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Effect of Compressive Deformation on Lenticular and Thin Plate Martensitic Transformations

ZHA NG Xiumu QI Yan ZHONG Jiaxiang GUO Yunyi ** Institute of Metal Research , Academia Sinica , Shenyang , 110015 , China.Beijing University of Science and Technology , Beijing , 100081 , China. To whom correspondence should be addressed.

材料科学技术(英文)

The effect of compressive deformation tested above the M_s temperature on the martensite morphology in Fe-Ni-C alloys has been studied.In the Fe-30Ni-0.12C alloy,the M_s temperature is -50℃ The cylindrical specimens were compressively deformed at -40℃.The strain rates were 10,20,30 and 40%.X-ray analysis and metallographic examination showed that no strain-induced martensite was found.After quench- ing to -53℃,some thin plates and unusual morphologies of lenticular martensites with bent and/or broken mid-ribs were observed.In the Fe-30Ni-0.34C alloy,the M_s temperature is -120℃.Compressive deformation with different strain rates were carried out at room temperature. After quenching to the liquid nitrogen temperature, some bent thin plate matensites(unbroken)occur- red.The transformed twins in bent plate were also bent and nearly parallel to the γ-α'interfaces. Orientation relationship between austenite and bent martensite has been examined by means of trans- mission electron microscope.It was proved that these unusual morphologies are inherent in the compressive pre-deformed austenite.

关键词: martensitic transformation , null , null , null

MICROSTRUCTURE AND PROPERTIES OF SiC_w/6061Al COMPOSITE The Author is now with Institute of Metal Research,Academia Sinica,China

MA Zongyi YAO Zhongkai Harbin Institute of Technology , Harbin , China

金属学报(英文版)

The SiC_w/Al composite prepared by squeeze casting has a combination of superior room temperature specific strength and modulus together with excellent thermal properties.The extrusion can make an improvement on the strength and ductility of the composite from 582 MPa as squeeze casted up to 639 MPa,and on the transformation from isotropic to the anisotropic structure.This seems to be explained by the orientation of whiskers and the densification of dislocations in matrix.TEM observation indicates that the stacking fault is the usual planar defect on the SiC_w surface. composite;;SiC whisker;;Al alloy;;microstructure

关键词: composite , null , null , null

原生QI成核中间相炭微球的结构

王成扬 , 姜卉 , 李鹏 , 郑嘉明

新型炭材料 doi:10.3969/j.issn.1007-8827.2000.04.003

以含有原生QI的煤沥青为原料,采用热缩聚方法制备出中间相炭微球.用扫描电子显微镜(SEM)观察了中间相炭微球的形貌和断面结构.经初步判断,在实验条件下原生QI成核煤沥青基中间相炭微球更倾向于"地球仪" 型结构.并对以QI为核形成中间相微球的过程进行了分析.

关键词: 原生喹啉不溶物 , 中间相炭微球 , 结构

Technical note: Research and development of localized corrosion rate monitoring instrument for nonpassivable metal in corrosive media

Corrosion

This paper introduces the design of a localized corrosion rate monitoring instrument that can monitor and evaluate the maximum and stable localized corrosion rate of a nonpassivable metal in a corrosive environment by measuring the current density in a corrosion sensor with an occluded anode.

关键词: instrument;localized corrosion rate;monitor

煤沥青原料中QI含量对中间相有序生长的影响

黄爱华 , 金鸣林 , 李和兴 , 房永征

材料导报

试验是以2种含不同QI的煤沥青为原料,采用变径反应管进行热转化反应制备有序性中间相的研究.试验采用偏光显微镜和扫描电镜(SEM)观察了原料各反应阶段的微观结构,考察了QI对热转化过程中中间相有序生长的影响,分析了热转化过程中软化点及族组分的变化.结果表明:少量的喹啉不溶物含量不会阻碍中间相有序的发展.高QI(2.03%)原料易生成镶嵌结构的中间相体,高温处理后样品呈轴状、短纤维、层片松散的石墨化焦结构;含低QI(0.11%)的原料能生成较好的、大区域的中间相体,域结构的中间相体在外力导向和内部裂解气流的作用下容易生成有序的半焦,高温处理后呈大区域、片层紧密、有序性强的细纤维焦结构.同时研究发现,在热转化过程中可通过测定软化点(SP)和TI含量来确定中间相转化程度.软化点约低于250℃、TI为75%左右时为初始中间相区域体形成阶段、半焦生成的前期.

关键词: 煤沥青 , 热转化反应 , 喹啉不溶物 , 中间相

T225NG和T42NG钛合金在水中的氧化行为和表面分析

于振涛 , 吴玮璐 , 李东 , 王兴旺 , 邱绍宇 , 周伟

稀有金属 doi:10.3969/j.issn.0258-7076.2004.01.015

研究了T225NG和T42NG钛合金在高温高压水蒸汽中腐蚀后的氧化膜形貌及结构特征. 测出了两种合金的氧化曲线, 并拟合出了其氧化动力学方程; 对试样表面进行了金相分析、表面形貌扫描电镜观察及X射线衍射分析. 结果表明: T225NG和T42NG合金的氧化动力学规律, 其中前者的耐蚀性明显优于T42NG合金. 经过高温高压水蒸汽腐蚀后, 在两种合金表面形成了均匀、致密的氧化膜, 且以金红石型TiO2为主, 并伴有少量的锐钛矿型TiO2形成; 还可观察到明显的氧化膜形核并长大的结晶学特征, 而两种合金的金相组织没有明显变化.

关键词: T225NG合金 , T42NG合金 , 氧化行为 , 表面分析

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