{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"研制了用溴邻苯三酚红(BPR)作修饰剂的碳糊修饰电极,将此电极用作工作电极,建立于CuCl存在下测定痕量锑的阳极溶出伏安法.研究了阳极溶出测定锑的条件.方法灵敏度高,检出限达2.0×10-9mol/L;选择性好,不用预分离直接测定锌电解液中痕量锑,结果满意.","authors":[{"authorName":"<span style=\"color:red\">夏</span><span style=\"color:red\">姣</span><span style=\"color:red\">云</span>","id":"323b0af9-f144-40aa-ba9b-41350a34e703","originalAuthorName":"夏姣云"},{"authorName":"严规有","id":"621a8c3c-506a-4818-aa18-fa58f8f18045","originalAuthorName":"严规有"}],"doi":"10.3969/j.issn.1000-7571.2004.03.001","fpage":"1","id":"2a48c913-cf45-4f36-b70d-4df48cb4fc65","issue":"3","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"44a5902f-22cb-4eab-8fde-790ddba93443","keyword":"碳糊修饰电极","originalKeyword":"碳糊修饰电极"},{"id":"49d0c5eb-94c2-4c1b-b355-8e773941da58","keyword":"锌电解液","originalKeyword":"锌电解液"},{"id":"2a840f3c-10e2-4d99-95b1-c76a6b3ea3ec","keyword":"吸附伏安法","originalKeyword":"吸附伏安法"},{"id":"a0a2450b-3650-466e-a520-e97e7a7cd64e","keyword":"锑","originalKeyword":"锑"}],"language":"zh","publisherId":"yjfx200403001","title":"溴邻苯三酚红修饰碳糊电极的研制及微量锑的测定","volume":"24","year":"2004"},{"abstractinfo":"在pH4.0的苯二甲酸氢钾介质中,有KBrO3存在的情况下,V(Ⅴ)与邻苯二酚紫(CV)生成络合物,在-0.83V(vs.SCE)处出现一灵敏的极谱峰.峰电流与V(Ⅴ)的浓度在8×10-8～2.4×10-6mol/L范围内呈线性关系,检出限为2×10-8mol/L.体系选择性好,灵敏度高,用于钢中痕量钒的测定,重复性好,结果满意.","authors":[{"authorName":"严规有","id":"3f72151a-a369-4a1c-9cb0-ed1c582be3ef","originalAuthorName":"严规有"},{"authorName":"<span style=\"color:red\">夏</span><span style=\"color:red\">姣</span><span style=\"color:red\">云</span>","id":"102b4a35-c5e1-4242-8995-816ad1657f58","originalAuthorName":"夏姣云"},{"authorName":"李竹英","id":"785359a0-d926-4a11-ae58-7b4b480e4425","originalAuthorName":"李竹英"},{"authorName":"杨娟玉","id":"60ee6754-19f2-4e56-a4e9-4a3c6bb107e9","originalAuthorName":"杨娟玉"},{"authorName":"王晓敏","id":"21e3e112-a76e-48d5-a6b1-4d2a2accf671","originalAuthorName":"王晓敏"}],"doi":"10.3969/j.issn.1000-7571.2003.01.010","fpage":"30","id":"575b90a9-b1fa-4e8a-a1ca-96bf201f2551","issue":"1","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"1e8ee5e2-eeda-44b5-94d3-7b75cac16efd","keyword":"钒","originalKeyword":"钒"},{"id":"38baaa5f-9855-4fe6-b6c7-122523691f13","keyword":"催化极谱法","originalKeyword":"催化极谱法"},{"id":"51498cba-0c27-420a-9458-df3630e0b1e5","keyword":"钢","originalKeyword":"钢"}],"language":"zh","publisherId":"yjfx200301010","title":"催化极谱法测定钢中痕量钒","volume":"23","year":"2003"},{"abstractinfo":"以巯基乙酸(TGA)为稳定剂,在加热回流氮气保护条件下制备CdTe量子点,用荧光分光光度计、透射电子显微镜和X射线粉末衍射仪对CdTe量子点进行表征.以该量子点为荧光探针,完善荧光淬灭法测定Cu2+、Hg2和Ag+等重金属离子的方法.考察缓冲溶液的pH值、反应时间、量子点浓度、量子点的稳定性和干扰离子等多种因素对重金属离子测定的影响.在pH值为6.2的三羟甲基氨基甲烷(tris)-盐酸缓冲溶液中,当量子点的浓度为4.2×10-2 μg/L和反应时间为30 min时,测得Cu2、Hg2+和Ag+的线性区间分别为2.3 ～250 μg、3.2～300 μg和4.3～ 150μg,检测下限分别为0.28 μg/L、0.53 μg/L和0.35 μg/L.