":"399ec5ac-e1f1-4232-a188-3ec884a53c5d","keyword":"钛","originalKeyword":"钛"},{"id":"b876be9f-4251-496a-a311-f5b22757bdc8","keyword":"钼","originalKeyword":"钼"},{"id":"5477f3b0-272b-4f1f-843c-5e821299a0fd","keyword":"钨","originalKeyword":"钨"},{"id":"5b97d4b9-be75-41a9-ae56-f7d0a8b077ff","keyword":"","originalKeyword":"铌"},{"id":"a7eccb9f-e522-4e74-9a4c-5acd233f30f6","keyword":"钽","originalKeyword":"钽"},{"id":"1b6a49e0-7539-497a-aa79-3db366c6ec90","keyword":"稀土金属","originalKeyword":"稀土金属"}],"language":"zh","publisherId":"xitu200501015","title":"ICP-AES法测定稀土金属中的钛、钼、钨、和钽","volume":"26","year":"2005"},{"abstractinfo":"研制9%Ni钢用镍基焊条的难点在于满足熔敷金属强度和塑性指标的前提下提高其低温韧性.在力学性能分析的基础上,采用彩色金相分析、扫描电镜及能谱分析、X射线衍射分析技术研究了对9%Ni钢用镍基焊条熔敷金属组织和性能的影响.试验结果表明,熔敷金属的加入能明显提高其强度和塑性.但的质量分数达到3.5%后,虽然熔敷金属的强度进一步提高,但形成了脆性的金属间化合物Laves相,导致熔敷金属低温韧性下降.","authors":[{"authorName":"吴智武","id":"a194b3cd-f50c-4d4e-922b-07212937435a","originalAuthorName":"吴智武"},{"authorName":"王移山","id":"552dab1d-d85e-4a5b-b750-1d26286175c0","originalAuthorName":"王移山"},{"authorName":"李少华","id":"79710205-ea57-45ad-89e2-7c3d749361be","originalAuthorName":"李少华"},{"authorName":"李箕福","id":"af488495-dbc4-4f3c-bb96-9469dcad067e","originalAuthorName":"李箕福"}],"doi":"","fpage":"28","id":"4f5ddc34-1fd7-4e14-a01d-6c28165bfee5","issue":"12","journal":{"abbrevTitle":"GTYJXB","coverImgSrc":"journal/img/cover/GTYJXB.jpg","id":"30","issnPpub":"1001-0963","publisherId":"GTYJXB","title":"钢铁研究学报"},"keywords":[{"id":"d2fd5e46-b13c-4453-9434-d0dd6b39232f","keyword":"9%Ni钢","originalKeyword":"9%Ni钢"},{"id":"083cd676-4bb5-4100-8f84-796e8f25ff3a","keyword":"焊接","originalKeyword":"焊接"},{"id":"10ca65b1-71ff-4158-9472-dd013017f9a7","keyword":"","originalKeyword":"铌"}],"language":"zh","publisherId":"gtyjxb200912007","title":"对9%Ni钢用镍基焊条熔敷金属组织和性能的影响","volume":"21","year":"2009"},{"abstractinfo":"设计了一种利用酸锂作为波导基片的双面金属包覆平板光波导,利用波导中超高阶导模高敏感特性制成了一种反射型光学电压传感器.入射激光束采用小角度入射,当光波导处于导模共振状态时,选择一个恰当的工作点,再通过两金属电极对该器件施加直流电压,通过检测反射光强,获得相应的电压值变化.实验测量中所用的电压范围是-800~800 V,得到的线性度值为0.995,波导反射光的反射率变化灵敏度为0.2% V-1,实验表明这种电压传感器具有较好的线性和灵敏度,该新型电压传感器具有结构与制作简单、调节方便和成本低廉等优点.","authors":[{"authorName":"袁文","id":"9e5d35d1-3d99-4f8f-9d96-5d7cb38f030f","originalAuthorName":"袁文"},{"authorName":"桑明煌","id":"b14938b0-7eab-4960-af0f-19c6eb2bb027","originalAuthorName":"桑明煌"},{"authorName":"陈险峰","id":"6e2881b9-e039-44c1-88e9-0b88497d2b2a","originalAuthorName":"陈险峰"},{"authorName":"肖平平","id":"85b314c4-27c4-46d7-86f9-2d921327ea