{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"为解决无机类富勒烯纳米化合物的制备过程中存在的技术问题,本文以二硫化钼和二硫化钨为主要原料,采用了剥离-重新堆垛-结构控制这一技术方法,用正丁基锂将上述二硫化物剥离成单层,通过掺杂将金属锰离子引入反应体系中,以将单层二硫化物重新堆垛起来,并进行结构控制.XRD、TEM、HRTEM结果表明,应用上述方法制备出了真空管状多元金属二硫化物纳米化合物;纳米管为多壁管,其微细结构具双层结构特征;并探讨了其形成机理.","authors":[{"authorName":"李国华","id":"c7717bb3-7c78-41b7-9269-2d7e7e9b20b1","originalAuthorName":"李国华"},{"authorName":"曾跃武","id":"3b4cdb75-3e30-4b05-9601-056a1ab14e99","originalAuthorName":"曾跃武"},{"authorName":"<span style=\"color:red\">宋</span><span style=\"color:red\">旭</span><span style=\"color:red\">春</span>","id":"09892fc3-372b-411c-903f-57653ecb6dd3","originalAuthorName":"宋旭春"},{"authorName":"夏军保","id":"fcbf1bc7-222d-4c2a-858a-45be3a5293a1","originalAuthorName":"夏军保"},{"authorName":"陈卫祥","id":"d2de63e4-2787-4bc8-8d9a-c81a32f27efb","originalAuthorName":"陈卫祥"},{"authorName":"徐铸德","id":"f1f8ad42-25b5-4246-a452-69d6e3ea32d8","originalAuthorName":"徐铸德"}],"categoryName":"|","doi":"","fpage":"481","id":"0dcd110a-4ec5-4014-8db8-f14321842973","issue":"3","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"c7bf3cd8-fc3b-4099-8bf6-74ff4224d345","keyword":"多元金属二硫化物","originalKeyword":"多元金属二硫化物"},{"id":"709df5bc-2d9b-4ead-bc8b-703f7b5f4f47","keyword":" exfoliating-restacking- structure controlling","originalKeyword":" exfoliating-restacking- structure controlling"},{"id":"506980ef-0835-42e4-a85a-02f33eb2d92e","keyword":" nanotube","originalKeyword":" nanotube"},{"id":"add60ba4-efe3-4959-90f1-83f4662afda1","keyword":" structural characteristic","originalKeyword":" structural characteristic"}],"language":"zh","publisherId":"1000-324X_2004_3_3","title":"多元金属二硫化物纳米管的制备与结构特征","volume":"19","year":"2004"},{"abstractinfo":"采用无机盐辅助水热法选择调控合成了WO3纳米颗粒和纳米线.通过SEM,TEM,EDX和XRD等手段对产物进行了表征.研究了形貌和尺寸对WO3的光致发光性能的影响,并探讨了形貌和尺寸对WO3光致发光性能影响的机制.","authors":[{"authorName":"<span style=\"color:red\">宋</span><span style=\"color:red\">旭</span><span style=\"color:red\">春</span>","id":"f8cea975-ee88-4a10-83f0-1fbe2f7d111a","originalAuthorName":"宋旭春"},{"authorName":"王芸","id":"de69c348-53c6-4a6f-9a6d-dd5c4671f9a6","originalAuthorName":"王芸"},{"authorName":"林深","id":"cb785f74-9918-4cf7-9937-88e404d62fde","originalAuthorName":"林深"},{"authorName":"杨娥","id":"fb04f994-6664-4ae7-a98b-05c930c3014a","originalAuthorName":"杨娥"}],"doi":"","fpage":"9","id":"55613221-c1d8-4e02-8db3-c42ff3c42829","issue":"z3","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"3a84ca40-7ef2-477b-ae5d-ed6f52ea900e","keyword":"氧化钨","originalKeyword":"氧化钨"},{"id":"02bd86b6-e5b7-42e8-bc79-fb962ec9691c","keyword":"水热","originalKeyword":"水热"},{"id":"e25b53a2-d4c5-4e10-a03f-146ebcb294ed","keyword":"光致发光","originalKeyword":"光致发光"}],"language":"zh","publisherId":"xyjsclygc2007z3003","title":"氧化钨纳米颗粒和纳米线的选择合成及光致发光研究","volume":"36","year":"2007"},{"abstractinfo":"采用简单的沉淀法制备了WS<SUB>3</SUB>前驱物,在高温下WS<SUB>3</SUB>前驱物与氢气反应在聚乙二醇做分散剂作用得到了具有嵌套球形层状封闭结构WS<SUB>2</SUB>纳米颗粒.