{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"采用单辊快淬法制备Fe78Co2Zr8Nb2 B0-xGex(x=1,2,3)系非晶合金,在不同热处理条件下对两种合金进行热处理.利用X射线衍射仪(XRD)、透射电镜(TEM)和振动样品磁强计(VSM)等测试手段对合金的微观结构和磁性能进行研究.研究结果表明,3种合金的晶化过程相似:非晶→非晶+α-Fe(Co)→αFe(Co)+ Fe3 Zr+ Fe2B.3种合金的比饱和磁化强度(Ms)大体上随退火温度的升高而增大;3种合金的矫顽力(Hc)随退火温度的升高均呈现先增加、后降低、再增加的复杂变化趋势.","authors":[{"authorName":"孟祥成","id":"5cdd18e2-5142-4616-a540-682d4fe46619","originalAuthorName":"孟祥成"},{"authorName":"刘洁","id":"76cf75a0-a192-4248-ac8c-6ce350084ca7","originalAuthorName":"刘洁"},{"authorName":"<span style=\"color:red\">左</span><span style=\"color:red\">斌</span>","id":"ec63380e-cf03-47ee-af2a-2ded1b373edd","originalAuthorName":"左斌"},{"authorName":"华中","id":"80310d4d-01f6-4515-ab54-3d3e76349b59","originalAuthorName":"华中"}],"doi":"","fpage":"99","id":"6cd948fa-efeb-446e-93a3-fd7c7c88dc5b","issue":"12","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"2c6101c9-d3e3-43ea-92c6-be60d0c50279","keyword":"快淬","originalKeyword":"快淬"},{"id":"0bac072c-3c69-49ca-9ca6-a1407bc00151","keyword":"晶化过程","originalKeyword":"晶化过程"},{"id":"7aae0b94-418f-4890-8fc3-d8f82589b6e1","keyword":"磁性能","originalKeyword":"磁性能"}],"language":"zh","publisherId":"cldb201412026","title":"Fe78Co2Zr8Nb2B10-xGex(x=1,2,3)合金的晶化过程和磁性能研究","volume":"28","year":"2014"},{"abstractinfo":"采用单辊快淬法制备Fe80Zr10B10非晶合金,并对该合金进行不同温度及不同保温时间热处理.利用X射线衍射仪(XRD)、透射电镜(TEM)和振动样品磁强计(VSM)对合金的晶化过程和磁性能进行测试分析.结果表明:Fe80 Zr10 B10非晶合金经550℃退火保温不同时间,仅析出 α-Fe相.经600 ℃退火,保温1 min后晶化产物为α-Fe相和x相(α-Mn型相),x相为亚稳相,随保温时间延长,x相转变为α-Fe相.经650℃退火,保温1 min的晶化产物为Laves C14(λ)相,随保温时间增加,λ相向α-Fe相转变,并伴有Fe3Zr相和Fe2Zr相析出.合金经550℃退火,矫顽力(Hc)随保温时间的延长变化不大,比饱和磁化强度(Ms)逐渐增大.600℃退火,矫顽力(Hc)在合金保温10 min后达到最大值然后减小,比饱和磁化强度(Ms)在合金保温10 min后达到最小值,然后增大.650℃退火,矫顽力(Hc)随保温时间的增加而减小,比饱和磁化强度(Ms)逐渐增大.","authors":[{"authorName":"<span style=\"color:red\">左</span><span style=\"color:red\">斌</span>","id":"9b4e1a5e-2847-4e34-ad84-6a3c7307123a","originalAuthorName":"左斌"},{"authorName":"孙亚明","id":"3ca36676-5bd5-4c9a-93d1-8f819c42e6f1","originalAuthorName":"孙亚明"},{"authorName":"王晓楠","id":"0c277fea-fb57-4a6a-9643-0f8c57116f9c","originalAuthorName":"王晓楠"},{"authorName":"华中","id":"0e364503-fab8-41bc-b034-bac0c6136de6","originalAuthorName":"华中"}],"doi":"","fpage":"34","id":"723efed0-351c-4ce