ZHU Na-qiong
,
LU Li
,
HE Yan-lin
,
LI Lin
,
LU Xiao-gang
钢铁研究学报(英文版)
Coarsening of M23C6 precipitates in an Fe-12.4Cr-0.13C ternary alloy has been investigated ageing at 780 ℃ up to 200 h. Evolution of M23C6 carbides at different ageing times was determined experimentally using transmission electron microscopy. Particle size distribution was obtained with different measuring methods. Simulations of coarsening of M23C6 precipitates were carried out using computational thermodynamics and kinetics. Results showed low coarsening rates for M23C6 precipitates in the Fe-Cr-C ternary alloy. Interfacial energy of M23C6/ferrite interface is between 0.1 and 0.3 J·m-2 for the coarsening of M23C6 ageing at 780 ℃.
关键词:
M23C6
,
coarsening
,
PSD
,
interfacial energy
LIU Xiong
,
DING Xing-ping
,
HE Yan-lin
,
et al
钢铁研究学报(英文版)
Aging treatments at the temperature range of 1000-1200 ℃ for different time intervals (10, 30, 60min) in a solution-treated 2205 duplex stainless steel(DSS) are carried out respectively. The migration of γ/α interface boundary after different ageing treatments is measured by optical metallography and calculated by DICTRA software. The agreement of the calculation and experimental results is satisfied. The migration of γ/α interface boundary with increased keeping time depends on the chemical potential of chromium in each phase. At the aging temperature of 1100℃, the back diffusion effect of chromium results in the opposite direction migration of γ/α interface, therefore, the ferrite volume fraction gets lower at first and then gets higher after 1800s diffusion
关键词:
WANG Hua
,
SHI Wen
,
HE Yan-lin
,
LU Xiao-gang
,
LI Lin
钢铁研究学报(英文版)
Specimens of two different kinds of bake hardening steels (BH-Mn and BH-P) were prepared and treated with different annealing processes (water quenching and overaging). A novel technique of three dimensional atom probe was used to investigate solute distributions in these steels. The results indicate that C concentration decreases, whereas V increases during overaging in both bake hardening steels. The conclusion that no vanadium carbides precipitate during the overaging is therefore originally obtained by microanalysis in bake hardening steels. Moreover, bake hardening values of all the specimens were tested by tensile experiments with 2% pre-deformation. However, those of overaged specimens were further measured with higher levels of pre-deformation because no bake hardening phenomenon was present at 2% pre-deformation. As the pre-deformation increases from 2% to 6% and 8%, both overaged steels show bake hardening values, and the value data are almost the same.
关键词:
ultra-low carbon
,
bake hardening steel
,
three dimensional atom probe
,
solute C
,
water quenching
,
overaging
,
bake hardening phenomenon