并发现只有当所测量的重金属离子能与所采用的量子点能生成更难溶于水的沉淀才能引起量子点的荧光淬火,从而可以对此类重金属离子进行定量检测.","authors":[{"authorName":"<span style=\"color:red\">夏</span><span style=\"color:red\">姣</span><span style=\"color:red\">云</span>","id":"9e221045-a3e9-4f08-9b06-2c3d23cf1c08","originalAuthorName":"夏姣云"},{"authorName":"徐万邦","id":"9c6f3ca3-3936-4d48-a55a-289ab827a634","originalAuthorName":"徐万邦"}],"doi":"","fpage":"193","id":"88a0bb26-4ec2-48cf-a4f6-0abf604c66c1","issue":"1","journal":{"abbrevTitle":"RGJTXB","coverImgSrc":"journal/img/cover/RGJTXB.jpg","id":"57","issnPpub":"1000-985X","publisherId":"RGJTXB","title":"人工晶体学报"},"keywords":[{"id":"2649f21e-168a-4c4b-aeda-0805172b5cd9","keyword":"碲化镉","originalKeyword":"碲化镉"},{"id":"cd98fe1d-dbfd-49c4-87f1-393860b00926","keyword":"荧光探针","originalKeyword":"荧光探针"},{"id":"07fcf6b6-f07a-475d-847c-9786c9cafea2","keyword":"量子点","originalKeyword":"量子点"}],"language":"zh","publisherId":"rgjtxb98201201038","title":"TGA-CdTe量子点在荧光探针方面应用","volume":"41","year":"2012"},{"abstractinfo":"以3-巯基丙基三甲氧基硅烷(MPS)为修饰剂,直接法制备得到闪锌矿结构的CdSe@SiO2核-壳型量子点,该方法简化了制备硅烷化核-壳型量子点的流程,缩短了制备的时间.用荧光分光光度计,透射电子显微镜,X射线粉末衍射仪等分析测试方法对得到的核-壳型核-壳型量子点的性能进行表征.结果表明:n(Cd2+):n(SeSO2-3)和反应体系Ph值,对纳米晶的光学性质具有显著影响.在最佳合成条件下得到的CdTe@SiO2纳米粒子的平均粒径约为20nm,其大小均匀.与CdSe纳米粒子相比,CdSe@SiO2核-壳型量子点光化学性能较稳定,常温下可以放置半年以上.SiO2包覆的CdSe纳米粒子有效地提高了核-壳型量子点的稳定性,大大增强了其抗光漂白性能.","authors":[{"authorName":"<span style=\"color:red\">夏</span><span style=\"color:red\">姣</span><span style=\"color:red\">云</span>","id":"09806c4e-7abe-49f9-a26d-1361bd745259","originalAuthorName":"夏姣云"},{"authorName":"徐万帮","id":"d072efec-934c-4c37-b091-32f5840936fa","originalAuthorName":"徐万帮"}],"doi":"","fpage":"251","id":"f05b7e89-2ac4-449c-b212-fe5a39882594","issue":"1","journal":{"abbrevTitle":"RGJTXB","coverImgSrc":"journal/img/cover/RGJTXB.jpg","id":"57","issnPpub":"1000-985X","publisherId":"RGJTXB","title":"人工晶体学报"},"keywords":[{"id":"8210fc41-344d-47b2-ad42-e11deec75e93","keyword":"CdSe@SiO2","originalKeyword":"CdSe@SiO2"},{"id":"37d01235-bd70-40cd-93a7-36480ea086dc","keyword":"纳米粒子","originalKeyword":"纳米粒子"},{"id":"26f5d169-e93c-45d8-a176-7d3aa3850ca9","keyword":"硅烷偶联剂","originalKeyword":"硅烷偶联剂"},{"id":"5ed0c487-7f4b-4a77-b481-cdbd12036e8c","keyword":"直接合成","originalKeyword":"直接合成"}],"language":"zh","publisherId":"rgjtxb98201101049","title":"直接合成法制备CdSe@SiO2荧光纳米材料","volume":"40","year":"2011"},{"abstractinfo":"","authors":[{"authorName":"严规有","id":"f0e9adde-dd71-4fde-8a55-9a473f157435","originalAuthorName":"严规有"},{"authorName":"<span style=\"color:red\">夏</span><span style=\"color:red\">姣</span><span