Haibin CHENG
,
Shuai XU
,
Wenyu ZHAO
,
Suling ZHAO
,
Pengcheng ZHAI
,
Zhigang SUN
,
Qingjie ZHANG
材料科学技术（英）
Electroless CoNiWP magnetic films were prepared by varying the bath pH and then characterized by energy dispersive X-ray analysis, X-ray diffraction and magnetic force microscopy. It has been found that the microstructure and the magnetic properties of films were influenced greatly by the bath pH. At the bath pH 8.06, the grain size and coercivity of the films reach maximum, while the squareness (Mr=Ms) of MH curves reaches minimum. The Henkel plots indicates that the exchange-coupling interaction is very weak at this pH, which may be caused by phase-separation and large grain size, and then results in the lowest squareness. At pH above 8.5, obvious exchange-coupling interaction is observed because of the inexistence of phase-separation and the refinement of grain size.
关键词:
CoNiWP magnetic film
,
Bath
,
pH
,
Squarenes
,
Exchang
Daihua HE
,
Zhengyi FU
,
Qingjie ZHANG
材料科学技术（英）
Combustion reaction welding, one promising method to weld ceramics and metals, was used to weld TiB¬2 and Mo. The results showed that the reacted products through combustion reaction were TiB¬2 and MoB when the Mo contents in reactants were 20 wt pct and 40 wt pct while there was Mo besides MoB and TiB¬2 when there were 60 wt pct and 80 wt pct Mo in reactants. Diffusion of elements occurred at the interfaces of the two substrates. The interfaces between the reacted and the two substrates were indistinct after being welded. The welding temperature strongly affected properties of the samples. The value of bending strength of the sample with 80 wt pct Mo in reactant welded at 1500℃ was the highest, 368.52 MPa. The highest value of shear strength among all the samples was that of the one with 40 wt pct Mo in reactant welded at 1500℃, 50.97 MPa.
关键词:
Combustion reaction welding
,
null
,
null
,
null