5-a7de-642d00edb1d4","issue":"8","journal":{"abbrevTitle":"CLRCLXB","coverImgSrc":"journal/img/cover/CLRCLXB.jpg","id":"15","issnPpub":"1009-6264","publisherId":"CLRCLXB","title":"材料热处理学报"},"keywords":[{"id":"081d6534-d3a2-42dc-ba27-9d1614203a7d","keyword":"非晶合金","originalKeyword":"非晶合金"},{"id":"f444cb47-70ce-4382-9a51-877426b8643a","keyword":"晶化过程","originalKeyword":"晶化过程"},{"id":"6f2fc7ac-ff21-4cd2-bf47-20853a9435e8","keyword":"热处理","originalKeyword":"热处理"},{"id":"2bbd7ecd-96d4-4f15-b94e-d4777a1bec66","keyword":"磁性能","originalKeyword":"磁性能"}],"language":"zh","publisherId":"jsrclxb201508007","title":"热处理条件对Fe80Zr10B10合金的晶化过程和磁性能的影响","volume":"36","year":"2015"},{"abstractinfo":"采用单辊快淬法制备(Fe1-xCox)80Zr10B10(x=0,0.1,0.2,0.3)非晶合金,并对4种合金在不同温度下进行等温热处理.利用差热分析仪(DTA),X射线衍射仪(XRD),透射电镜(TEM)和振动样品磁强计(VSM)等测试手段对样品的热性能、微观结构及磁性能进行研究.结果表明,未添加Co元素的Fe80Zr10B10合金的热稳定性明显高于添加Co元素的合金,而(Fe1-xCox)80Zr10B10(x=0.1,0.2,0.3)合金的热稳定性相差不大.Fe80Zr10B10和Fe72Co8Zr10B10合金的晶化过程相似;Fe64Co16Zr10B10和Fe56Co24Zr10B10合金的晶化过程相似.4种合金的矫顽力(Hc)呈现先上升后下降的趋势,在873 K达到最大值.","authors":[{"authorName":"华中","id":"f80e8fbf-fb64-474a-b59e-5eeb567b171f","originalAuthorName":"华中"},{"authorName":"<span style=\"color:red\">左</span><span style=\"color:red\">斌</span>","id":"75dbe56d-aa81-449f-a79c-2995d0968105","originalAuthorName":"左斌"},{"authorName":"王丽丽","id":"6b6ab619-7cf5-41a6-b926-de6beb158132","originalAuthorName":"王丽丽"},{"authorName":"刘尧棣","id":"48f21c07-ae68-4af4-8551-8ee9e8cf46a6","originalAuthorName":"刘尧棣"},{"authorName":"董丽荣","id":"d2c72dca-7032-440c-b44b-e36b79cf305c","originalAuthorName":"董丽荣"},{"authorName":"孙亚明","id":"75a34f06-4957-4fd4-9b3a-dd5071c9eb24","originalAuthorName":"孙亚明"}],"doi":"","fpage":"616","id":"b8067ff4-203b-40b8-9904-0ff1dbbb21bd","issue":"3","journal":{"abbrevTitle":"XYJS","coverImgSrc":"journal/img/cover/XYJS.jpg","id":"67","issnPpub":"0258-7076","publisherId":"XYJS","title":"稀有金属"},"keywords":[{"id":"aca66485-2f55-4c50-84b7-520f931dda59","keyword":"非晶合金","originalKeyword":"非晶合金"},{"id":"0ef17b90-cdab-4e77-b904-497f4d235107","keyword":"热稳定性","originalKeyword":"热稳定性"},{"id":"f4b627c2-e7a1-469f-8c17-6950c5fea9ba","keyword":"亚稳相","originalKeyword":"亚稳相"}],"language":"zh","publisherId":"xyjsclygc201503020","title":"(Fe1-xCox)80Zr10B10(x=0,0.1,0.2,0.3)合金的热性能、结构和磁性能研究","volume":"44","year":"2015"},{"abstractinfo":"采用单辊快淬法制备Fe78Co2Zr8Nb2B9M1(M =Ta、Cu)非晶合金薄带,在不同温度下对合金进行等温热处理.