{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"在0.02mol/L H2SO4-4.0%乙醇介质中及紫外光照射条件下,钼同多酸光还原生成钼多蓝(λmax＝760nm);于相同条件,有PVA存在,钼多蓝和RDB反应,生成稳定的红紫色缔合物,最佳条件:在0.02mol/L H2SO4-2.0×10-5mol/L RDB-0.05%PVA-4.0%乙醇介质中及光照10min.钼浓度在1.0-7～1.0×10-5mol/L范围内与吸光度呈线性关系,据此建立了一个测定钢中微量钼的<span style=\"color:red\">光化学分析</span>新方法.","authors":[{"authorName":"吴群娣","id":"1f71da9f-fe53-4988-973c-ca8a3f2e5de3","originalAuthorName":"吴群娣"},{"authorName":"王盛棉","id":"9dbba4e8-ccdc-49e0-8719-3e84185a4057","originalAuthorName":"王盛棉"},{"authorName":"蒋治良","id":"647eb953-c17f-46a6-9f98-a5a9c94f4ebc","originalAuthorName":"蒋治良"}],"doi":"10.3969/j.issn.1000-7571.2000.01.002","fpage":"4","id":"2f641806-9a58-4d3d-bba3-c60e888b362c","issue":"1","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   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style=\"color:red\">化学分析</span>法是除气相色谱法以外的另一种简便、实用、准确的方法.","authors":[{"authorName":"苏春海","id":"445c1d16-26a9-4e7d-a943-ee5896e0da1d","originalAuthorName":"苏春海"}],"doi":"10.3969/j.issn.0253-4312.2002.03.016","fpage":"40","id":"8b950090-de44-48bd-b802-d44a399221f7","issue":"3","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业   "},"keywords":[{"id":"1da787e8-b9bd-4e1f-bf29-1a0888055793","keyword":"苯丙乳液","originalKeyword":"苯丙乳液"},{"id":"e628dafa-bbc1-462b-b0b6-fddf908b193b","keyword":"游离单体含量","originalKeyword":"游离单体含量"},{"id":"305e081a-23a2-4d25-b46a-8518e2961d74","keyword":"测定","originalKeyword":"测定"}],"language":"zh","publisherId":"tlgy200203016","title":"<span style=\"color:red\">化学分析</span>法测定苯丙乳液中游离单体含量","volume":"32","year":"2002"},{"abstractinfo":"系统综述和讨论了近十年我国钨工业<span style=\"color:red\">化学分析</span>的进展,包括<span style=\"color:red\">化学分析</span>、分光光度<span style=\"color:red\">分析</span>、<span style=\"color:red\">化学</span>发光与荧光<span style=\"color:red\">分析</span>、原子吸收光谱<span style=\"color:red\">分析</span>、原子发射光谱<span style=\"color:red\">分析</span>、电<span style=\"color:red\">化学分析</span>、X 荧光光谱<span style=\"color:red\">分析</span>及其它<span style=\"color:red\">分析</span>方法研究及应用.","authors":[{"authorName":"吴辛友","id":"3e36bec2-4252-4594-a3a0-19372ca4e48e","originalAuthorName":"吴辛友"},{"authorName":"童坚","id":"96779d19-0bcd-4eb3-b017-e5530d4fcc90","originalAuthorName":"童坚"}],"doi":"10.3969/j.issn.0258-7076.2000.06.007","fpage":"427","id":"c2ac144f-3655-4282-acf3-b8d3556093b8","issue":"6","journal":{"abbrevTitle":"XYJS","coverImgSrc":"journal/img/cover/XYJS.jpg","id":"67","issnPpub":"0258-7076","publisherId":"XYJS","title":"稀有金属"},"keywords":[{"id":"71001d43-80e5-4809-8baa-3c68e5cad5ac","keyword":"钨工业","originalKeyword":"钨工业"},{"id":"480d71e7-c120-42de-bbd8-29a2e24c23e1","keyword":"<span 