style=\"color:red\">云</span>","id":"71d9269b-178a-4e19-91b1-c5a18af7fdef","originalAuthorName":"夏姣云"},{"authorName":"王彦","id":"1c7cde16-d21c-40e4-b8a6-547e42d8dd1c","originalAuthorName":"王彦"}],"doi":"10.3969/j.issn.1000-7571.1999.03.014","fpage":"37","id":"dc433334-7d7c-499b-8d63-98c007aaadeb","issue":"3","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"7aac4844-3c35-4464-a5ed-46ab6b1a9828","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"yjfx199903014","title":"催化极谱法直接快速测定钢中微量钼","volume":"19","year":"1999"},{"abstractinfo":"为了比较几种自动化测云仪器的性能,中国气象局气象探测中心在南京信息工程大学的气象探测基地首次组织了一次为期近5个月的比对试验,试验仪器包括四台激光<span style=\"color:red\">云</span>高仪、两部红外测云仪、一台全天空成像仪以及一部毫米波<span style=\"color:red\">云</span>雷达.对其中大部分仪器取得的三个月<span style=\"color:red\">云</span>底高度数据进行了初步分析,结果表明:三台激光<span style=\"color:red\">云</span>高仪测量结果比较一致；两部红外测云仪在测量低云时一致性稍差；<span style=\"color:red\">云</span>雷达与激光<span style=\"color:red\">云</span>高仪测量的最低层云底高度数据一致性较差,但与红外测云仪的测量结果匹配较好.","authors":[{"authorName":"黄兴友","id":"ab1918ea-4979-44a9-bc78-6a184f16960f","originalAuthorName":"黄兴友"},{"authorName":"胡汉峰","id":"e31b1f2c-a61b-466b-a0e8-23915c86b389","originalAuthorName":"胡汉峰"},{"authorName":"<span style=\"color:red\">夏</span>俊荣","id":"f8fcf8ee-ece7-4b2b-9022-f14685b68fa8","originalAuthorName":"夏俊荣"},{"authorName":"卜令兵","id":"d2123620-5158-4198-aa7d-c86d5eaaa362","originalAuthorName":"卜令兵"},{"authorName":"张雪芬","id":"f5e54ac7-727f-4888-aaf6-bb7be02faf50","originalAuthorName":"张雪芬"},{"authorName":"雷勇","id":"65805f0d-18fe-4259-9178-d3380e50a32f","originalAuthorName":"雷勇"},{"authorName":"黄建松","id":"f8f737b5-899d-4bb5-a695-4f2ce0acc798","originalAuthorName":"黄建松"},{"authorName":"王巍巍","id":"263663b2-cd8b-402d-aa28-a1281907f1ce","originalAuthorName":"王巍巍"},{"authorName":"吴迪","id":"f9cb8422-eb40-4180-8dba-b1dbece6c1c0","originalAuthorName":"吴迪"},{"authorName":"蒋昌华","id":"2fab0bdb-dbb3-4248-89ea-8cd2cf0113d8","originalAuthorName":"蒋昌华"}],"doi":"10.3969/j.issn.1007-5461.2013.01.013","fpage":"73","id":"9958e720-9dba-4430-bfc1-dce894108b82","issue":"1","journal":{"abbrevTitle":"LZDZXB","coverImgSrc":"journal/img/cover/LZDZXB.jpg","id":"53","issnPpub":"1007-5461","publisherId":"LZDZXB","title":"量子电子学报   "},"keywords":[{"id":"515e85eb-4059-4f54-808a-baed98faaab2","keyword":"大气光学","originalKeyword":"大气光学"},{"id":"08f03b33-4a9d-4eb8-95c9-db91bcd5e415","keyword":"<span style=\"color:red\">云</span>底高","originalKeyword":"云底高"},{"id":"e161ff5d-2d6c-45c4-9da4-02a4841c291e","keyword":"激光<span style=\"color:red\">云</span>高仪","originalKeyword":"激光云高仪"},{"id":"5dfeb526-9cc5-4ba1-97c6-934661e00f12","keyword":"红外测云仪","originalKeyword":"红外测云仪"},{"id":"e3470aec-3087-4fbe-859f-07adb1c6dc67","keyword":"<span style=\"color:red\">云</span>雷达","originalKeyword":"云雷达"}],"language":"zh","publisherId":"lzdzxb201301013","title":"<span style=\"color:red\">云</span>底高度的激光<span style=\"color:red\">云</span>高仪、红外测云仪以及<span style=\"color:red\">云</span>雷达观测比对分析","volume":"30","year":"2013"},{"abstractinfo":"采用特级矾土、黏土为主要原料,液体磷酸盐做结合剂,制备了6种满足不同施工方式的w(Al2O3)>70%的高铝可塑料,并采用马<span style=\"color:red\">夏</span>值测定仪测定了可塑料的可塑性.