利用DTA、XRD、TEM、VSM和阻抗分析仪研究合金的热行为、微观结构、磁性能及巨磁阻抗效应.结果表明,晶化初期,Fe78Co2Zr8Nb2B9Ta1非晶合金析出α-Mn亚稳相和α-Fe(Co)相,Fe78Co2Zr8Nb2B9Cu1非晶合金仅析出α-Fe(Co)相.600℃退火后的Fe78Co2Zr8Nb2B9Cu1合金中晶化相的平均晶粒尺寸小于Fe78Co2Zr8Nb2B9Ta1合金.合金的Ms均随退火温度的升高而逐渐增大.Fe78Co2Zr8Nb2B9Ta1合金的Hc在600℃退火后明显增大,这与α-Mn型相的析出有关;而Fe78Co2Zr8Nb2B9Cu1合金的Hc在600℃退火后达到极小值.合金的GMImax值随退火温度增加先上升后下降.Fe78Co2Zr8Nb2B9Cu1合金具有比Fe78Co2Zr8Nb2B9Ta1合金更显著的GMI效应.","authors":[{"authorName":"华中","id":"06afd8e4-f312-4bd6-aa3c-6327f8f1243f","originalAuthorName":"华中"},{"authorName":"刘洁","id":"de6ec5a6-89f3-4ae3-ba6e-71d85597b607","originalAuthorName":"刘洁"},{"authorName":"<span style=\"color:red\">左</span><span style=\"color:red\">斌</span>","id":"b1a731db-1464-4a85-90ee-dbadc936bffd","originalAuthorName":"左斌"},{"authorName":"王丽丽","id":"6ed99a9a-29c5-41bc-8051-c3e5ac0495da","originalAuthorName":"王丽丽"},{"authorName":"于万秋","id":"fdd77ab0-3448-420e-92e8-366485546eeb","originalAuthorName":"于万秋"},{"authorName":"赵立猛","id":"54de4998-7bf0-424d-86a6-0704c4d7ddde","originalAuthorName":"赵立猛"}],"doi":"","fpage":"25","id":"cf75a079-77b1-468a-8c57-2606372cde9b","issue":"10","journal":{"abbrevTitle":"CLRCLXB","coverImgSrc":"journal/img/cover/CLRCLXB.jpg","id":"15","issnPpub":"1009-6264","publisherId":"CLRCLXB","title":"材料热处理学报"},"keywords":[{"id":"804653ac-aa6d-4489-b63e-7399164bc906","keyword":"微观结构","originalKeyword":"微观结构"},{"id":"359ab657-f77c-4147-b6a6-b9789f20022f","keyword":"亚稳相","originalKeyword":"亚稳相"},{"id":"35e99db1-4cde-4531-94a1-25801105c369","keyword":"磁性能","originalKeyword":"磁性能"},{"id":"9f3c3e18-e31a-441f-9f55-6c3bb1932ebb","keyword":"巨磁阻抗效应","originalKeyword":"巨磁阻抗效应"}],"language":"zh","publisherId":"jsrclxb201310005","title":"Fe78Co2Zr8Nb2B9M1(M=Ta、Cu)合金的微观结构和巨磁阻抗效应","volume":"34","year":"2013"},{"abstractinfo":"采用单辊快淬法制备Fe40Co40Zr(10-x)MoxB9Cu1(x=0,2,4)系非晶合金,并对3种合金进行不同温度热处理.利用X射线衍射仪(XRD)、透射电镜(TEM)、差热分析仪(DTA)和振动样品磁强计(VSM)对合金的微观结构、热性能和磁性能进行测试分析.