{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"以环氧树脂E-51、甲基纳迪克酸酐、聚乙二醇为原料合成了反应型乳化剂,最佳工艺条件是酯化反应时间为3h,温度为75℃;环氧开环反应时间为5h,温度为100℃.通过相反转法制备出水性环氧树脂乳液,并调节配方得到水性环氧地坪面漆,该漆膜性能优异.","authors":[{"authorName":"<span style=\"color:red\">李</span><span style=\"color:red\">晴</span>","id":"c43e24fa-e5d4-42f9-924c-54abee7866fa","originalAuthorName":"李晴"},{"authorName":"朱殿奎","id":"3bbebdbf-1eec-4fe8-a8b9-20f49a16ee74","originalAuthorName":"朱殿奎"},{"authorName":"沈志明","id":"29bacd86-823a-46b1-9683-69b20d3474d9","originalAuthorName":"沈志明"},{"authorName":"徐磊","id":"74e6e0db-3f63-4087-b7b5-da742c3494d7","originalAuthorName":"徐磊"},{"authorName":"朱灿银","id":"e86c916e-1980-4e65-bef2-d3fcfa829e7b","originalAuthorName":"朱灿银"},{"authorName":"曹静","id":"67e749d1-c3e8-4c72-aa29-73ad90509c2a","originalAuthorName":"曹静"},{"authorName":"<span style=\"color:red\">李</span>文","id":"f13566cc-82f3-4b1f-ba20-c38bcd02da06","originalAuthorName":"李文"},{"authorName":"<span style=\"color:red\">李</span>娟","id":"305bd425-05fa-4230-bed2-80ca946a8f41","originalAuthorName":"李娟"},{"authorName":"李安宁","id":"8497c741-78eb-42c4-8d74-1b04c987ce24","originalAuthorName":"李安宁"}],"doi":"","fpage":"41","id":"cc5de67c-c2a9-4549-a4ab-e299c0a84ed5","issue":"3","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业   "},"keywords":[{"id":"203f9d11-e8f2-456d-8764-434a84d10254","keyword":"反应型乳化剂","originalKeyword":"反应型乳化剂"},{"id":"e655f527-b0a7-415e-bdad-875c355973de","keyword":"水性环氧树脂","originalKeyword":"水性环氧树脂"},{"id":"8d30dd4f-a0b3-407f-8c1f-01a20c23e57b","keyword":"地坪涂料","originalKeyword":"地坪涂料"}],"language":"zh","publisherId":"tlgy201503009","title":"水性环氧树脂乳液的制备及其应用","volume":"45","year":"2015"},{"abstractinfo":"制备了反射隔热弹性涂料,分析了涂膜厚度、颜基比、钛白粉的粒径大小及含量、空心玻璃微珠等对反射隔热弹性涂料的太阳反射比的影响,同时研究了陶瓷粉含量对半球发射率的影响.实验结果表明:当涂膜厚度为480μm,钛白粉含量为30％且粒径为100～800 nm,陶瓷粉含量为4％,空心玻璃微珠含量为10％时,可制得太阳反射比为0.891 4,半球发射率为0.89的高性能反射隔热弹性涂料.","authors":[{"authorName":"李伟","id":"c086e361-ca58-4cb3-8cec-172f13c54779","originalAuthorName":"李伟"},{"authorName":"李安宁","id":"c5cf16fb-78f1-4941-a0db-1fe889ded849","originalAuthorName":"李安宁"},{"authorName":"朱殿奎","id":"aa04acfb-59e0-47c4-a40f-c8a54c652ab1","originalAuthorName":"朱殿奎"},{"authorName":"沈志明","id":"4fbf43f7-d1d2-46d5-a121-1465cfa73482","originalAuthorName":"沈志明"},{"authorName":"<span