84","originalAuthorName":"肖平平"},{"authorName":"曹庄琪","id":"0adb586a-cc07-45b8-b478-ebc6752d9755","originalAuthorName":"曹庄琪"},{"authorName":"郭琴","id":"2064de3e-84d4-4f4c-b5d3-7f9e8db110ef","originalAuthorName":"郭琴"}],"doi":"10.3969/j.issn.1007-5461.2011.02.014","fpage":"202","id":"e4ccdfbc-d364-4fec-bb01-8db6ca8635b7","issue":"2","journal":{"abbrevTitle":"LZDZXB","coverImgSrc":"journal/img/cover/LZDZXB.jpg","id":"53","issnPpub":"1007-5461","publisherId":"LZDZXB","title":"量子电子学报 "},"keywords":[{"id":"a10ba7be-4886-478b-9329-03d909c87bc6","keyword":"导波光学","originalKeyword":"导波光学"},{"id":"2c8f155b-83c2-4636-af25-eda8cb597b8f","keyword":"双面金属波导","originalKeyword":"双面金属波导"},{"id":"7705942d-dd10-44d2-b007-87f28a4d205a","keyword":"酸锂","originalKeyword":"铌酸锂"},{"id":"a03c4eb6-29fe-4dec-a2db-4dfcca0c6912","keyword":"电压传感","originalKeyword":"电压传感"}],"language":"zh","publisherId":"lzdzxb201102014","title":"酸锂双面金属包覆波导电压传感特性","volume":"28","year":"2011"},{"abstractinfo":"针对我国包头现有高炉-转炉-电炉-电炉提工艺存在流程长、成本高、损失率大且只能生产含13 %~15 %铁的情况,提出包头资源选冶新思路:用CO-CO2混合气体选择性热还原含铁矿,90 %以上的铁矿物被还原为金属铁,矿物不被还原.磁选分离被还原的金属铁和其他矿物,得到含Nb2O5为6.91 %的含氧化物,其品位较原矿富集了4倍.然后用盐酸浸洗上述含氧化物,90 %以上的铁矿物、磷矿物以及CaO和MgO进入浸液,儿乎全部留在浸渣中,得到的浸渣含Nb2O5近30 %,Nb/Fe=6,Nb/P=12,此浸渣可用于冶炼符合工业标准的铁(含60 %~65 %Nb).","authors":[{"authorName":"陈宏","id":"882e0fa3-0e0e-4414-afd5-dbcf58aafb91","originalAuthorName":"陈宏"},{"authorName":"韩其勇","id":"ccaae70d-9d66-47a5-a899-7a400a9a4032","originalAuthorName":"韩其勇"},{"authorName":"魏寿昆","id":"89c546b2-1edd-4fa9-9ffb-2f61126207c5","originalAuthorName":"魏寿昆"},{"authorName":"胡志高","id":"1732ea93-630a-4038-af98-761222422c01","originalAuthorName":"胡志高"}],"doi":"","fpage":"13","id":"3a13fdae-6c10-4739-b36f-fdeddc8ece44","issue":"3","journal":{"abbrevTitle":"GT","coverImgSrc":"journal/img/cover/GT.jpg","id":"27","issnPpub":"0449-749X","publisherId":"GT","title":"钢铁"},"keywords":[{"id":"4040c857-79a6-416e-a789-461de4d4499b","keyword":"含铁矿","originalKeyword":"含铌铁矿"},{"id":"a2001cb7-1884-4930-8555-66a3d62ce956","keyword":"选择性还原","originalKeyword":"选择性还原"},{"id":"c0c46c47-73b3-46c6-9b28-696ee0d16b62","keyword":"酸浸","originalKeyword":"酸浸"},{"id":"d6bc004d-4c94-4128-afc5-88a90a86c25a","keyword":"含氧化物","originalKeyword":"含铌氧化物"},{"id":"f00c68f7-a7a2-4b16-ba8f-8344fac36cfc","keyword":"铁","originalKeyword":"铌铁"}],"language":"zh","publisherId":"gt199903004","title":"从含铁矿中提及制铁的新方法","volume":"","year":"1999"}],"totalpage":2189,"totalrecord":21884}