{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"以膨胀珍珠岩为载体,TiOSO4为钛源,采用均匀沉淀法制备了纳米TiO2/膨胀珍珠岩复合材料,通过SEM、TEM、XRD和BET比表面积法进行了分析表征,并以罗丹明B溶液为降解对象研究其光催化性能.结果表明随着TiOSO4加入量的增加,复合材料的TiO2负载量和比表面积越来越大,而光催化性能先升高后降低.当TiO2负载量为15.27％时光催化性能最好,此时纳米TiO2颗粒在膨胀珍珠岩表面均匀致密分布成一层薄膜,TiO2晶粒尺寸为11.93nm,经300 W高压汞灯照射60 min时对罗丹明B溶液的降解率超过95％,达到了与P25相同的降解效果.","authors":[{"authorName":"<span style=\"color:red\">徐</span><span style=\"color:red\">春</span><span style=\"color:red\">宏</span>","id":"693f79c7-ff14-4de2-9510-ae9452fbbfff","originalAuthorName":"徐春宏"},{"authorName":"郑水林","id":"c769172e-f548-42fc-a262-7fbeed6ab735","originalAuthorName":"郑水林"},{"authorName":"张广心","id":"77fc54ac-dc86-446c-9179-579a4c5fefe6","originalAuthorName":"张广心"},{"authorName":"孙青","id":"56e43343-b7af-462e-9c34-3323efe23dfa","originalAuthorName":"孙青"}],"doi":"","fpage":"1991","id":"1343e007-5621-43b3-8be6-7254bbc2c81f","issue":"8","journal":{"abbrevTitle":"RGJTXB","coverImgSrc":"journal/img/cover/RGJTXB.jpg","id":"57","issnPpub":"1000-985X","publisherId":"RGJTXB","title":"人工晶体学报"},"keywords":[{"id":"e4342fbd-e27c-499f-9ef0-a79fa37a8cfc","keyword":"膨胀珍珠岩","originalKeyword":"膨胀珍珠岩"},{"id":"72f2f737-b0e9-4991-bb9e-92759213d366","keyword":"纳米TiO2","originalKeyword":"纳米TiO2"},{"id":"a5b03323-8587-4c01-b69d-7c5911f21956","keyword":"光催化","originalKeyword":"光催化"},{"id":"d9db5602-0db0-48e7-b5a3-ba135bec6a4a","keyword":"均匀沉淀法","originalKeyword":"均匀沉淀法"}],"language":"zh","publisherId":"rgjtxb98201408020","title":"均匀沉淀法制备纳米TiO2/膨胀珍珠岩复合材料","volume":"43","year":"2014"},{"abstractinfo":"为研究循环荷载加大混凝土<span style=\"color:red\">徐</span>变的内因,以循环荷载和恒荷载下混凝土<span style=\"color:red\">徐</span>变试验结果为基础,基于多孔介质理论的混凝土<span style=\"color:red\">徐</span>变模型,编制了<span style=\"color:red\">徐</span>变模拟分析程序,在细观尺度下模拟了受循环荷载作用的混凝土内部骨料、砂浆与水的耦合过程,得到了宏观尺度下模型内部节点位移过程图、细观尺度下水分流速分布图、孔隙压力消散过程图、等效应力变化图.研究结果表明:(1)数值模拟方法可以描述细观尺度下混凝土内部骨料、砂浆、水分的运动规律;(2)与恒定荷载相比,循环荷载通过影响水分的运动,加快了骨料与砂浆的内力重分布速度,推进了混凝土固相的受力均匀化的过程,从而加大混凝土<span style=\"color:red\">徐</span>变.","authors":[{"authorName":"陈松","id":"034eeaf3-83ef-4673-8863-8ee62234b05d","originalAuthorName":"陈松"},{"authorName":"王岩","id":"a7a90936-4fb9-4bc5-bae1-8ce23f6149d8","originalAuthorName":"王岩"},{"authorName":"宁聪","id":"8f449774-d9c0-4cbf-817e-1de8b8966199","originalAuthorName":"宁聪"}],"doi":"10.11896/j.issn.1005-023X.2016.12.033","fpage":"153","id":"2933bac8-737f-4c7d-9bb6-3960f355bb51","issue":"12","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"3bb3aa08-d7a7-49ac-b103-683cb5cd4d9e","keyword":"混凝土<span