结果表明:马<span style=\"color:red\">夏</span>值测定法可以用于耐火可塑料的可塑性测定,而且其检测范围更宽,可测定采用橡皮锤人工捣打或风镐机械捣打等不同施工方式的可塑料的可塑性.橡皮锤人工捣打可塑料的马<span style=\"color:red\">夏</span>值范围为1.36～3.74 MPa,风镐机械捣打可塑料的马<span style=\"color:red\">夏</span>值范围为7.1～22 MPa.","authors":[{"authorName":"曹喜营","id":"75c4caa4-cb66-4650-9067-a96802cbd298","originalAuthorName":"曹喜营"},{"authorName":"张三华","id":"43ffecdb-33e9-4587-943d-7c3cca4ceb55","originalAuthorName":"张三华"},{"authorName":"石会营","id":"74153ff2-9fb1-4c8a-ab01-11ea89d857bb","originalAuthorName":"石会营"},{"authorName":"王金相","id":"2a1842f6-d156-4294-9978-b13ab33937d2","originalAuthorName":"王金相"},{"authorName":"洪彦若","id":"1ba110b1-55eb-4bdb-9617-fa7f68da0f6e","originalAuthorName":"洪彦若"},{"authorName":"李再耕","id":"bf228091-639a-406c-979b-de66faebbf18","originalAuthorName":"李再耕"}],"doi":"10.3969/j.issn.1001-1935.2009.06.015","fpage":"456","id":"1f9ca5f2-d90c-4817-a0ea-f1443735996c","issue":"6","journal":{"abbrevTitle":"NHCL","coverImgSrc":"journal/img/cover/NHCL.jpg","id":"55","issnPpub":"1001-1935","publisherId":"NHCL","title":"耐火材料   "},"keywords":[{"id":"c6527163-0345-4f02-86c3-414f7ac5e25e","keyword":"耐火可塑料","originalKeyword":"耐火可塑料"},{"id":"17abe30e-e375-4791-90c4-3902889717d3","keyword":"马<span style=\"color:red\">夏</span>值","originalKeyword":"马夏值"},{"id":"e85deede-fb42-4f63-94ec-fc04241724db","keyword":"可塑性","originalKeyword":"可塑性"},{"id":"6b06311f-183d-4f12-956d-3348733d141c","keyword":"施工方法","originalKeyword":"施工方法"}],"language":"zh","publisherId":"nhcl200906015","title":"耐火可塑料马<span style=\"color:red\">夏</span>值的测定","volume":"43","year":"2009"},{"abstractinfo":"<span style=\"color:red\">夏</span>甸金矿充分利用现有的提升系统,将相邻两矿区提升系统统筹考虑,进行优化,应用取得了良好的经济效益和社会效益.","authors":[{"authorName":"郭建军","id":"d945edcb-4fdd-499c-8977-99e04e8f8cf6","originalAuthorName":"郭建军"},{"authorName":"江国建","id":"a7c42ef0-b58e-487a-9090-4531806698d3","originalAuthorName":"江国建"},{"authorName":"汪宗文","id":"34a7195c-e1a3-40db-bca3-9c627c0ac75b","originalAuthorName":"汪宗文"}],"doi":"10.3969/j.issn.1001-1277.2002.11.007","fpage":"23","id":"e2b820e3-93d9-40ef-9daa-e7b94b145154","issue":"11","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"5859fd11-c34e-4afd-82a8-c123fb734309","keyword":"提升系统","originalKeyword":"提升系统"},{"id":"37fa81cf-d76a-4286-b154-1093df03403f","keyword":"优化","originalKeyword":"优化"},{"id":"c2f48dcc-29af-4ad1-92e0-d6a3b0d92b7d","keyword":"应用","originalKeyword":"应用"}],"language":"zh","publisherId":"huangj200211007","title":"<span style=\"color:red\">夏</span>甸金矿提升系统优化与应用","volume":"23","year":"2002"},{"abstractinfo":"为增加<span style=\"color:red\">夏</span>甸金矿分级尾砂供应量,提高了全尾砂旋流器分级产率并开展了相关充填材料试验.介绍了分级尾砂胶结充填体强度试验、分级尾砂充填料浆塌落度试验及分级尾砂胶结充填料浆凝固时间测定试验.试验结果表明,<span style=\"color:red\">夏</span>甸金矿选厂全尾砂经旋流器分级的尾砂是一种良好的充填骨料,可以作为充填骨料进行充填.