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Synthesis and Characterization of Mixed Al+AlN Nanoparticles

Xiangcheng SUN , Mingchuan YANG , Feng YE , Xiukui SUN and Wenduo WEI(State Key Lab. for RSA , Institute of Metal Research , Chinese Academy of Sciences , Shenyang 110015 , China)Yingda YU and Dehai PING(Lab. of Atomic Imaging of Solids , Institute of Metal Resea

材料科学技术(英文)

Mixed Al+AlN nanoparticles were synthesized by an active plasma-metal reaction method. Mean particle size of the mixed Al+AlN nanoparticles is about 30-50 nm. Defects were found in some AlN particles. Moreover, the AlN ratio and its particle size in mixed Al+AIN nanoparticles obtained in different atmospheres (N2+Ar) increase with increasing N2 particle pressure, and the specific sudece areas of the mixed Al+AlN nanoparticles increase with the AlN ratio. The surface degradation of the Al+AlN exposed to air is estimated by the infrared absorption spectra

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Surface Degradation of Bulk AlN+Al Nano-composites

Xiangcheng SUN , Feng YE , Xaoping SONG , Mngchuan YANG and Xiukui SUN (State Key Lab. for RSA , Institute of Metal Research , Chinese Academy of Sciellces , Shenyang 110015 , China)

材料科学技术(英文)

Bulk AlN + Al nanocomposite materials were Synthesized by sintering the compacts of AlN and Al nanoparticles, which were produced by an active plasma-metal reaction method. The sudeces of as-prepared nanocomposite was investigated by X-ray photoelectron spectroscopy (XPS).Results show the surfaces are much degraded and the degradation products are alumina(Al2O3),boehmite(AIOOH), bayerite(AI(OH)3) layer. The mechanism of degradation behaviour in moist environment was also discussed

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