style=\"color:red\">李</span><span style=\"color:red\">晴</span>","id":"7b43a5b4-baff-4201-8a22-3021603ff092","originalAuthorName":"李晴"},{"authorName":"<span style=\"color:red\">李</span>娟","id":"9c6e34d9-d0e6-486a-9403-6773c63faa53","originalAuthorName":"李娟"}],"doi":"","fpage":"7","id":"4a433591-5cad-4fde-92fa-43a4879006fe","issue":"5","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业   "},"keywords":[{"id":"e6b2c07e-ebe4-402d-8439-48a753be2838","keyword":"反射隔热弹性涂料","originalKeyword":"反射隔热弹性涂料"},{"id":"dcf9e2a4-62b3-41f2-88f1-75c42c7f0bc5","keyword":"太阳反射比","originalKeyword":"太阳反射比"},{"id":"cf2315b0-9622-4511-9aff-8f54b7d09d12","keyword":"陶瓷粉","originalKeyword":"陶瓷粉"}],"language":"zh","publisherId":"tlgy201505002","title":"高性能反射隔热弹性涂料的研究","volume":"45","year":"2015"},{"abstractinfo":"手性2,3-二氢呋喃衍生物是一类重要的杂环化合物,广泛存在于天然产物和生物活性分子中.它们也经常被用于手性四氢呋喃化合物的不对称合成.因此,人们发展了很多合成手性2,3-二氢呋喃化合物的方法,如有机小分子催化的多米诺迈克尔-烷基化反应、“中断的”Feist-Bénary反应或改进的 Feist-Bénary反应.此外,过渡金属催化的手性2,3-二氢呋喃的不对称合成在近些年引起了人们的极大关注. Ozawa等通过 Pd-催化2,3-二氢呋喃的动力拆分方法获得了手性2-芳基-2,3-二氢呋喃. Evans发展了一种 Sc-催化联烯硅和乙醛酸乙酯的[3+2]环加成反应合成手性2,3-二氢呋喃的方法.最近, Fu和 Tang等发展了 Cu催化烯酮和重氮化合物的[4+1]环加成反应合成手性2,3-二氢呋喃的方法.在 Nishibayashi和 van Maarseveen的开创性工作之后, Cu催化的不对称炔丙基转化反应取得了很大的进展.最近,我们发展了一类新的三齿手性 P,N,N-配体,在 Cu催化不对称炔丙基取代、脱羧炔丙基取代、[3+2]、[3+3]和[4+2]环加成反应中表现出优秀的对映和非对映选择性.其中,我们发现采用 Cu催化炔丙醇酯和β-酮酯的[3+2]环加成反应,能高对映选择性地获得手性2,3-二氢呋喃.我们设想,采用β-羰基膦酸酯代替β-酮酯,通过这种 Cu催化[3+2]环加成反应,将可以合成一类具有重要生物活性的手性膦酰化2,3-二氢呋喃化合物.基于这种设想,本文使用手性 P,N,N-配体,通过 Cu催化炔丙醇酯与β-羰基膦酸酯的不对称[3+2]环加成反应,以很好的收率和最高92% ee的对映选择性获得了一系列光学活性的膦酰化2,3-二氢呋喃化合物.我们以炔丙醇酯1a与β-羰基膦酸酯2a为标准底物,优化了反应条件,考察了配体、Cu盐、碱和反应温度等对反应收率和对映选择性的影响.我们确定了最佳的反应条件：以4b为配体,以 Cu(OTf)2为铜盐,以t-BuOK为碱,以 MeOH为溶剂,–20oC反应24 h.在此条件下,我们对β-羰基磷酸酯2的适用范围进行了考察.结果表明,各种苯基取代的β-羰膦磷酸酯均能得到很好的收率和对映选择性.苯环上取代基的空间效应对反应的对映选择性影响不大,但对反应收率影响较大,与相应3-取代或4-取代底物相比较,2-取代的底物获得的收率较低.苯环对位取代基的电子效应对反应的影响不大,给电子基或吸电子基的底物,均得到了较好的收率和对映选择性.杂环取代的底物同样适用于该反应,以90%的收率和89% ee的对映选择性获得了相应的[3+2]环加成产物.对于烷基底物,虽然反应的产率略低,但是得到了高达92% ee的产物.此外,我们对炔丙醇酯底物的适用范围也进行了考察.结果表明,该体系对于各种取代的炔丙醇酯底物均可以获得较高的收率和良好的对映选择性.总之,本文发展了一种铜催化炔丙醇酯与β-羰基膦酸酯的不对称[3+2]环加成反应的方法,成功合成了手性膦酰化2,3-二氢呋喃化合物.