H. Ying1)
,
X. D. Sun1)
,
Q. B. Yang1)
,
J. B. Li2)
,
Y. M. Wang2)
,
Z. Zhang3) and J. You3)1) School of Materials and Metallurgy
,
Northeastern University
,
Shenyang 110006
,
China2) Departm ent of Materials
,
School of Mechanical Engineering
,
Shenyang University
,
Shenyang110044
,
China3) Liaoning Analyzing and Testing Research Center
,
Shenyang 110015
,
China
金属学报(英文版)
Starting from cheap inorganic salts , ultrafine P L Z T po w ders were synthesized by a co pre cipitation m ethod . The results show that the precursor precipitate obtained by the co precipita tion method transfor ms co m pletely to P L Z T phase by calcining at 420 ℃ for 4 hours , about300 ℃low er than the nor m al transform ation te m perature of P L Z T obtained by m ixed oxidemethod . The effect of residual N H4 N O3 in the precursor precipitate on transfor m ation te m perature of the P L Z Tpow der w as investigated . The residual N H4 N O3 in the precursor po w der can reduce further the P L Z Ttransfor m ation tem perature to about 300 ℃, but a sm alla mount of Zr O2 and Pb Ti O3 re m ained . By a proper control of the synthesizing route , a P L Z T po w der with a pri m ary particle size of 10 n m and an agglom eration size of 0 3 μm hasbeen produced .
关键词:
P L Z T
,
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,
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