通过高分辨透射电镜(HRTEM)、粉末X射线衍射(XRD)和X射线能量散射谱(EDS)等方法对其形貌、结构和成分进行了表征,对其形成机理进行了探讨.","authors":[{"authorName":"郑遗凡","id":"c7421120-1d1f-4bba-8bdf-b859ef4f0cab","originalAuthorName":"郑遗凡"},{"authorName":"<span style=\"color:red\">宋</span><span style=\"color:red\">旭</span><span style=\"color:red\">春</span>","id":"87192a70-e7ca-4dd1-9049-16fbd57e66d8","originalAuthorName":"宋旭春"},{"authorName":"刘波","id":"0e1aa9cd-28e5-486c-98f9-688d1683fd0c","originalAuthorName":"刘波"},{"authorName":"韩贵","id":"6be12229-a72a-4a7a-89d3-a5641fbe0fe4","originalAuthorName":"韩贵"},{"authorName":"徐铸德","id":"5d540633-ade1-43e2-9668-5374db75ad60","originalAuthorName":"徐铸德"}],"categoryName":"|","doi":"","fpage":"653","id":"77035954-7c78-4e6b-9de0-265a07621d3f","issue":"3","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"fd67123c-ce49-4e93-ba39-754a63935ed2","keyword":"无机类富勒烯","originalKeyword":"无机类富勒烯"},{"id":"2318bf66-7e88-423c-b76a-91f543db3776","keyword":" WS<SUB>2</SUB>","originalKeyword":" WS<SUB>2</SUB>"},{"id":"eddfe99d-db24-41ba-9614-15ad0be0aa73","keyword":" precipitation","originalKeyword":" precipitation"}],"language":"zh","publisherId":"1000-324X_2004_3_41","title":"嵌套球形层状封闭结构纳米二硫化钨的合成与机理探讨","volume":"19","year":"2004"},{"abstractinfo":"采用简单的水热法合成了Dy(OH)3纳米棒和纳米带,通过SEM、TEM、EDS和XRD等手段对产物进行了表征.研究了pH值和水热温度对Dy(OH)3纳米晶形貌的影响.实验发现,调节水热温度可以控制Dy(OH)3纳米棒的形貌,而Dy(OH)3纳米带的形成与pH值密切相关.这为合成其它稀土化合物一维纳米材料提供了一个新的途径.","authors":[{"authorName":"<span style=\"color:red\">宋</span><span style=\"color:red\">旭</span><span style=\"color:red\">春</span>","id":"78cb2b2d-2440-426c-b82c-28cbf3116b12","originalAuthorName":"宋旭春"},{"authorName":"杨娥","id":"09fc276e-0c9e-41c5-8a22-bb0dc0d00d94","originalAuthorName":"杨娥"},{"authorName":"郑遗凡","id":"2ef9f7c9-f6a2-40c7-831a-314ecedfa298","originalAuthorName":"郑遗凡"},{"authorName":"王芸","id":"b54bf30e-889a-4eb1-8838-c261f3fe0fc8","originalAuthorName":"王芸"}],"doi":"","fpage":"670","id":"8265f55f-84be-4f33-a771-8428cf163f9a","issue":"z3","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"0f33ccda-ccbf-45d3-a909-ed6de458f0cf","keyword":"水热","originalKeyword":"水热"},{"id":"f87545b4-24d8-4089-85aa-03bf03e74e4b","keyword":"Dy(OH)3","originalKeyword":"Dy(OH)3"},{"id":"4a0d4d9b-e2ee-40dd-9de4-888bf055fd8f","keyword":"纳米棒","originalKeyword":"纳米棒"},{"id":"45a99b7a-ca56-4bf0-8c92-46fc066eb76c","keyword":"纳米带","originalKeyword":"纳米带"}],"language":"zh","publisherId":"xyjsclygc2007z3161","title":"水热合成Dy(OH)3纳米棒和纳米带","volume":"36","year":"2007"},{"abstractinfo":"<FONT face=Verdana>采用Na<SUB>3</SUB>PO<SUB>4</SUB>辅助水热法合成了单晶WO<SUB>3</SUB>纳米棒, 通过SEM、TEM、EDX和XRD等手段对产物进行了表征. 研究了其他无机盐(Na<SUB>2</SUB>SO<SUB>4</SUB>、NaNO<SUB>3</SUB>和NaCl)对WO<SUB>3</SUB>纳米晶形貌的影响. 