通过使用一个结构刚性的酮亚胺三齿 P,N,N-配体,以很好的收率和最高92% ee的对映选择性获得了一系列光学活性的膦酰化2,3-二氢呋喃化合物.","authors":[{"authorName":"陈修帅","id":"aaa76959-9b83-440b-bd0e-8301b2d7ba0f","originalAuthorName":"陈修帅"},{"authorName":"侯传金","id":"79452a7e-7472-4764-b69b-7f2de9f9c8a4","originalAuthorName":"侯传金"},{"authorName":"<span style=\"color:red\">李</span><span style=\"color:red\">晴</span>","id":"cf7caa8f-45d7-4928-b7e0-767813ac6257","originalAuthorName":"李晴"},{"authorName":"刘彦军","id":"7bbb880f-2376-45db-ac9e-6db2712a90be","originalAuthorName":"刘彦军"},{"authorName":"杨瑞丰","id":"08468e78-18b2-45fd-911f-a9cfcd9ee7d2","originalAuthorName":"杨瑞丰"},{"authorName":"胡向平","id":"bbcd7026-daf2-47d2-8e46-b8d9ff2ab1bd","originalAuthorName":"胡向平"}],"doi":"10.1016/S1872-2067(16)62488-9","fpage":"1389","id":"f43aeff7-a12b-4181-8457-450bfad579b2","issue":"8","journal":{"abbrevTitle":"CHXB","coverImgSrc":"journal/img/cover/CHXB.jpg","id":"18","issnPpub":"0253-9837","publisherId":"CHXB","title":"催化学报   "},"keywords":[{"id":"ee659bb2-9826-42a6-91fa-decdadc1ba0a","keyword":"铜","originalKeyword":"铜"},{"id":"49f33854-b76e-4932-9c88-c1be3e690097","keyword":"不对称合成","originalKeyword":"不对称合成"},{"id":"7822dd19-057c-443c-873d-b8816591ee53","keyword":"3+2环加成","originalKeyword":"3+2环加成"},{"id":"c618784b-1dc2-4947-a5a1-05d69c5251b8","keyword":"β-羰基膦酸酯","originalKeyword":"β-羰基膦酸酯"},{"id":"5ef7843b-f942-4e24-9e82-33162bdff844","keyword":"膦酰化 2,3-二氢呋喃","originalKeyword":"膦酰化 2,3-二氢呋喃"}],"language":"zh","publisherId":"cuihuaxb201608025","title":"铜催化炔丙醇酯与β-羰基膦酸酯的不对称[3+2]环加成反应合成手性膦酰化2,3-二氢呋喃","volume":"37","year":"2016"},{"abstractinfo":"将螺纹钢浸入0.8 mmol/L硅酸钠水溶液中制备了防锈膜.通过电化学测试、露天耐候试验、扫描电镜、红外光谱和耐水性试验评价了常温(25 ℃)下自然干燥的以及经过热固化处理的防锈膜的性能,考察了固化时间对防锈膜性能的影响.结果表明:在220℃固化3.5 h后的防锈膜形成了由Si—O—Si键构成的三维网状结构,膜层均匀致密,防锈期超过2个月,耐蚀性和耐水性均好于自然干燥的防锈膜.","authors":[{"authorName":"王然","id":"ed8498a0-8811-4745-bdd0-6f0ef88428a1","originalAuthorName":"王然"},{"authorName":"衣守志","id":"08c42ad1-7e24-4c02-9c9d-0d3f458f240f","originalAuthorName":"衣守志"},{"authorName":"<span style=\"color:red\">李</span><span style=\"color:red\">晴</span>","id":"0f624382-8224-4fc2-b6a9-1f1922cfe7a8","originalAuthorName":"李晴"},{"authorName":"殷嘉蔚","id":"ceb7a5b0-4af9-4816-bca5-eebd869ac997","originalAuthorName":"殷嘉蔚"},{"authorName":"肖早早","id":"5d930360-66da-48eb-80ca-7fe909c6c047","originalAuthorName":"肖早早"}],"doi":"","fpage":"1056","id":"76d88487-3028-472d-b42f-120aca75384a","issue":"20","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰   "},"keywords":[{"id":"e50381f1-4fe9-4842-9a0e-e000a48ba5ea","keyword":"螺纹钢","originalKeyword":"螺纹钢"},{"id":"409c5691-8e5f-4920-9420-2d2cad8d9ad5","keyword":"硅酸钠","originalKeyword":"硅酸钠"},{"id":"95321e0b-b05b-40c8-91e0-d4110891f6d4","keyword":"防锈膜","originalKeyword":"防锈膜"},{"id":"d089e4f7-e13c-41b7-a92f-fb37ab8f763c","keyword":"热固化","originalKeyword":"热固化"},{"id":"9f7f5884-6794-4f7c-90f9-a492eaed51b3","keyword":"电化学","originalKeyword":"电化学"},{"id":"7fa0ba0b-09c4-4d5b-a3e6-81978e6035d5","keyword":"耐候性","originalKeyword":"耐候性"}],"language":"zh","publisherId":"ddyts201620002","title":"热固化对螺纹钢上硅酸钠防锈膜性能的影响","volume":"35","year":"2016"},{"abstractinfo":"采用六亚甲基二异氰酸酯(HDI)作为桥接剂在玻璃鳞片表面接枝包覆端羧基液态丁<span style=\"color:red\">晴</span>橡胶(CTBN),制备GF-HDI-CTBN三元复合材料,并通过FT-IR、SEM、EDS、TGA等手段对复合材料的结构、形貌、表面元素和接枝率等进行表征.以复合材料为填料配制防腐涂料,测试其对涂料性能的影响.结果表明,以HDI为桥接剂,在玻璃鳞片表面成功接枝包覆上了端羧基液态丁<span style=\"color:red\">晴</span>橡胶,端羧基液态丁<span style=\"color:red\">晴</span>橡胶呈密集肌纤维状,均匀包覆在玻璃鳞片表面;所制备的端羧基液态丁<span style=\"color:red\">晴</span>橡胶改性玻璃鳞片防腐涂料的拉伸强度、断裂伸长率、附着力和耐冲击性都得到了明显的提高,且当GF-HDI-CTBN添加量为20％时改善最为明显.","authors":[{"authorName":"宋玉强","id":"3dc7bc68-037d-4df4-bf5d-d6ce828bab6f","originalAuthorName":"宋玉强"},{"authorName":"沈以赴","id":"4603438e-c44c-4b08-b354-b11310334440","originalAuthorName":"沈以赴"},{"authorName":"陈凯锋","id":"e5c278cd-4967-4c30-8c8c-0d1bdc989838","originalAuthorName":"陈凯锋"},{"authorName":"许超","id":"776800ca-650a-42f5-9760-722836a89e9e","originalAuthorName":"许超"},{"authorName":"王晶晶","id":"ab3559c1-029a-464a-bd96-41d1e87cb5b8","originalAuthorName":"王晶晶"}],"doi":"","fpage":"94","id":"44889c3f-25af-4823-a664-6dbd9a58d3da","issue":"3","journal":{"abbrevTitle":"CLKFYYY","coverImgSrc":"journal/img/cover/CLKFYYY.jpg","id":"10","issnPpub":"1003-1545","publisherId":"CLKFYYY","title":"材料开发与应用"},"keywords":[{"id":"ee018f48-780c-40b8-ae0a-f59feeb1a2d6","keyword":"端羧基液态丁<span