Mustafa BOZ
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Adem KURT
材料科学技术（英文）
Friction-wear properties of the ZrSiO4 reinforced samples were measured and compared with those of plain bronze based ones. For this purpose, density, hardness, friction coefficient wear behaviour of the samples were tested. Microstructures of samples before and after sintering and worn surfaces were also investigated by scanning electron microscopy (SEM), and the wear types were determined. The optimum friction-wear behaviour was obtained in the sample compacted at 500 MPa and sintered at 820oC. Density of the final samples decreased with increasing the amount of reinforcing elements (ZrSiO4) before pre-sintering. However after sintering, there is no change in density of the samples including reinforcing elements (ZrSiO4). With increasing friction surface temperature, a reduction in the friction coefficient of the samples was observed. However, the highest reductions in the friction coefficients were observed in the as-received samples containing 0, 5% reinforced ZrSiO4. The SEM images of the sample indicated that while bronze-based break lining material without ZrSiO4showed abrasive wear behaviour, increasing the amount of ZrSiO4resulted a change in abrasive to adhesive wear mechanism. All samples exhibited friction-wear values, which were within the values shown in SAE-J661 standard. With increasing the amount of reinforcing ZrSiO4, wear resistance of the samples was increased. However samples reinforced with 5% and 6% ZrSiO4showed the best results.
关键词:
Friction materials
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Juxian ZHANG
,
Jinjun FENG
,
Longqiao GAO
材料科学技术（英文）
The sintering additives such as Al2O3 and/or Y2O3 were coated on the surfaces of Si3N4 particles via heterogeneous nucleation processing using a buffered pH solution as the precipitation reagent. They nucleated and grew only on the surfaces of Si3N4 and did not form sol particles in solution by TEM observation. The isoelectric point (IEP) of coated Si3N4 was different from that of as-received Si3N4. The IEP of Al(OH)3-coated Si3N4 occurred at pH8.4, which is close to that of alumina. When Al(OH)3-coated Si3N4 particles were coated with Y(OH)3, the IEP of coated Si3N4 powder shifted from pH8.4 to pH9.2, similar to that of yttria. In addition, the rheological data showed that Al2O3 and/or Y2O3 coated Si3N4 suspension is nearly Newtonian and that added Si3N4 suspension shows a shear rate thinning behavior.
关键词:
Si3N4 powder
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