结果表明:Fe40Co40Zr(10-x)MoxB9Cu1(x=0,2,4)3种合金第1个晶化峰的激活能随Mo含量的增加而减小,Mo的添加不利于合金的热稳定性.Mo含量的增加抑制了ZrCo3B2等化合物的析出,细化了结晶相的晶粒尺寸.Fe40Co40Zr(10-x)MoxBgCu1 (X=0,2,4)3种非晶合金的矫顽力Hc均随退火温度的升高而逐渐增大.Mo的添加明显降低了合金的矫顽力.","authors":[{"authorName":"华中","id":"c86665a4-ddd9-4482-9a54-7f7fe844917f","originalAuthorName":"华中"},{"authorName":"<span style=\"color:red\">左</span><span style=\"color:red\">斌</span>","id":"0cb88242-a26f-40d6-bce1-061d47cd18f5","originalAuthorName":"左斌"},{"authorName":"王晓楠","id":"99145132-2d61-4cb0-aa71-739789a31a1f","originalAuthorName":"王晓楠"},{"authorName":"孙亚明","id":"89a1358e-3e33-4301-988c-be2cd603bed4","originalAuthorName":"孙亚明"},{"authorName":"董丽荣","id":"4f4519b6-ddb8-4d71-b6a9-250b6a4bc8b1","originalAuthorName":"董丽荣"}],"doi":"","fpage":"358","id":"3ca73e9e-8a44-464f-a2b2-9abe0e0cb66f","issue":"2","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"adca2d81-2996-40bf-92b7-c99e0584a4c8","keyword":"非晶合金","originalKeyword":"非晶合金"},{"id":"bfd7141a-cc04-46c3-b976-6d7b08ad0436","keyword":"Mo含量","originalKeyword":"Mo含量"},{"id":"0982c4d1-d90b-4541-91ca-8fa56db04121","keyword":"微观结构","originalKeyword":"微观结构"},{"id":"e0156157-3e74-4aab-aab1-afc482b387ba","keyword":"热性能","originalKeyword":"热性能"},{"id":"256d7fb5-80e9-481b-9118-fb91f468e850","keyword":"矫顽力","originalKeyword":"矫顽力"}],"language":"zh","publisherId":"xyjsclygc201602019","title":"Mo含量对Fe40Co40Zr(10-x)MoxB9Cu1(x=0,2,4)合金的微观结构,热性能和磁性能的影响","volume":"45","year":"2016"},{"abstractinfo":"在HAc-NaAc介质中,铕(Ⅲ)与盐酸<span style=\"color:red\">左</span>氧氟沙星形成络合物使盐酸<span style=\"color:red\">左</span>氧氟沙星的荧光显著猝灭,由此建立了测定铕(Ⅲ)的新方法.该体系的最大激发波长λex=365nm,最大发射波长λem=500nm.实验结果表明,铕(Ⅲ)的浓度在2.00×10-7 mol·L-1～2.80×10-5 mol·L-1范围内与△F=F-F0形成良好的线性关系,最低检出限为8.80×10-8 mol·L-1,回收率在96.0%～101.5%之间,本法灵敏度高、选择性好,结果满意.","authors":[{"authorName":"孙雪花","id":"cf3818de-cde0-49fe-818e-f646f63613e7","originalAuthorName":"孙雪花"},{"authorName":"马红燕","id":"de489c7d-94de-4a68-a4ed-545b3cb12056","originalAuthorName":"马红燕"},{"authorName":"齐广才","id":"b8521f4b-22df-4533-900d-5ba8115e7fb4","originalAuthorName":"齐广才"},{"authorName":"田锐","id":"ca561830-6a46-41ec-be3e-a922498f83e9","originalAuthorName":"田锐"},{"authorName":"杨阳","id":"182480c2-afce-4224-bd63-a4ad4c244896","originalAuthorName":"杨阳"},{"authorName":"樊江鹏","id":"0c468e1b-a78c-4908-859a-79bc1edea965","originalAuthorName":"樊江鹏"}],"doi":"10.3969/j.issn.1004-0277.2011.02.013","fpage