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style=\"color:red\">化学分析</span>专业技术和管理人员参考借鉴.","authors":[{"authorName":"夏英姿","id":"04823989-dcb8-4aef-b096-a8d0cb3efa4c","originalAuthorName":"夏英姿"}],"doi":"10.3969/j.issn.1001-4381.2002.12.002","fpage":"6","id":"77e49133-2177-4783-847d-1d89cc480215","issue":"12","journal":{"abbrevTitle":"CLGC","coverImgSrc":"journal/img/cover/CLGC.jpg","id":"9","issnPpub":"1001-4381","publisherId":"CLGC","title":"材料工程"},"keywords":[{"id":"5a5081ed-d060-4b67-a059-56119ccfd380","keyword":"航空企业","originalKeyword":"航空企业"},{"id":"fe81c9ee-ddf6-48ae-8285-78d278a4d9e6","keyword":"管理方法","originalKeyword":"管理方法"},{"id":"b95e8925-a9de-4098-89fe-d77fae96f4f4","keyword":"管理模式","originalKeyword":"管理模式"},{"id":"b0782e76-4542-4aa2-9e89-3294563338d9","keyword":"人员轮岗培训","originalKeyword":"人员轮岗培训"}],"language":"zh","publisherId":"clgc200212002","title":"航空企业<span style=\"color:red\">化学分析</span>专业管理方法初探","volume":"","year":"2002"},{"abstractinfo":"介绍了<span style=\"color:red\">化学分析</span>中的部分常用量、法定计量单位及其使用规则,以及非法定计量单位与法定计量单位之间的换算.","authors":[{"authorName":"周文沛","id":"1590589e-052f-4db2-9302-b0568cd05b72","originalAuthorName":"周文沛"}],"doi":"10.3969/j.issn.0253-4312.2002.10.014","fpage":"38","id":"0a75b9b5-18a7-4b4d-b5e4-81b0c8c8d069","issue":"10","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业   "},"keywords":[{"id":"05237d0c-4faf-4f73-96e8-53fe0e02ffdb","keyword":"法定计量单位","originalKeyword":"法定计量单位"},{"id":"206a9e1b-aeab-4027-8eac-225690ca46a9","keyword":"摩尔","originalKeyword":"摩尔"},{"id":"e46f6548-4cde-4da1-a58c-5bceea85e92f","keyword":"摩尔质量","originalKeyword":"摩尔质量"},{"id":"05a9f05f-6565-4d7c-bf6a-8e5804787f3c","keyword":"物质B的浓度","originalKeyword":"物质B的浓度"}],"language":"zh","publisherId":"tlgy200210014","title":"<span style=\"color:red\">化学分析</span>中的常用量及法定计量单位","volume":"32","year":"2002"},{"abstractinfo":"概括了铁矿石<span style=\"color:red\">化学分析</span>方法国家标准现状,通过与国际标准比较,提出了今后发展趋势及修制订内容.","authors":[{"authorName":"董玉兰","id":"958a9ad5-c6e2-4556-9afe-bab4c0c96406","originalAuthorName":"董玉兰"},{"authorName":"魏春艳","id":"0bdc4588-2f93-480b-8b47-b1d550a52eeb","originalAuthorName":"魏春艳"}],"doi":"10.3969/j.issn.1000-7571.2003.01.023","fpage":"63","id":"6dcbe710-b574-46e7-8cf0-3694d6262ffe","issue":"1","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"101bbf20-2fd1-4dc3-b1d5-e67419dbafe4","keyword":"铁矿石","originalKeyword":"铁矿石"},{"id":"1985c454-2391-4413-9e96-db19e2a404c6","keyword":"国家标准","originalKeyword":"国家标准"},{"id":"94284fca-4c5e-459e-916b-5ceaa7b80cc9","keyword":"<span style=\"color:red\">化学分析</span>方法","originalKeyword":"化学分析方法"}],"language":"zh","publisherId":"yjfx200301023","title":"铁矿石<span style=\"color:red\">化学分析</span>方法国家标准概述","volume":"23","year":"2003"},{"abstractinfo":"微波溶样技术是世界上最先进的样品预处理技术之一.