{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"采用浓HNO3和H2O2,消解法对样品进行预处理,采用火焰原子吸收分光光度法直接进行测定.通过对火焰原子吸收分光光度法中波长、狭缝宽度、灯电流、燃气流量比、燃烧器高度、<span style=\"color:red\">干扰</span><span style=\"color:red\">消除</span><span style=\"color:red\">剂</span>的选择确定茵栀黄注射液及其4味药材金银花、茵陈、栀子、黄芩中Cu、Fe、Zn、K、Na 5种金属元素的最佳测定条件,从而测定其含量.体积分数为2%HNO3、2%HCl及6%正丁醇分别作为测定Cu、K、Na、Fe及Zn的<span style=\"color:red\">干扰</span><span style=\"color:red\">消除</span><span style=\"color:red\">剂</span>,可<span style=\"color:red\">消除</span>基体<span style=\"color:red\">干扰</span>,提高测定灵敏度.线性回归方程及相关系数分别为:Acu=0.087 4c+0.007 8,rCu=0.999 5;AZn=0.244 6c+0.072 4,rZn=0.999 6;AFe=0.065 9c+0.022 1,rFe=0.999 9;AK=0.224 2c+0.008 3,rK=0.999 5;ANa=0.613 0c+0.038 0,rNa=0.999 3.方法回收率为95.6%～111%,相对标准偏差小于4.0%.","authors":[{"authorName":"宗水珍","id":"180d6386-9669-48fe-a810-7d814bd6220f","originalAuthorName":"宗水珍"},{"authorName":"汪学英","id":"cccdd891-854e-4b1c-9569-08287aa8c6d2","originalAuthorName":"汪学英"},{"authorName":"徐娟","id":"1cde0ade-d30c-4b0b-8cd8-93aa28f6e71f","originalAuthorName":"徐娟"}],"doi":"10.3969/j.issn.1000-0518.2007.07.025","fpage":"841","id":"9fe61dba-f023-4218-9fb2-d4ba6538ebcd","issue":"7","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"f49d014a-39bf-45fb-a42f-4da68ec79796","keyword":"火焰原子吸收光谱法","originalKeyword":"火焰原子吸收光谱法"},{"id":"2b2f7347-a29b-4c2f-9d15-a013ec1abcdf","keyword":"金属元素","originalKeyword":"金属元素"},{"id":"cd4cc143-fd1a-44d5-9665-e1d6377bea42","keyword":"茵栀黄注射液","originalKeyword":"茵栀黄注射液"},{"id":"2d964796-b037-4588-8c8c-6d6a559b77d5","keyword":"<span style=\"color:red\">干扰</span><span style=\"color:red\">消除</span><span style=\"color:red\">剂</span>","originalKeyword":"干扰消除剂"}],"language":"zh","publisherId":"yyhx200707025","title":"茵栀黄注射液及其药材中5种金属元素含量的FAAS法测定","volume":"24","year":"2007"},{"abstractinfo":"综述了含金矿样的溶解方法和<span style=\"color:red\">干扰</span>元素的<span style=\"color:red\">消除</span>.主要介绍各种溶样方法、溶样体系和常见<span style=\"color:red\">干扰</span>元素的<span style=\"color:red\">消除</span>方法.引用文献27篇.","authors":[{"authorName":"冯月斌","id":"35f558b1-2f7a-40d1-bc11-a52bbd433606","originalAuthorName":"冯月斌"}],"doi":"10.3969/j.issn.1001-1277.2003.02.014","fpage":"50","id":"0e4ad41b-4e8b-48ea-aea3-294bc1ba14c8","issue":"2","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"adb98f93-24f3-4a3f-8d54-bc5fca94f170","keyword":"金","originalKeyword":"金"},{"id":"15a0c906-a876-4556-aca8-0e59a6c240f1","keyword":"溶解","originalKeyword":"溶解"},{"id":"df05a8c4-a831-477e-9bc1-80bef93ba580","keyword":"<span style=\"color:red\">干扰</span>元素","originalKeyword":"干扰元素"}],"language":"zh","publisherId":"huangj200302014","title":"含金矿样的溶样方法和<span style=\"color:red\">干扰</span>元素的<span style=\"color:red\">消除</span>","volume":"24","year":"2003"},{"abstractinfo":"根据含碳铅精矿自身的性质与特点,通过试验,选用氯酸钾硝酸饱和溶液同时<span