":"58","id":"e71aca44-443c-4b5b-ba75-cf504fa9ed17","issue":"2","journal":{"abbrevTitle":"XT","coverImgSrc":"journal/img/cover/XT.jpg","id":"65","issnPpub":"1004-0277","publisherId":"XT","title":"稀土"},"keywords":[{"id":"3d34813f-73dd-460d-b3a0-cfae92332f10","keyword":"荧光光度法","originalKeyword":"荧光光度法"},{"id":"3cac8261-4681-44e0-8377-bda57cc8a985","keyword":"盐酸<span style=\"color:red\">左</span>氧氟沙星","originalKeyword":"盐酸左氧氟沙星"},{"id":"ce35d450-81d4-4d8d-9ca1-7a5019017325","keyword":"铕","originalKeyword":"铕"}],"language":"zh","publisherId":"xitu201102013","title":"铕-盐酸<span style=\"color:red\">左</span>氧氟沙星荧光光度法测定铕","volume":"32","year":"2011"},{"abstractinfo":"通过批试验研究了针铁矿存在时，<span style=\"color:red\">左</span>氧氟沙星对大肠杆菌的毒性效应以及吸附态的<span style=\"color:red\">左</span>氧氟沙星对微生物生长的影响．结果表明，中性条件下存在培养基时，<span style=\"color:red\">左</span>氧氟沙星在针铁矿上4h可达到吸附平衡，吸附等温线符合Freundlich吸附方程，傅里叶变换红外光谱分析得出<span style=\"color:red\">左</span>氧氟沙星的羧酸基团和酮基基团与针铁矿表面发生络合作用；0．016 g针铁矿的存在一定程度上能够促进大肠杆菌的生长（约50％），随着针铁矿含量的变化（0—0．1 g），在扣除其生长促进的影响后<span style=\"color:red\">左</span>氧氟沙星对大肠杆菌的毒性作用仍显著减弱，由90％降低至60％．","authors":[{"authorName":"王阳","id":"7d6c41c9-345e-420f-a814-b8832eb8f0bf","originalAuthorName":"王阳"},{"authorName":"刘菲","id":"ae526858-645f-4767-83cb-7549ed896bb3","originalAuthorName":"刘菲"},{"authorName":"秦晓鹏","id":"0ab2a482-6ee8-49cf-a09f-2593f089572f","originalAuthorName":"秦晓鹏"},{"authorName":"李璐","id":"0aaf8f62-05e0-4c70-9424-6ed57d846cb6","originalAuthorName":"李璐"},{"authorName":"李晋阳","id":"c71a6918-f34d-4f2f-9444-48821a0435df","originalAuthorName":"李晋阳"}],"doi":"10.7524/j.issn.0254-6108.2015.05.2014081206","fpage":"891","id":"4bfa43cc-f866-4f57-b6eb-93c8459a310d","issue":"5","journal":{"abbrevTitle":"HJHX","coverImgSrc":"journal/img/cover/HJHX.jpg","id":"43","issnPpub":"0254-6108","publisherId":"HJHX","title":"环境化学   "},"keywords":[{"id":"759b1319-79ab-470a-937e-f04b65a1485d","keyword":"针铁矿","originalKeyword":"针铁矿"},{"id":"a28b1fac-52ea-4fea-905c-211936142af0","keyword":"<span style=\"color:red\">左</span>氧氟沙星","originalKeyword":"左氧氟沙星"},{"id":"ab1fcdf2-9d8b-437b-aa43-2f646b42cb37","keyword":"大肠杆菌","originalKeyword":"大肠杆菌"},{"id":"e76dd196-646a-4ec0-a6ec-6990d28d566a","keyword":"吸附","originalKeyword":"吸附"}],"language":"zh","publisherId":"hjhx201505010","title":"<span style=\"color:red\">左</span>氧氟沙星在针铁矿-溶液体系存在形态对大肠杆菌的毒性效应?","volume":"","year":"2015"},{"abstractinfo":"当前市场上的药品种类繁多,因此对不同厂商的同类药品进行识别分析对规范医药市场及保障人民用药安全有重要现实意义.