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Nano ZrO2 Particulate-reinforced Lead-Free Solder Composite

Jun SHEN , Yongchang LIU , Dongjiang WANG , Houxiu GAO

材料科学技术(英文)

A lead-free solder composite was prepared by adding ZrO2 nanopowders in eutectic Sn-Ag alloy. Microstructural features and microhardness properties of those solders with different ZrO2 nanopowder fraction were examined. Results indicate that the addition of ZrO2 nanopowders reduced the size of β-Sn grains and restrained the formation of bulk Ag3Sn intermetallic compounds (IMCs) due to the adsorption effect of the ZrO2 particles. The Vicker's hardness of the obtained lead-free solder composites fits well with the Hall-Petch relationship. The refinement of β-Sn grains favors to improve the microhardness of composite solders.

关键词: ZrO2 nanopowders , null , null , null

Effects of Austenite Stabilization on the Onset of Martensite Transformation in T91 Steel

Baoqun NING , Yongchang LIU , Qingzhi SHI

材料科学技术(英文)

The influences of thermal stabilization of austenitic on the onset temperature for a martensite transformation in T91 ferritic heat-resistant steel were studied by high-resolution differential dilatometer. The phase transformation kinetic information was obtained by adopting lever rule from the recorded dilatometric curves. The results show that an inverse stabilization, featured by the damage of “the atmosphere of carbon atoms” and the increase of the starting temperature for martensite transformation takes place when the T91 ferritic steel is isothermally treated above the Ms point, and it becomes strong with increasing the holding time. While the continued temperature for martensite transformation decreases gradually when isothermally holding at a temperature below Ms point. The observed inverse stabilization behavior could be attributed to the relatively high temperature of Ms point in the explored T91 ferritic heat-resistant steel.

关键词: T91 ferritic heat-resistant steel , 奥氏体热稳定化 , 碳原子气

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