试验所得数据和结论对于矿山充填作业具有直接的指导意义.","authors":[{"authorName":"唐占信","id":"aa836ffb-04bf-4cf2-b40d-15d21cec1bcc","originalAuthorName":"唐占信"},{"authorName":"王金波","id":"c21424a5-101a-4d3a-8db8-7c44266b56d0","originalAuthorName":"王金波"},{"authorName":"周东良","id":"aa957e67-c6f6-4bca-b58f-690e533d83a0","originalAuthorName":"周东良"},{"authorName":"秦秀合","id":"e0c97c79-3a9e-4842-8554-237497382d73","originalAuthorName":"秦秀合"},{"authorName":"何少博","id":"9db332f4-b62b-4f75-b856-93722da06c0d","originalAuthorName":"何少博"},{"authorName":"林卫星","id":"74f43218-c920-45de-915e-588bdba33e0d","originalAuthorName":"林卫星"}],"doi":"10.11792/hj20160610","fpage":"43","id":"a04551f3-5105-4102-8b07-480b3e6c1324","issue":"6","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"b2a05bf2-7eac-4d01-bd4e-87ea233a935b","keyword":"充填采矿","originalKeyword":"充填采矿"},{"id":"6d635d11-a300-4f28-8dce-b57692cad022","keyword":"分级尾砂","originalKeyword":"分级尾砂"},{"id":"02d88ffe-26d5-40fc-80bd-a18d7efb3746","keyword":"强度","originalKeyword":"强度"},{"id":"a6fa0929-3d36-4d96-8a85-7a29d766b0a2","keyword":"塌落度","originalKeyword":"塌落度"},{"id":"a259b871-69b8-49a0-9377-4ef797df93d0","keyword":"凝结时间","originalKeyword":"凝结时间"}],"language":"zh","publisherId":"huangj201606014","title":"<span style=\"color:red\">夏</span>甸金矿分级尾砂充填材料试验研究","volume":"37","year":"2016"},{"abstractinfo":"为了合理利用<span style=\"color:red\">云</span>铜渣,采用ITmk3工艺获得高质量粒铁,在实验室条件下进行了一系列的基础研究.通过比较试样全铁质量和熔分得到的粒铁质量,得到了金属铁的收得率,结合化学分析方法,分别得到了试样还原后的金属化率以及熔分后金属铁中的碳质量分数,研究了各个因素对以上指标的影响规律,形成了对<span style=\"color:red\">云</span>铜渣合理还原熔分的工艺路线,得到如下结论:渣熔化是形成粒铁的必要条件,铁的聚合程度取决于渣铁分离熔化之前铁的渗碳质量分数.渣中SiO2的存在是渣相低熔点的根本原因,碱度改变时<span style=\"color:red\">云</span>铜渣的熔化区间会发生变化,但对熔化开始温度的影响不显著.当碱度大于0.4后,添加CaO能显著地提高云铜渣的还原性能.","authors":[{"authorName":"何鹏","id":"dbab97f5-d12b-4a0a-bad0-a959625d6185","originalAuthorName":"何鹏"},{"authorName":"张俊","id":"d83fb0b5-604e-42e2-9c21-05d815abb339","originalAuthorName":"张俊"},{"authorName":"严定鎏","id":"858533e8-e701-4864-8fb8-af36b4f5ef2f","originalAuthorName":"严定鎏"}],"doi":"10.13228/j.boyuan.issn1006-9356.20160096","fpage":"33","id":"782f7e45-0426-4cf2-b982-c59def030561","issue":"2","journal":{"abbrevTitle":"ZGYJ","coverImgSrc":"journal/img/cover/ZGYJ.jpg","id":"87","issnPpub":"1006-9356","publisherId":"ZGYJ","title":"中国冶金"},"keywords":[{"id":"ddcf7b2d-9641-4743-9350-5b22fc2aa278","keyword":"铜渣","originalKeyword":"铜渣"},{"id":"3f5d464c-f42b-4dc2-ba77-4bacbda434a6","keyword":"还原熔分","originalKeyword":"还原熔分"},{"id":"d9a3b998-0a4a-47a8-b6a4-627dfffb5032","keyword":"渗碳","originalKeyword":"渗碳"},{"id":"6a3f5d91-7e3a-4681-a996-c8999f34749a","keyword":"粒铁","originalKeyword":"粒铁"}],"language":"zh","publisherId":"zgyj201702007","title":"<span style=\"color:red\">云</span>铜铜渣还原熔分试验分析","volume":"27","year":"2017"}],"totalpage":30,"totalrecord":300}