style=\"color:red\">消除</span>硫、碳、铅的<span style=\"color:red\">干扰</span>,实现<span style=\"color:red\">消除</span><span style=\"color:red\">干扰</span>因素与溶解金同时完成的一体化方法,并取得了满意的效果.","authors":[{"authorName":"邓淑萍","id":"2ec81ac1-f3f0-4e37-adec-98c31b073972","originalAuthorName":"邓淑萍"}],"doi":"10.3969/j.issn.1001-1277.2001.06.014","fpage":"45","id":"a461090a-4692-4fff-a0df-e8a8fe7ac41e","issue":"6","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"933b0f0d-c368-458e-aa81-ddf5e21b9b6f","keyword":"合碳铅精矿","originalKeyword":"合碳铅精矿"},{"id":"e4b16b5f-0be2-4114-a79d-983863929720","keyword":"氯酸钾硝酸饱和溶液","originalKeyword":"氯酸钾硝酸饱和溶液"},{"id":"abd84005-5a44-4e65-afeb-f409a7d5a890","keyword":"硫","originalKeyword":"硫"},{"id":"3646f669-164a-4088-b559-36dabdfd2376","keyword":"碳","originalKeyword":"碳"},{"id":"9e15e457-a896-4388-8b6e-b4b053f0ab29","keyword":"铅","originalKeyword":"铅"},{"id":"b53d474f-89b5-47cc-b29e-7f6b8050d81a","keyword":"金","originalKeyword":"金"}],"language":"zh","publisherId":"huangj200106014","title":"含碳铅精矿中<span style=\"color:red\">干扰</span>元素的<span style=\"color:red\">消除</span>与金的溶解试验研究","volume":"22","year":"2001"},{"abstractinfo":"研究了Pb,Ag对碘量法测定铅精矿中Au的影响,提出了改进方法并<span style=\"color:red\">消除</span>Pb,Ag的<span style=\"color:red\">干扰</span>,提高了分析结果的准确度.","authors":[{"authorName":"曹会兰","id":"74a7455f-2791-493a-bf7d-7a827acba539","originalAuthorName":"曹会兰"}],"doi":"10.3969/j.issn.1000-7571.2003.03.023","fpage":"61","id":"42b11485-2e32-4a04-ac91-82e6dd3031a6","issue":"3","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"7547cca8-c470-4729-9d85-9730bf2b7956","keyword":"铅精矿","originalKeyword":"铅精矿"},{"id":"3b53df09-28b4-4fc7-a675-26396c17ac64","keyword":"Pb","originalKeyword":"Pb"},{"id":"dbf93632-a06d-4efc-a3bb-893511c02eb2","keyword":"Ag","originalKeyword":"Ag"},{"id":"d2e739b4-753a-40a7-a65d-3096b44fc8d7","keyword":"Au","originalKeyword":"Au"}],"language":"zh","publisherId":"yjfx200303023","title":"碘量法分析铅精矿中金时铅、银的<span style=\"color:red\">干扰</span>与<span style=\"color:red\">消除</span>","volume":"23","year":"2003"},{"abstractinfo":"本文详细介绍了在SQUID系统中,由于50Hz工频<span style=\"color:red\">干扰</span>导致系统无法正常工作的原因以及我们为此而设计的一种解决方案,实验取得了良好的效果,<span style=\"color:red\">消除</span>了50Hz<span style=\"color:red\">干扰</span>对SQUID系统的影响.系统在50Hz<span style=\"color:red\">干扰</span>很强的环境中能稳定工作.","authors":[{"authorName":"张升原","id":"04bc1634-0cac-410e-8550-66ce3588e559","originalAuthorName":"张升原"},{"authorName":"谢飞翔","id":"ea42c415-8b9b-4de7-b097-46fbeea25a8f","originalAuthorName":"谢飞翔"},{"authorName":"刘新元","id":"c9f2ca5a-8808-4bf9-97a3-7985ead8bf52","originalAuthorName":"刘新元"},{"authorName":"马平","id":"c47f7233-bfc1-4195-a947-4c8741f6e6c5","originalAuthorName":"马平"},{"authorName":"王守证","id":"587a162f-905b-