style=\"color:red\">晴</span>橡胶","originalKeyword":"端羧基液态丁晴橡胶"},{"id":"b1a6d3a7-fc86-40b1-83ea-eb2994868c92","keyword":"玻璃鳞片","originalKeyword":"玻璃鳞片"},{"id":"1df7257f-a770-4b35-bfe5-90516229ed61","keyword":"涂料","originalKeyword":"涂料"},{"id":"9fa36c6d-5dc3-4e69-93a0-e325d399d621","keyword":"接枝改性","originalKeyword":"接枝改性"}],"language":"zh","publisherId":"clkfyyy201603018","title":"端羧基液态丁<span style=\"color:red\">晴</span>橡胶/玻璃鳞片复合材料的制备与表征","volume":"31","year":"2016"},{"abstractinfo":"<正> 一、为纪念<span style=\"color:red\">李</span>薰创办和主编《金属学报》,继承并发扬他毕生致力于科技进步的业绩,特设立《金属学报》纪念<span style=\"color:red\">李</span>薰奖金基金.二、基金来源是乐于赞助的科研单位、高等院校、企业、团体的捐赠.基金属于专款,全部存入银行,每年支取利息,直接用于奖励.","authors":[],"categoryName":"|","doi":"","fpage":"2","id":"53b5b4af-4a26-4ab3-9944-a079f1cdb6c6","issue":"2","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[],"language":"zh","publisherId":"0412-1961_1985_2_2","title":"《金属学报》纪念<span style=\"color:red\">李</span>薰奖金基金简章","volume":"21","year":"1985"},{"abstractinfo":"<正> 1983年3月20日凌晨,《金属学报》的创刊人、主编<span style=\"color:red\">李</span>薰同志和我们永别了。 <span style=\"color:red\">李</span>薰同志1913年11月20日出生于湖南省邵阳县。1937年以优异成绩通过湖南省试,留学英国Sheffield大学,先后获得哲学博士和冶金学的科学博士学位。1950年受中国科学院郭沫若院长聘,翌年毅然回归祖国。历任中国科学院金属研究所所长,中国科学院","authors":[],"categoryName":"|","doi":"","fpage":"1","id":"e58ce4aa-af81-477f-8509-f13a621fe343","issue":"2","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[],"language":"zh","publisherId":"0412-1961_1983_2_14","title":"深切悼念本刊创刊人、主编<span style=\"color:red\">李</span>薰同志","volume":"19","year":"1983"},{"abstractinfo":"防治水是矿山建设施工的重要环节.南<span style=\"color:red\">李</span>庄矿属于水文地质条件复杂的大水岩溶矿山,介绍了主井掘进-129 m水平突水及治水过程,在查清该矿区水文地质条件及矿井突水要因的基础上,为综合防治竖井掘进期间通过特殊地质构造段突水,提出相应的主井掘进帷幕注浆防治水技术及措施,并在掘进工程中收到了良好的应用效果,对类似特殊条件下的矿山井巷掘进工程具有借鉴意义.","authors":[{"authorName":"董华兴","id":"c08faef8-222f-4269-ab57-068e213c04a0","originalAuthorName":"董华兴"},{"authorName":"郑翠敏","id":"71818941-893c-450e-8900-6d9f7dc6d4f4","originalAuthorName":"郑翠敏"},{"authorName":"董凤霞","id":"ce559c6e-5477-4acc-96d6-55cc93294757","originalAuthorName":"董凤霞"},{"authorName":"韩建国","id":"d72c3f8a-9086-4000-8209-5e6a1f371d1d","originalAuthorName":"韩建国"}],"doi":"10.11792/hj20130209","fpage":"35","id":"50da3555-9182-4c83-b8b8-7c218b723d08","issue":"2","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"c8ee1711-e9ee-4c00-a471-1354d308bfe1","keyword":"大水矿山","originalKeyword":"