Xianghua LIU
,
Ge YAN
,
Liya CUI
,
Shaoxiong ZHOU
,
Wu ZHENG
,
Ailing WANG
,
Jinchang CHEN
材料科学技术（英文）
Sm22Co78/Fe65Co35/Sm22Co78/Fe65Co35 multilayer films were prepared by magnetron sputtering. The temperature dependence of coercivity (H-c), remanence (M-r) and reduced remanence (M-r/M-s) has been measured. The coercivity decreases with increasing of temperature. The remanence decreases with increasing the temperature from 26 to 100 degrees C, and then increases with continuously increasing the temperature from 100 to 150 degrees C. The reduced remanence increases with increasing the temperature.
关键词:
Fengli SUI
,
Liqing CHEN
,
Xianghua LIU
,
Lintao WANG
,
Wei LI
金属学报(英文版)
doi:10.1016/S1006-7191(08)60074-5
A coupled thermo-mechanical model containing metal flow and temperature field for calculating temperature variation has been developed on fourteen-pass hot continuous rolling of round rod for Inconel 718 alloy using 3D elastic-plastic finite element method (FEM). The temperature of characteristic analysis points in the intermediate cross-section of the workpiece has been simulated at initial temperature ranging from 960 to 1000 ℃ and initial velocity in range of 0.15-0.55 m．s-1. Based on finite element analysis and microstructural observation in cylindrical hot compression experiments, the appropriate hot continuous rolling technologies have been designed for rod products with different diameters. For a real rolling practice, the simulated surface temperature was examined and is in good agreement with the measured one.
关键词:
Hot continuous rolling
,
null
,
null
,
null
,
null
Shengjie YAO
,
Shengjie YAO
,
Xianghua LIU
,
Guodong WANG
金属学报(英文版)
doi:10.1016/S1006-7191(08)60064-2
Ultrafine austenite grains (UFAGs) with size of 1-5 μm were prepared through repetitive treatment, four times, of rapid heating and quenching, and the growth behaviors of these UFAGs during both the reheating and cooling stages were investigated. The results indicated that UFAGs without pinning particles appeared with significant coarsening when the reheating temperature reached 1000℃. Although coarsening still occurred in the cooling stage, the growth was obscured during the isothermal holding process at temperatures between 900 ℃ and Ar3
关键词:
Ultrafine austenite grain
,
null
,
null
,
null
Huawei ZHANG
,
Lizhong LIU
,
Ping HU
,
Xianghua LIU
金属学报(英文版)
Residual stress developed during the rolling process of tailor rolled blank (TRB) can affect the springback of finished parts considerably. Springback characteristics of unannealed and annealed TRBs were investigated by means of numerical simulation and experiments taking U-Channel as an example. TRBs were annealed by the annealing process (700℃, holding time 10h), then stamping and springback processes of unannealed and annealed TRBs were simulated, and corresponding experiments were also carried out. Effects of the transition zone length, the blank thickness, the friction coefficient and the die clearance on the springback of TRB were analyzed. The results demonstrate that the springback of TRB annealed at 700℃ for 10 h reduces significantly. For unannealed and annealed U-Channels, the springback of TRB U-Channel is in direct proportion to the die clearance and is in inverse proportion to the transition zone length, the blank thickness and the friction coefficient. Springbacks of the thinner monolithic (uniform thickness) blank, the thinner side of TRB, the thicker side of TRB and the thicker monolithic blank are sorted in descending order.
关键词:
Tailor rolled blank
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null
,
null
徐卫兵
,
戈明亮
,
何平笙
应用化学
doi:10.3969/j.issn.1000-0518.2001.09.011
用熔融插层法制备聚甲醛/蒙脱土纳米复合材料,用X射线衍射研究聚甲醛及复合材料的微观结构,表明复合材料是纳米复合材料.用DSC法研究其非等温结晶行为,对所得数据分别用Jeziorny法、Ozawa法和Liu法进行处理.结果表明,Jeziorny法和Liu法处理非等温结晶过程比较理想.聚甲醛及聚甲醛/有机蒙脱土纳米复合材料的结晶活化能分别为334.6和196.9 kJ/mol,说明有机蒙脱土的加入,降低了聚甲醛的结晶活化能,且t1/z缩短,起到了异相成核的作用.