40f5-a50c-e7e213a806b8","originalAuthorName":"王守证"},{"authorName":"戴远东","id":"3b17be6d-d61e-4a54-bef3-985c255dd45b","originalAuthorName":"戴远东"}],"doi":"10.3969/j.issn.1000-3258.2002.04.005","fpage":"264","id":"532e7096-4134-4737-894c-955b22c5dd7c","issue":"4","journal":{"abbrevTitle":"DWWLXB","coverImgSrc":"journal/img/cover/DWWLXB.jpg","id":"19","issnPpub":"1000-3258","publisherId":"DWWLXB","title":"低温物理学报   "},"keywords":[{"id":"d4104168-b2ab-4a96-9a3b-34d50ec6b7f2","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"dwwlxb200204005","title":"一种<span style=\"color:red\">消除</span>HTc SQUID系统中50Hz工频<span style=\"color:red\">干扰</span>的有效方法","volume":"24","year":"2002"},{"abstractinfo":"在原子吸收光谱分析中，应用正交多项式回归设计对<span style=\"color:red\">干扰</span>效应进行计算<span style=\"color:red\">消除</span>。通过对高纯Eu2O3中钙含量测定实验建立了<span style=\"color:red\">消除</span><span style=\"color:red\">干扰</span>的最优回归方程，回归方程精度为1.32×10－2，用于高纯Eu2O3中钙含量测定，计算值与实测值基本一致，相对误差为1%～4％。","authors":[{"authorName":"廖列文","id":"38e72c03-bfbb-4c02-8bec-d9a05a3ab943","originalAuthorName":"廖列文"},{"authorName":"邱春","id":"283905dc-c088-43f5-b822-0faafec58d93","originalAuthorName":"邱春"},{"authorName":"陈涛","id":"4b19c321-1896-4e25-bcb0-a434a4504edc","originalAuthorName":"陈涛"}],"doi":"10.3969/j.issn.1000-7571.2001.03.013","fpage":"39","id":"2dacbd50-ebe4-45ac-92ed-60e82487b4e4","issue":"3","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"c26a344e-d575-4011-97ec-668b51daf796","keyword":"正交多项式回归设计","originalKeyword":"正交多项式回归设计"},{"id":"c12ab973-58a2-4ba8-8047-0f5e83e7829b","keyword":"计算<span style=\"color:red\">消除</span>","originalKeyword":"计算消除"},{"id":"0835085e-a67c-4896-bfd7-49ac4b8c5df7","keyword":"原子吸收光谱分析","originalKeyword":"原子吸收光谱分析"},{"id":"4502df45-721a-4b9d-88f9-645a6ce37dcc","keyword":"<span style=\"color:red\">干扰</span>效应","originalKeyword":"干扰效应"}],"language":"zh","publisherId":"yjfx200103013","title":"正交多项式回归设计在计算<span style=\"color:red\">消除</span>原子吸收光谱分析中<span style=\"color:red\">干扰</span>效应的应用","volume":"21","year":"2001"},{"abstractinfo":"建立了固相萃取／液相色谱-串联质谱检测水中18种苯胺类化合物的分析方法，并优化了固相萃取和色谱条件。水样经混合型阳离子交换柱（ MCX）或硅胶基体阳离子交换柱（ SCX）富集后，用氨水甲醇溶液洗脱，用超纯水适当地稀释后，用液相色谱-串联质谱法测定。以 ODS柱为分离柱，甲醇-0.005％（ v／v）甲酸水溶液为流动相，梯度洗脱，多反应监测模式分析，内标法定量。18种苯胺类化合物的分析时间在15 min之内。采用 MCX柱萃取时，16种苯胺化合物的方法检出限为0.002～0.035μg／L，地表水样品的加标回收率为72.5％～92.5％，相对标准偏差为1.4％～9.6％；采用 SCX柱萃取时，17种苯胺类化合物的方法检出限为0.013～0.207μg／L，地表水样品的加标回收率为66.5％～102％，相对标准偏差为2.4％～13.6％。本实验还考察了<span style=\"color:red\">消除</span>基质<span style=\"color:red\">干扰</span>的5种方法，结果表明，调整色谱分离条件是最有效的方法，其次是选择合适的前处理方法。