实验发现 WO<SUB>3</SUB>纳米棒的形成与添加Na<SUB>3</SUB>PO<SUB>4</SUB>密切相关, 当Na<SUB>3</SUB>PO4的添加量达到50g时, 在这个反应体系中可以制得质量较好的WO<SUB>3</SUB>纳米棒. </FONT>\n<FONT face=Verdana></FONT>","authors":[{"authorName":"<span style=\"color:red\">宋</span><span style=\"color:red\">旭</span><span style=\"color:red\">春</span>","id":"da3eee2f-e1dc-4ec4-aa38-3a772f8540b5","originalAuthorName":"宋旭春"},{"authorName":"郑遗凡","id":"76bf79ef-f5b0-4b23-866e-edf9d70dc9f4","originalAuthorName":"郑遗凡"},{"authorName":"王芸","id":"3dc87a41-efbe-4ccb-aba8-e8c96cee0e8e","originalAuthorName":"王芸"},{"authorName":"曹广胜","id":"e8439f02-a8a7-4903-8fcd-2eeab794d370","originalAuthorName":"曹广胜"},{"authorName":"殷好勇","id":"00496476-8d87-4874-b212-54cde27c4342","originalAuthorName":"殷好勇"}],"categoryName":"|","doi":"10.3724/SP.J.1077.2006.01472","fpage":"1472","id":"9e1e3430-190b-480a-b48b-b63fdb6ca930","issue":"6","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"e348504c-ecec-44cf-a6a6-cbe696b60bd7","keyword":"水热","originalKeyword":"水热"},{"id":"0d9a1b96-fbf4-4ead-a4cb-b641f0b9c3ca","keyword":" WO3","originalKeyword":" WO3"},{"id":"ccee2d49-10fc-4c59-95a3-2ce6108cdd58","keyword":" nanorod","originalKeyword":" nanorod"}],"language":"zh","publisherId":"1000-324X_2006_6_7","title":"Na<SUB>3</SUB>PO<SUB>4</SUB>辅助水热合成WO<SUB>3</SUB>纳米棒","volume":"21","year":"2006"},{"abstractinfo":"利用HCI与掺入不同量(NH<SUB>4</SUB>)<SUB>6</SUB>Mo<SUB>7</SUB>O<SUB>24</SUB>·4H<SUB>2</SUB>O的Na<SUB>2</SUB>WO<SUB>4</SUB>溶液反应生成的掺杂钼的钨酸沉淀作为前驱体,通过简单的水热方法,合成了过渡元素钼掺杂氧化钨纳米棒,通过XRD、SEM、EDS、TEM和PL等手段对产物进行了表征.研究表明,随着钼的掺杂量的增加,氧化钨纳米棒的尺寸逐渐减小,并且氧化钨纳米棒的荧光发射峰强度也逐渐减弱.","authors":[{"authorName":"曹广胜","id":"c8f18cde-f416-4674-a6b9-6f1ac5cba970","originalAuthorName":"曹广胜"},{"authorName":"俞庆森","id":"77e76f6f-72c0-4202-ab80-3e09ec999de5","originalAuthorName":"俞庆森"},{"authorName":"董喜贵","id":"f278bd55-99b0-4d8f-b2b6-ff9ae5e1edc7","originalAuthorName":"董喜贵"},{"authorName":"<span style=\"color:red\">宋</span><span style=\"color:red\">旭</span><span style=\"color:red\">春</span>","id":"45391489-1f01-4ba3-ab4a-78f2a83694c6","originalAuthorName":"宋旭春"},{"authorName":"谭非","id":"d73b680f-a53e-4a75-af24-5b480a488b10","originalAuthorName":"谭非"}],"categoryName":"|","doi":"","fpage":"815","id":"ac3befed-5490-4b9e-815b-8cc56aac53c3","issue":"4","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"e9baf2a6-9c74-49fd-a17c-3ed3a8e04542","keyword":"氧化钨","originalKeyword":"氧化钨"},{"id":"c4de7e18-bf58-4fe6-b6e8-6e14b1d488aa","keyword":" molybdenum","originalKeyword":" molybdenum"},{"id":"629725f9-29ec-4eff-86fc-236568e457df","keyword":" doping","originalKeyword":" doping"},{"id":"3f08225d-0e28-4da9-966a-7f7f0f08c08c","keyword":" nanorod","originalKeyword":" nanorod"}],"language":"zh","publisherId":"1000-324X_2005_4_2","title":"过渡元素钼掺杂氧化钨纳米棒的合成","volume":"20","year":"2005"},{"abstractinfo":"采用简单的沉淀法制备了WS3前驱物,在高温下WS3前驱物与氢气反应在聚乙二醇做分散剂作用得到了具有嵌套球形层状封闭结构WS2纳米颗粒.