关键词:
聚甲醛
,
蒙脱土
,
纳米复合材料
,
非等温结晶动力学
王平华
,
徐国永
应用化学
doi:10.3969/j.issn.1000-0518.2004.08.007
用熔融复合法制备聚丙烯/凹凸棒土纳米复合材料,用DSC法研究其非等温结晶行为,对所得的数据分别用Jeziorny法、Ozawa法和Liu法进行处理.结果表明,Jeziorny法和Liu法处理非等温结晶过程比较理想.聚丙烯及聚丙烯/凹凸棒土纳米复合材料的结晶活化能分别为194.1和162.8 kJ/mol,表明凹凸棒土的加入,降低了聚丙烯的结晶活化能,且t1/2缩短,起到了异相成核作用.
关键词:
聚丙烯
,
凹凸棒土
,
纳米复合材料
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非等温结晶动力学
Scripta Materialia
A recent comment on a previously published paper addressed the invalid explanation of the off diagonal interdiflusion coefficients of the beta-Ni(Al,Cr) phase in the Ni-Cr-Al system according to the symmetric property of the thermodynamic matrix. In this paper, the experimental data presented by Hou et al. was reanalyzed and the interdiffusion coefficient matrix was estimated again. The results of the analysis have been discussed in terms of a brief reply to the comments of Liu and Liang. (C) 2010 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.
关键词:
Diffusion;Intermetallic compound;Ni-Cr-Al
邓超
,
邵玮
,
李春忠
高分子材料科学与工程
采用元机纳米锑掺杂二氧化锡(ATO)和有机聚醚酯(PEE)协同提高聚时苯二甲酸乙二酯(PET)的抗静电性能,合成了聚对苯二甲酸乙二酯-聚醚酯/锑掺杂二氧化锡纳米复合材料(PET-PEE/ATO).使用Czawa方程和Liu-Mo方程研究了PET-PEE/ATO纳米复合材料的非等温结晶过程.Ozawa方程研究发现,在非等温结晶过程中,PET、PET-PEE、PET/ATO、PET-PEE/ATO的成核性能依次提高.Liu-Mo方程发现,ATO和PEE的加入分别促进了异相成核作用和加快了结晶生长,PET-PEE/ATO结晶成核性能最好,结晶速率最快.
关键词:
聚对苯二甲酸乙二酯
,
有机聚醚酯
,
无机纳米锑掺杂二氧化锡
,
纳米复合材料
,
非等温结晶动力学
王浩
,
刘国权
金属学报
doi:10.3321/j.issn:0412-1961.2008.07.001
以MacPherson-Srolovitz提出的三维个体晶粒长大拓扑依赖速率方程以及三维晶粒组织的晶粒尺寸-晶粒面数间的抛物线型统计关系为基础,导出了相应的描述三维准稳态晶粒尺寸分布的函数族.采用纯Fe实验数据以及顶点法、基元演化法.相场模型和Monte Carlo法进行了验证,结果表明,函数族中峰值左偏的函数适合三维准稳态晶粒尺寸分布的定量表述.将该函数与Liu等提出的2种三维准稳态晶粒尺寸分布函数进行的对比表明:此3种函数的解析表达形式有所不同,但其曲线图在一定条件下相互吻合.此外,MacPherson-Srolovitz三维拓扑依赖速率方程、Hillert三维速率方程及Yu-Liu三维速率方程尽管表达形式不同均能较好地反映三维正常晶粒长大的动力学规律.
关键词:
三维晶粒长大
,
准稳态晶粒尺寸分布
,
长大速率方程
,
计算机仿真