更换离子源、内标法定量和利用基质标准溶液校正也可在一定程度上<span style=\"color:red\">消除</span>或补偿基质<span style=\"color:red\">干扰</span>。","authors":[{"authorName":"赵云芝","id":"a1b9a531-b736-4afa-86bb-7913f9a80749","originalAuthorName":"赵云芝"},{"authorName":"谢振伟","id":"46761275-a8e6-4ccc-8396-356d61f0f004","originalAuthorName":"谢振伟"},{"authorName":"潘乐丹","id":"236b11b0-e7ae-4ceb-9553-b7dbf541fef3","originalAuthorName":"潘乐丹"},{"authorName":"姚欢","id":"bc076557-36e6-4d27-a757-fa31a49deefd","originalAuthorName":"姚欢"}],"doi":"10.3724/SP.J.1123.2015.11009","fpage":"289","id":"b8df2eaa-95cf-4093-b19f-d50b0295b487","issue":"3","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"a4d2b758-9415-43d6-96fe-644d5696f6d1","keyword":"固相萃取","originalKeyword":"固相萃取"},{"id":"6905df1a-a74f-4632-a56e-c8b51c347fff","keyword":"液相色谱-串联质谱法","originalKeyword":"液相色谱-串联质谱法"},{"id":"0a814fee-6255-4264-b1cd-1056b7b3aa84","keyword":"<span style=\"color:red\">消除</span>基质<span style=\"color:red\">干扰</span>的方法","originalKeyword":"消除基质干扰的方法"},{"id":"3ed25006-1014-4118-b5bd-132a865a37a5","keyword":"苯胺类化合物","originalKeyword":"苯胺类化合物"},{"id":"4a8cf012-df46-4274-a792-c739e688f5ed","keyword":"水样","originalKeyword":"水样"}],"language":"zh","publisherId":"sp201603011","title":"固相萃取／液相色谱-串联质谱法测定水中苯胺类化合物及基质<span style=\"color:red\">干扰</span>的<span style=\"color:red\">消除</span>","volume":"34","year":"2016"},{"abstractinfo":"用正交试验设计[1]对高纯氧化铕中钙测定时,基体和酸度的<span style=\"color:red\">干扰</span>进行了试验.结果表明,基体的影响最为显著,酸度影响次之,而<span style=\"color:red\">干扰</span>效应与钙的浓度无关.","authors":[{"authorName":"林建原","id":"a125fe3d-a35b-4155-bd06-798050f1bab1","originalAuthorName":"林建原"},{"authorName":"黄志勤","id":"32728cdc-dec6-4704-91a8-058c5903384a","originalAuthorName":"黄志勤"},{"authorName":"邱春","id":"ef00595c-b96a-4dac-9c94-88d8fca3c227","originalAuthorName":"邱春"}],"doi":"10.3969/j.issn.1004-0277.2004.06.015","fpage":"56","id":"df92f415-dfcc-4424-ac2b-6d84bafd4f25","issue":"6","journal":{"abbrevTitle":"XT","coverImgSrc":"journal/img/cover/XT.jpg","id":"65","issnPpub":"1004-0277","publisherId":"XT","title":"稀土"},"keywords":[{"id":"eec577a9-65b3-4c2f-b3f6-3fc512175eab","keyword":"原子吸收光谱法","originalKeyword":"原子吸收光谱法"},{"id":"e631cab8-4c9c-412e-8f62-8c30ec8b8ddb","keyword":"Eu2O3","originalKeyword":"Eu2O3"},{"id":"108bf9f1-82bd-4178-a73a-562d28d21530","keyword":"钙","originalKeyword":"钙"}],"language":"zh","publisherId":"xitu200406015","title":"原子吸收光谱法测定高纯氧化铕中钙<span style=\"color:red\">干扰</span>效应计算<span style=\"color:red\">消除</span>方法的研究","volume":"25","year":"2004"},{"abstractinfo":"柴油车尾气排放的污染物已引起严重的环境问题,其中氮氧化物(NOx)和碳烟(Soot)是主要且较难去除的污染物,目前最有效的尾气处理技术之一是NOx-Soot同时催化<span style=\"color:red\">消除</span>技术,而高效催化<span style=\"color:red\">剂</span>的研制和开发是该技术的核心,其中稀土催化<span style=\"color:red\">剂</span>是非常有前景的催化<span style=\"color:red\">剂</span>之一.