通过高分辨透射电镜(HRTEM)、粉末X射线衍射(XRD)和X射线能量散射谱(EDS)等方法对其形貌、结构和成分进行了表征,对其形成机理进行了探讨.","authors":[{"authorName":"郑遗凡","id":"bd243b59-9eac-4bdc-8182-e134f4d0ae37","originalAuthorName":"郑遗凡"},{"authorName":"<span style=\"color:red\">宋</span><span style=\"color:red\">旭</span><span style=\"color:red\">春</span>","id":"6a292fa4-5b8c-45d8-b9e4-63034972bd32","originalAuthorName":"宋旭春"},{"authorName":"刘波","id":"fc0f848b-9702-45d3-843f-21930bd6e15e","originalAuthorName":"刘波"},{"authorName":"韩贵","id":"f25f52b9-6f7c-4d62-a2ec-2885cab987ce","originalAuthorName":"韩贵"},{"authorName":"徐铸德","id":"3ed3a802-2881-4d77-bccf-26b2df94d9df","originalAuthorName":"徐铸德"}],"doi":"10.3321/j.issn:1000-324X.2004.03.034","fpage":"653","id":"eb4ec1cf-feff-4260-bfde-0bd08edc9c93","issue":"3","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"4625577f-68f0-4d58-b99f-f99b9560a91a","keyword":"无机类富勒烯","originalKeyword":"无机类富勒烯"},{"id":"a2160d9c-6397-4815-bc94-b11f8173e201","keyword":"二硫化钨","originalKeyword":"二硫化钨"},{"id":"3bf0d2ec-a481-4094-a5d6-cad594bb1fc4","keyword":"纳米","originalKeyword":"纳米"},{"id":"c66c6758-5c2b-426d-8869-257e027516ae","keyword":"沉淀法","originalKeyword":"沉淀法"}],"language":"zh","publisherId":"wjclxb200403034","title":"嵌套球形层状封闭结构纳米二硫化钨的合成与机理探讨","volume":"19","year":"2004"},{"abstractinfo":"为解决无机类富勒烯纳米化合物的制备过程中存在的技术问题,本文以二硫化钼和二硫化钨为主要原料,采用了剥离-重新堆垛-结构控制这一技术方法,用正丁基锂将上述二硫化物剥离成单层,通过掺杂将金属锰离子引入反应体系中,以将单层二硫化物重新堆垛起来,并进行结构控制.XRD、TEM、HRTEM结果表明,应用上述方法制备出了真空管状多元金属二硫化物纳米化合物;纳米管为多壁管,其微细结构具双层结构特征;并探讨了其形成机理.","authors":[{"authorName":"李国华","id":"f67f880d-39f4-475d-81a9-e14e013ed839","originalAuthorName":"李国华"},{"authorName":"曾跃武","id":"c27e025f-d1ce-4411-a1fc-c8e56f65016e","originalAuthorName":"曾跃武"},{"authorName":"<span style=\"color:red\">宋</span><span style=\"color:red\">旭</span><span style=\"color:red\">春</span>","id":"cb3efa11-5653-4560-92b5-a0b9acf975e3","originalAuthorName":"宋旭春"},{"authorName":"夏军保","id":"43813c3e-0316-417b-af46-fea9376f1526","originalAuthorName":"夏军保"},{"authorName":"陈卫祥","id":"f736b98c-8d63-41b1-8163-79d2cee2ee0b","originalAuthorName":"陈卫祥"},{"authorName":"徐铸德","id":"7a485785-9dcb-49db-a3d7-12f13802dae4","originalAuthorName":"徐铸德"}],"doi":"10.3321/j.issn:1000-324X.2004.03.006","fpage":"481","id":"ee7427e3-be7d-43fb-bc10-59dbcef29f30","issue":"3","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"eafa293d-86e4-4534-9215-78587ec8a61b","keyword":"多元金属二硫化物","originalKeyword":"多元金属二硫化物"},{"id":"4ccb44c0-3011-4561-87d1-05b4db331b76","keyword":"剥离-重新堆垛-结构控制","originalKeyword":"剥离-重新堆垛-结构控制"},{"id":"2cf9b629-1c05-462e-9c4f-a9f883ac6b05","keyword":"纳米管","originalKeyword":"纳米管"},{"id":"80b3b651-26da-4a48-aa10-2ef1890a1b53","keyword":"结构特征","originalKeyword":"结构特征"}],"language":"zh","publisherId":"wjclxb200403006","title":"多元金属二硫化物纳米管的制备与结构特征","volume":"19","year":"2004"},{"abstractinfo":"利用HCl与掺入不同量(NH4)6Mo7O24.4H2O的Na2WO4溶液反应生成的掺杂钼的钨酸沉淀作为前驱体,通过简单的水热方法,合成了过渡元素钼掺杂氧化钨纳米棒,通过XRD、SEM、EDS、TEM和PL等手段对产物进行了表征.