大水矿山"},{"id":"5da58d6c-dff5-4998-b645-b63ba8ec37c0","keyword":"主井掘进","originalKeyword":"主井掘进"},{"id":"a29b56b2-06f6-49a2-9412-0a6cbd37c8f5","keyword":"特殊地质构造","originalKeyword":"特殊地质构造"},{"id":"49c4c65b-3993-4060-b81d-5caf117fa377","keyword":"突水","originalKeyword":"突水"},{"id":"5f22c680-f6b2-4312-8b46-fe823c71eddb","keyword":"防治","originalKeyword":"防治"}],"language":"zh","publisherId":"huangj201302009","title":"南<span style=\"color:red\">李</span>庄矿主井施工突水防治技术","volume":"34","year":"2013"},{"abstractinfo":"解析设计控制器,通过配置相应的<span style=\"color:red\">李</span>雅谱诺夫指数,使统一混沌系统趋于预期点.由于受控后系统<span style=\"color:red\">李</span>雅谱诺夫指数具有先知性,因此,我们可以根据需要改变<span style=\"color:red\">李</span>雅谱诺夫指数的大小来控制系统收敛速度.设计还表明,受控的统一混沌系统的收敛情况与参数无关.","authors":[{"authorName":"<span style=\"color:red\">李</span>国辉","id":"a87d9208-0f6c-4189-b9bd-ebc278e566d3","originalAuthorName":"李国辉"},{"authorName":"雷云逸","id":"14e8001b-cd35-4319-b4db-b18f74687765","originalAuthorName":"雷云逸"},{"authorName":"徐得名","id":"d483ede1-f372-4f69-8f66-3292818382c5","originalAuthorName":"徐得名"},{"authorName":"周世平","id":"994ece4e-2a84-4ceb-84b2-b905c11a2be4","originalAuthorName":"周世平"}],"doi":"10.3969/j.issn.1007-5461.2004.01.010","fpage":"39","id":"2ac637e0-2c08-47c3-9516-29ecd43ace59","issue":"1","journal":{"abbrevTitle":"LZDZXB","coverImgSrc":"journal/img/cover/LZDZXB.jpg","id":"53","issnPpub":"1007-5461","publisherId":"LZDZXB","title":"量子电子学报   "},"keywords":[{"id":"a819811e-bd0b-4552-8929-81a5ed93e840","keyword":"量子光学","originalKeyword":"量子光学"},{"id":"a6435ee1-87f2-4c1d-af2d-1cb48ef24c3b","keyword":"统一混沌系统","originalKeyword":"统一混沌系统"},{"id":"831db573-677f-47fe-8d3a-96cbffc7453f","keyword":"<span style=\"color:red\">李</span>雅谱诺夫指数","originalKeyword":"李雅谱诺夫指数"},{"id":"1c6a112f-e491-4f10-b9bc-4df3d8d3b045","keyword":"控制混沌","originalKeyword":"控制混沌"},{"id":"c53814f3-b4a5-472c-9bf6-e936ec1bab22","keyword":"Jacobi矩阵","originalKeyword":"Jacobi矩阵"}],"language":"zh","publisherId":"lzdzxb200401010","title":"用<span style=\"color:red\">李</span>雅谱诺夫指数配置法控制统一混沌系统","volume":"21","year":"2004"},{"abstractinfo":"生物表面活性剂鼠<span style=\"color:red\">李</span>糖脂是微生物在一定条件下产生的次级代谢产物，其分子具有极性亲水基团和非极性亲油基团结构，通常表现出很高的表面活性和界面优先分配能力。