实验采用基于傅里叶变换近红外漫反射光谱的光谱判别分析方法,结合矢量归一化方法和导数方法对光谱进行预处理,对不同品牌的盐酸<span style=\"color:red\">左</span>西替利嗪片建立定性识别模型,并用验证集样品对模型进行验证.验证结果表明,通过光谱库判别分析法建立识别模型不能正确识别同一厂家的两种样品,但对不同厂家盐酸<span style=\"color:red\">左</span>西替利嗪片的识别正确率为100％,该方法可以用于不同企业同类药品的快速定性识别和质量控制.","authors":[{"authorName":"陈芬芬","id":"705b1107-5dae-4531-bcf4-0141d7c3127d","originalAuthorName":"陈芬芬"},{"authorName":"高闽光","id":"1beaef1e-ebf7-4d41-afed-19e96bec1e01","originalAuthorName":"高闽光"},{"authorName":"徐亮","id":"1c41c0cf-20e8-4681-a753-62790ce1e5e0","originalAuthorName":"徐亮"}],"doi":"10.3969/j.issn.1007-5461.2015.01.001","fpage":"1","id":"4f0d7845-56e0-4621-bbe8-ea35e9d4dade","issue":"1","journal":{"abbrevTitle":"LZ","coverImgSrc":"journal/img/cover/LZ.jpg","id":"52","issnPpub":"1005-4006","publisherId":"LZ","title":"连铸"},"keywords":[{"id":"b58adcc7-9575-4ab6-b999-f1c29cc0f92e","keyword":"傅里叶光学","originalKeyword":"傅里叶光学"},{"id":"1793d2e0-459e-4115-82a7-7957a5f699aa","keyword":"近红外光谱","originalKeyword":"近红外光谱"},{"id":"522c8900-450d-495a-b13a-fa27f1b60434","keyword":"盐酸<span style=\"color:red\">左</span>西替利嗪片","originalKeyword":"盐酸左西替利嗪片"},{"id":"a23d1490-1301-463e-bae3-56b028df64ed","keyword":"判别分析","originalKeyword":"判别分析"},{"id":"0eb96020-460d-4dad-8ea0-094844afba0e","keyword":"快速鉴别","originalKeyword":"快速鉴别"}],"language":"zh","publisherId":"lzdzxb201501001","title":"基于近红外漫反射光谱的盐酸<span style=\"color:red\">左</span>西替利嗪片判别分析","volume":"32","year":"2015"},{"abstractinfo":"　　根据某车型<span style=\"color:red\">左</span>/右车门内板的工艺特点，制定不同的工艺补充面模型，采用冲压模拟分析软件AUTOFORM对其拉延成形进行数值模拟，通过对零件可成形性分析图和零件变薄量图的分析、比较及工艺补充部分的调整，得到优化的拉延件型面，最终生产出合格产品。实践证明，该模拟分析结果可靠、准确，为同类型产品零件的生产起到指导作用。","authors":[{"authorName":"张玉平","id":"1d97f5f5-ff61-4161-96c3-88415249364a","originalAuthorName":"张玉平"}],"doi":"","fpage":"96","id":"de023cde-0238-4768-b677-8bed162753d3","issue":"3","journal":{"abbrevTitle":"BQCLKXYGC","coverImgSrc":"journal/img/cover/BQCLKXYGC.jpg","id":"4","issnPpub":"1004-244X","publisherId":"BQCLKXYGC","title":"兵器材料科学与工程   "},"keywords":[{"id":"4af19b98-9c73-47e6-8745-646f47b977e9","keyword":"<span style=\"color:red\">左</span>/右车门内板","originalKeyword":"左/右车门内板"},{"id":"1a4e98db-8af1-42c9-8699-ff456534ba84","keyword":"工艺补充面","originalKeyword":"工艺补充面"},{"id":"f69ed88b-1779-4b32-8bfa-c8fe1aa47797","keyword":"数值模拟","originalKeyword":"数值模拟"},{"id":"f2bafa2b-3c10-4987-b293-efceaf433944","keyword":"可成形性分析图","originalKeyword":"可成形性分析图"},{"id":"0c6a8206-f7ff-4016-b90e-3b91f180a641","keyword":"零件变薄量图","originalKeyword":"零件变薄量图"}],"language":"zh","publisherId":"bqclkxygc201303036","title":"某车型<span style=\"color:red\">左</span>/右车门内板的成形分析及有限元模拟","volume":"","year":"2013"},{"abstractinfo":"建立了同时测定加味<span style=\"color:red\">左</span>金丸中9种药效成分含量的超高效液相色谱-串联质谱(UPLC-MS/MS)分析方法.采用Zorbax RRHD Eclipse Plus C18色谱柱,以含0.2％甲酸的水-甲醇为流动相进行梯度洗脱,流速0.4 mL/min,在电喷雾电离(ESI)正离子模式下,采用多重反应监测模式进行检测.结果表明,芍药苷、延胡索乙素、药根碱、小檗碱、巴马汀、吴茱萸碱、柴胡皂苷C、柴胡皂苷A、柴胡皂苷D的线性范围分别为0.025～5.0 mg/L、0.0010～2.0mg/L、0.0023 ～ 7.2 mg/L、0.0027 ～ 28.9 mg/L、0.0023 ～9.1 mg/L、0.0050 ～1.0 mg/L、0.050～10 mg/L、0.005～ 1.0 mg/L、0.0075 ～ 1.5 mg/L;检出限分别为5.0、0.20、0.45、0.54、0.45、1.0、10、1.0、1.5μg/L.9种成分的加样回收率为99.3％ ～105％,相对标准偏差均不大于2.6％.该法快捷、准确、重复性好,已成功用于实际样品的分析.","authors":[{"authorName":"覃莎","id":"dad25592-6c5c-4d24-a378-a4f48659e050","originalAuthorName":"覃莎"},{"authorName":"王锦","id":"48a400a0-08e7-4453-bec8-abb9f2158508","originalAuthorName":"王锦"},{"authorName":"徐远金","id":"c516b077-e2a5-4ed2-8673-475924733978","originalAuthorName":"徐远金"}],"doi":"10.3724/SP.J.1123.2012.06040","fpage":"1153","id":"1239535c-d9b9-458c-9da5-3d901d2cda1d","issue":"11","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"f8421728-4984-48c4-876f-07a33d0ebe9d","keyword":"超高效液相色谱-串联质谱(UPLC-MS/MS)","originalKeyword":"超高效液相色谱-串联质谱(UPLC-MS/MS)"},{"id":"677d73b2-e2b3-4bbe-91fc-ef09755357ba","keyword":"有效成分","originalKeyword":"有效成分"},{"id":"7fac8bc1-5ab1-456d-b9b0-b0128d8db1f6","keyword":"加味<span style=\"color:red\">左</span>金丸","originalKeyword":"加味左金丸"},{"id":"fed55cd2-b252-4365-a08e-8d3bbab3d5df","keyword":"中成药","originalKeyword":"中成药"}],"language":"zh","publisherId":"sp201211011","title":"超高效液相色谱-串联质谱同时测定加味<span style=\"color:red\">左</span>金丸中的9种有效成分","volume":"30","year":"2012"}],"totalpage":6,"totalrecord":57}