研究表明,随着钼的掺杂量的增加,氧化钨纳米棒的尺寸逐渐减小,并且氧化钨纳米棒的荧光发射峰强度也逐渐减弱.","authors":[{"authorName":"曹广胜","id":"0ce61157-6bfb-4085-ad2e-0cf425608e77","originalAuthorName":"曹广胜"},{"authorName":"俞庆森","id":"1d92ce95-6c0b-40b0-90a9-a6c9ebafdc67","originalAuthorName":"俞庆森"},{"authorName":"董喜贵","id":"c431eeed-6ce5-46ac-a6ed-299aba0b9746","originalAuthorName":"董喜贵"},{"authorName":"<span style=\"color:red\">宋</span><span style=\"color:red\">旭</span><span style=\"color:red\">春</span>","id":"4e42665c-d97f-4b5e-852f-e750faeef9e2","originalAuthorName":"宋旭春"},{"authorName":"谭非","id":"2bda46f2-7789-4107-82b0-d8d93d083ab5","originalAuthorName":"谭非"}],"doi":"10.3321/j.issn:1000-324X.2005.04.008","fpage":"815","id":"62b55ebe-5ebf-4e64-b9fb-5e23ad495e4c","issue":"4","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"31c72cb4-3f75-487c-97c6-bb9f3a77dedb","keyword":"氧化钨","originalKeyword":"氧化钨"},{"id":"078c4e98-98c4-4eb1-a930-661b4ebae127","keyword":"钼","originalKeyword":"钼"},{"id":"5b676736-9605-454e-a7d4-797ea1ff865d","keyword":"掺杂","originalKeyword":"掺杂"},{"id":"90300fad-e305-4bde-a676-9801161a5f48","keyword":"纳米棒","originalKeyword":"纳米棒"}],"language":"zh","publisherId":"wjclxb200504008","title":"过渡元素钼掺杂氧化钨纳米棒的合成","volume":"20","year":"2005"},{"abstractinfo":"采用Na3PO4辅助水热法合成了单晶WO3纳米棒,通过SEM、TEM、EDX和XRD等手段对产物进行了表征.研究了其他无机盐(Na2SO4、NaNO3和NaCl)对WO3纳米晶形貌的影响.实验发现WO3纳米棒的形成与添加Na3PO4密切相关,当Na3PO4的添加量达到50g时,在这个反应体系中可以制得质量较好的WO3纳米棒.","authors":[{"authorName":"<span style=\"color:red\">宋</span><span style=\"color:red\">旭</span><span style=\"color:red\">春</span>","id":"003a268e-706d-47c9-bf30-752957f636d4","originalAuthorName":"宋旭春"},{"authorName":"郑遗凡","id":"c878d940-879d-4ccd-8e68-149b2202163b","originalAuthorName":"郑遗凡"},{"authorName":"王芸","id":"4d69b67a-4b97-4cfa-a984-917753e2b3b2","originalAuthorName":"王芸"},{"authorName":"曹广胜","id":"be9cdfb9-8053-46dd-a1d0-c2a42ba09cd9","originalAuthorName":"曹广胜"},{"authorName":"殷好勇","id":"ef95c470-264d-42b2-b5f0-5a8d3bd263c1","originalAuthorName":"殷好勇"}],"doi":"10.3321/j.issn:1000-324X.2006.06.031","fpage":"1472","id":"24c9d430-abf6-44d1-8c0f-93c1451e929f","issue":"6","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"0bc83a9f-9d0b-4128-8780-36b90843f1b6","keyword":"水热","originalKeyword":"水热"},{"id":"9a236718-ae88-441b-9b09-0fead58a80fb","keyword":"WO3","originalKeyword":"WO3"},{"id":"cb731808-e5be-4930-9cc6-73cf1f97aced","keyword":"纳米棒","originalKeyword":"纳米棒"}],"language":"zh","publisherId":"wjclxb200606031","title":"Na3PO4辅助水热合成WO3纳米棒","volume":"21","year":"2006"}],"totalpage":6,"totalrecord":52}