介绍了微波消解溶样技术的基本原理、优点及其在冶金<span style=\"color:red\">化学分析</span>中的应用.","authors":[{"authorName":"李洁","id":"5675e739-2e3c-4dd5-a163-37b024508657","originalAuthorName":"李洁"},{"authorName":"张穗忠","id":"db5483d7-9acb-46ff-9db4-907534a3e8b3","originalAuthorName":"张穗忠"},{"authorName":"宋卫良","id":"39c3458a-e496-447b-b5eb-cc4964640797","originalAuthorName":"宋卫良"}],"doi":"10.3969/j.issn.1001-1447.2006.02.011","fpage":"41","id":"4f0101b8-28b2-4556-9749-86a4cfd7739e","issue":"2","journal":{"abbrevTitle":"GTYJ","coverImgSrc":"journal/img/cover/GTYJ.jpg","id":"29","issnPpub":"1001-1447","publisherId":"GTYJ","title":"钢铁研究"},"keywords":[{"id":"5b2286b2-3b1b-4d4d-9650-aab1a711a7f7","keyword":"微波消解溶样技术","originalKeyword":"微波消解溶样技术"},{"id":"f2daae57-1395-4653-8fd0-1edd8cf838f2","keyword":"样品预处理","originalKeyword":"样品预处理"},{"id":"62397cca-01a1-469c-9b6d-9a55b5e8f4ee","keyword":"冶金<span style=\"color:red\">化学分析</span>","originalKeyword":"冶金化学分析"},{"id":"3e6ae53a-c079-4e70-9007-f3412144b8f0","keyword":"应用","originalKeyword":"应用"}],"language":"zh","publisherId":"gtyj200602011","title":"微波消解溶样技术在冶金<span style=\"color:red\">化学分析</span>中的应用","volume":"34","year":"2006"},{"abstractinfo":"材料<span style=\"color:red\">化学分析</span>是一门重要的质量技术,如何选择<span style=\"color:red\">化学分析</span>方法和如何进行<span style=\"color:red\">分析</span>过程质量控制对提高<span style=\"color:red\">分析</span>人员技术水平十分必要.依据多年理论学习和工作经验对此进行了探讨.选择<span style=\"color:red\">分析</span>方法应综合考虑<span style=\"color:red\">分析</span>目的、准确度要求、<span style=\"color:red\">分析</span>室现有技术水平、<span style=\"color:red\">分析</span>样品特性及<span style=\"color:red\">分析</span>成本等要素.湿法<span style=\"color:red\">分析</span>法和仪器<span style=\"color:red\">分析</span>法、标准<span style=\"color:red\">分析</span>法和非标准<span style=\"color:red\">分析</span>法要灵活运用.对<span style=\"color:red\">分析</span>过程中影响<span style=\"color:red\">分析</span>质量的主要因素要采取相应的的控制措施,如样品制备要有代表性,样品分解要完全、无干扰、时间短,正确使用标准物质,消除或降低<span style=\"color:red\">分析</span>空白,玻璃器皿、标准溶液和<span style=\"color:red\">分析</span>仪器要进行计量检定等.","authors":[{"authorName":"吴岩青","id":"b736ee3c-9db0-4b8d-825a-cd9c7a9998f0","originalAuthorName":"吴岩青"}],"doi":"10.3969/j.issn.1004-244X.2005.05.012","fpage":"41","id":"1bf186cb-b6ee-4693-9716-cc2ded22fc85","issue":"5","journal":{"abbrevTitle":"BQCLKXYGC","coverImgSrc":"journal/img/cover/BQCLKXYGC.jpg","id":"4","issnPpub":"1004-244X","publisherId":"BQCLKXYGC","title":"兵器材料科学与工程   "},"keywords":[{"id":"9aed45c9-ae29-4232-a259-1f057d85b9eb","keyword":"<span style=\"color:red\">分析</span>方法","originalKeyword":"分析方法"},{"id":"cd8b6e11-0fc9-49f3-b42d-ad176ad983f8","keyword":"选择","originalKeyword":"选择"},{"id":"6a9dcb72-5c4a-4b29-b3cd-05b4cbd141e8","keyword":"质量控制","originalKeyword":"质量控制"}],"language":"zh","publisherId":"bqclkxygc200505012","title":"<span style=\"color:red\">化学分析</span>方法选择与<span style=\"color:red\">分析</span>过程质量控制的探讨","volume":"28","year":"2005"},{"abstractinfo":"针对生物、<span style=\"color:red\">化学</span>和环境领域对集成化<span style=\"color:red\">分析</span>仪器的需求,提出了具有多通道同步检测功能的电<span style=\"color:red\">化学分析</span>仪设计与制造方案,详细介绍了仪器的主要组成部分:函数发生器、恒电位仪、电流检测模块和USB接口的具体设计.本文并对所研制多通道仪器进行了电<span style=\"color:red\">化学</span>实验性能测试.