可靠的分离提纯方法和成分鉴定手段是鼠<span style=\"color:red\">李</span>糖脂生产工艺成功的重要保证。实验通过好氧发酵培养铜绿假单胞菌CCTCCAB93066、酸沉降分离得到鼠<span style=\"color:red\">李</span>糖脂后，利用柱色谱提纯技术得到纯化的鼠<span style=\"color:red\">李</span>糖脂的单糖脂和二糖脂，最后采用高效液相色谱-质谱联用法进行成分鉴定。结果显示这两种鼠<span style=\"color:red\">李</span>糖脂均含有3种主要成分，其中单糖脂的主要成分为RhaC10C10、RhaC10C12-H2、RhaC10C12，二糖脂的主要成分为Rha2C10C10、Rha2C10C12-H2、Rha2C10C12。该研究结果表明，铜绿假单胞菌CCTCCAB93066是一种良好的鼠<span style=\"color:red\">李</span>糖脂产生菌；酸沉降-柱色谱技术可以用于鼠<span style=\"color:red\">李</span>糖脂的深度提纯，且有较好的效果；而高效液相色谱-质谱联用技术对鼠<span style=\"color:red\">李</span>糖脂成分鉴定具有灵敏度高和准确性好等优点，是一种较为可靠的检测方法。","authors":[{"authorName":"刘洋","id":"d92d9b1c-f72e-4fcf-bbb0-17ff46f70d06","originalAuthorName":"刘洋"},{"authorName":"钟华","id":"af1417aa-bf0d-49f8-9eb0-6b2c8a4caeb2","originalAuthorName":"钟华"},{"authorName":"刘智峰","id":"a85b6803-7235-4efb-aaf3-48d0169a372a","originalAuthorName":"刘智峰"},{"authorName":"蒋勇兵","id":"669bcaa0-edb9-4002-bb97-0e076d921aa7","originalAuthorName":"蒋勇兵"},{"authorName":"谈菲","id":"7a68e398-ba8e-4aad-9860-95e4ab4b8688","originalAuthorName":"谈菲"},{"authorName":"曾光明","id":"883e9227-a4f9-465b-9e06-8bf596ba6343","originalAuthorName":"曾光明"},{"authorName":"赖明勇","id":"5ac36d12-f1e6-4dc2-b5d9-e0755b6e4af4","originalAuthorName":"赖明勇"},{"authorName":"何益斌","id":"190cde84-4d27-458e-95f6-d82465b24718","originalAuthorName":"何益斌"}],"doi":"10.3724/SP.J.1123.2013.10026","fpage":"248","id":"8925555f-3d9f-488a-a5bf-6f13ce780e02","issue":"3","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"3a2adc8e-db6b-4699-86c7-84cccc1b8846","keyword":"酸沉降","originalKeyword":"酸沉降"},{"id":"84e0a9e7-ace6-49f3-b53c-88cf42990f69","keyword":"柱色谱","originalKeyword":"柱色谱"},{"id":"11e5b6d7-1de2-4c9b-b6b8-a2ac9450e7e2","keyword":"高效液相色谱-质谱联用","originalKeyword":"高效液相色谱-质谱联用"},{"id":"cb3bce2d-ee35-4f13-ad56-f29477f22bed","keyword":"鼠<span style=\"color:red\">李</span>糖脂","originalKeyword":"鼠李糖脂"},{"id":"534c9e67-8a9a-4802-b1e5-efb96c8e17f3","keyword":"铜绿假单胞菌","originalKeyword":"铜绿假单胞菌"},{"id":"fb340070-5f7a-4e09-b97b-1d5410d26af2","keyword":"生物表面活性剂","originalKeyword":"生物表面活性剂"}],"language":"zh","publisherId":"sp201403007","title":"生物表面活性剂鼠<span style=\"color:red\">李</span>糖脂的纯化与表征","volume":"","year":"2014"}],"totalpage":11,"totalrecord":107}