本文以NOx-Soot同时催化<span style=\"color:red\">消除</span>为主线,介绍了该技术中选择稀土催化<span style=\"color:red\">剂</span>的原因、用于该反应稀土催化<span style=\"color:red\">剂</span>的类型及反应机理,对不同稀土催化<span style=\"color:red\">剂</span>同时<span style=\"color:red\">消除</span>NOx-Soot的活性与选择性进行了对比,并总结性的提出目前该催化<span style=\"color:red\">剂</span>存在的主要问题和发展方向.","authors":[{"authorName":"王艳","id":"1fd58791-5c86-407d-915f-a8c9552117cc","originalAuthorName":"王艳"},{"authorName":"李兆强","id":"4917434c-8a4b-40ad-a289-f888ae40b4a2","originalAuthorName":"李兆强"}],"doi":"10.16533/J.CNKI.15-1099/TF.201505024","fpage":"133","id":"ca29a9bd-dc4a-4e61-bb71-acbe670b1b61","issue":"5","journal":{"abbrevTitle":"XT","coverImgSrc":"journal/img/cover/XT.jpg","id":"65","issnPpub":"1004-0277","publisherId":"XT","title":"稀土"},"keywords":[{"id":"60815f18-957f-4329-b0ca-166d4533244b","keyword":"柴油车尾气","originalKeyword":"柴油车尾气"},{"id":"93d9a81b-089a-416c-a684-4010657e39a6","keyword":"NOx","originalKeyword":"NOx"},{"id":"9b1d4e14-c4cb-4b5d-a7fd-66cb73bc330c","keyword":"Soot","originalKeyword":"Soot"},{"id":"cdfd7607-ec04-45cb-b96b-268a359d0e1c","keyword":"同时<span style=\"color:red\">消除</span>","originalKeyword":"同时消除"},{"id":"7802a4fc-8f07-4bd0-afda-bab1fb88a0cc","keyword":"稀土催化<span style=\"color:red\">剂</span>","originalKeyword":"稀土催化剂"}],"language":"zh","publisherId":"xitu201505024","title":"同时<span style=\"color:red\">消除</span>柴油车Soot与NOx稀土催化<span style=\"color:red\">剂</span>的研究进展","volume":"36","year":"2015"},{"abstractinfo":"介绍了在火焰原子吸收光谱法中三乙醇胺及氯化十二烷基三甲基铵对钼的增感作用及<span style=\"color:red\">消除</span><span style=\"color:red\">干扰</span>的能力.其机理是溶液表面张力的降低、雾化效率的提高、胶团化合物的形成及表面活性<span style=\"color:red\">剂</span>对钼的富集作用.","authors":[{"authorName":"李枚枚","id":"93eaa17c-027c-44de-8832-5ffe46220257","originalAuthorName":"李枚枚"},{"authorName":"提淑华","id":"85bb1267-ac10-4439-bbe9-236dab5f075b","originalAuthorName":"提淑华"},{"authorName":"崔力","id":"c283e1b2-ac70-4d7c-bf4c-976765211d1d","originalAuthorName":"崔力"},{"authorName":"王敬涛","id":"4369ba8a-f13d-4dbd-bf4f-e3ff7a4cb320","originalAuthorName":"王敬涛"}],"doi":"10.3969/j.issn.1000-7571.2000.05.006","fpage":"15","id":"501a3025-7074-444c-8118-c279565134f1","issue":"5","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"f546a94a-fcd4-4deb-86d3-3ef7591fa45e","keyword":"火焰原子吸收光谱法","originalKeyword":"火焰原子吸收光谱法"},{"id":"f67e5948-e62f-4ba4-9cb3-70376f42b82b","keyword":"表面活性<span style=\"color:red\">剂</span>","originalKeyword":"表面活性剂"},{"id":"a371aab5-e0f4-4a05-a8c1-0113df79ebd1","keyword":"增感","originalKeyword":"增感"},{"id":"113901fa-623e-4fe0-a951-3dc97e4f1ce5","keyword":"<span style=\"color:red\">干扰</span>","originalKeyword":"干扰"},{"id":"844c98aa-0657-40e1-9e48-1441922358f7","keyword":"钼","originalKeyword":"钼"}],"language":"zh","publisherId":"yjfx200005006","title":"火焰原子吸收光谱法中表面活性<span style=\"color:red\">剂</span>对钼增感和抑制<span style=\"color:red\">干扰</span>作用的机理","volume":"20","year":"2000"}],"totalpage":3347,"totalrecord":33470}