结果表明,所设计和研制的多通道电<span style=\"color:red\">化学分析</span>仪完全能够满足电<span style=\"color:red\">化学</span>实验中多通道<span style=\"color:red\">分析</span>测试的需求.","authors":[{"authorName":"孟伟丽","id":"e59c2e7c-9579-47b7-806d-b84182a88f98","originalAuthorName":"孟伟丽"},{"authorName":"姜智能","id":"432096ab-6f63-4290-a84e-f655eb31ec21","originalAuthorName":"姜智能"},{"authorName":"朱欣华","id":"60190a73-c7eb-4241-b675-d3edcfe97f8d","originalAuthorName":"朱欣华"},{"authorName":"苏岩","id":"e7d0a460-8990-4f43-9218-4329ea94b691","originalAuthorName":"苏岩"},{"authorName":"宋世平","id":"ac31507a-13aa-4266-b228-4e787b7a0c0b","originalAuthorName":"宋世平"},{"authorName":"樊春海","id":"ee3ac672-e926-491f-a578-fe4ba18c2ec7","originalAuthorName":"樊春海"}],"doi":"10.3969/j.issn.1007-4252.2010.05.004","fpage":"424","id":"8b98cfe7-9380-4bd9-9014-b0db683b8f42","issue":"5","journal":{"abbrevTitle":"GNCLYQJXB","coverImgSrc":"journal/img/cover/GNCLYQJXB.jpg","id":"34","issnPpub":"1007-4252","publisherId":"GNCLYQJXB","title":"功能材料与器件学报   "},"keywords":[{"id":"3b56bc2e-8e4c-4418-ad7f-868dbb77cf3f","keyword":"电<span style=\"color:red\">化学</span>","originalKeyword":"电化学"},{"id":"f1bbd66d-f7ec-43d4-b709-35c6c565b6eb","keyword":"<span style=\"color:red\">分析</span>仪器","originalKeyword":"分析仪器"},{"id":"fe66235e-4215-4fcf-89ce-a9dc5a128e17","keyword":"多通道","originalKeyword":"多通道"}],"language":"zh","publisherId":"gnclyqjxb201005004","title":"多通道电<span style=\"color:red\">化学分析</span>仪的研制及性能测试","volume":"16","year":"2010"},{"abstractinfo":"在90℃下,采用含有25 g/L硫酸镍,20 g/L次磷酸钠、35 g/L柠檬酸钠、0～6 g/t,卤磷酸钙和15 g/t.硫酸铵的镀液(pH 5.5),制备了基于卤磷酸钙的发<span style=\"color:red\">光化学</span>镍复合镀层.研究了镀液pH对复合镀层的沉积速率及卤磷酸钙含量的影响.采用硬度测量、磨损测试、腐蚀试验、紫外光谱,扫描电镜和X射线衍射对复合镀层进行了表征.在最佳卤磷酸钙质量浓度(4 g/L)下所得的复合镀层含77.59%(质量分数)镍、7.58%(质量分数)磷和14.83%(质量分数)卤磷酸钙.由于卤磷酸钙是硬质粒子,随着其嵌入量的增多,复合镀层的硬度增大.在存在卤磷酸钙的条件下,<span style=\"color:red\">化学</span>镍复合镀层的耐磨和耐蚀性能均显著提高.","authors":[{"authorName":"","id":"1827b42e-e4e6-45f1-b9c8-fef0242a06ad","originalAuthorName":""},{"authorName":"","id":"917bb699-fa4c-4f9d-9954-c2adc29c3fd5","originalAuthorName":""},{"authorName":"","id":"ccb43bee-6383-4e24-a922-7e49d84bb037","originalAuthorName":""}],"doi":"","fpage":"15","id":"ce532a1c-81ac-4ad3-a7bf-b8b2eeb05c24","issue":"1","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰   "},"keywords":[{"id":"db76b4b8-d95d-47c4-b1b8-ad17e0f626b1","keyword":"<span style=\"color:red\">化学</span>镀镍","originalKeyword":"化学镀镍"},{"id":"07ab4f37-7dec-405d-ad2b-512896892b87","keyword":"卤磷酸钙","originalKeyword":"卤磷酸钙"},{"id":"0b4f964e-2ff1-4783-a188-a0fa1022fea7","keyword":"复合镀层","originalKeyword":"复合镀层"},{"id":"756f37f2-852b-4d90-869c-202dfc52e9ff","keyword":"发光","originalKeyword":"发光"},{"id":"e34852f1-b63c-4c41-8dbd-16a65be8459f","keyword":"耐磨性","originalKeyword":"耐磨性"},{"id":"35313cb3-a33b-40e8-958d-d687c4af235c","keyword":"耐蚀性","originalKeyword":"耐蚀性"}],"language":"zh","publisherId":"ddyts200901006","title":"发<span style=\"color:red\">光化学</span>镍复合镀层","volume":"28","year":"2009"}],"totalpage":10183,"totalrecord":101822}