style=\"color:red\">徐</span>变","originalKeyword":"混凝土徐变"},{"id":"c13a4ddb-bfc2-4a81-82ac-6c21892ba7a1","keyword":"<span style=\"color:red\">宏</span>细观","originalKeyword":"宏细观"},{"id":"09654dbd-cb5d-4225-b789-121fbbd66527","keyword":"数值模拟","originalKeyword":"数值模拟"},{"id":"b9346fbd-41e4-448b-b14e-a5ce67de0e1f","keyword":"循环荷载","originalKeyword":"循环荷载"}],"language":"zh","publisherId":"cldb201612033","title":"循环荷载下混凝土<span style=\"color:red\">徐</span>变特性的<span style=\"color:red\">宏</span>细观分析","volume":"30","year":"2016"},{"abstractinfo":"以膨胀珍珠岩为载体,TiOSO4为钛源,采用均匀沉淀法制备了纳米TiO2/膨胀珍珠岩复合材料,通过XRD、SEM和FT-IR对复合材料的TiO2晶体结构、表面性质和形貌进行分析表征.研究了煅烧温度和煅烧时间对复合材料中TiO2结晶和光催化性能的影响.结果显示在550℃下煅烧2h时,复合材料的光催化性能最高,此时TiO2为锐钛矿,晶粒尺寸为11.93 nm,对罗丹明溶液的降解率达到95％以上.复合材料具有良好的再生重复使用性能,经5次回收再利用后仍表现较高的光催化性能.","authors":[{"authorName":"<span style=\"color:red\">徐</span><span style=\"color:red\">春</span><span style=\"color:red\">宏</span>","id":"6b2c2b07-5521-45cb-9443-45bdd60e93bd","originalAuthorName":"徐春宏"},{"authorName":"郑水林","id":"5960c223-68e6-430a-8fc0-43546e19a7ab","originalAuthorName":"郑水林"},{"authorName":"胡志波","id":"7a3ee3d7-1254-48a6-abb9-82c08bd0d176","originalAuthorName":"胡志波"}],"doi":"","fpage":"2022","id":"293d9087-f70a-4769-913b-38bf937a3413","issue":"8","journal":{"abbrevTitle":"RGJTXB","coverImgSrc":"journal/img/cover/RGJTXB.jpg","id":"57","issnPpub":"1000-985X","publisherId":"RGJTXB","title":"人工晶体学报"},"keywords":[{"id":"11f229cf-59a0-4338-bfdf-8fbbdd7b34c5","keyword":"膨胀珍珠岩","originalKeyword":"膨胀珍珠岩"},{"id":"097a25b7-297d-4427-b711-f3bee965021b","keyword":"纳米TiO2","originalKeyword":"纳米TiO2"},{"id":"afaba031-7e42-4757-981c-0a9a99917d2b","keyword":"均匀沉淀法","originalKeyword":"均匀沉淀法"},{"id":"b3bab3f7-ec81-4d32-a305-3c1adda3bccc","keyword":"光催化","originalKeyword":"光催化"}],"language":"zh","publisherId":"rgjtxb98201408025","title":"煅烧条件对纳米TiO2/膨胀珍珠岩复合材料性能的影响","volume":"43","year":"2014"},{"abstractinfo":"采用Chiralpak IC手性柱(250 mm×4.6 mm,5 μm),建立了正相高效液相色谱测定板蓝根中表告依<span style=\"color:red\">春</span>(R-告依<span style=\"color:red\">春</span>)和告依<span style=\"color:red\">春</span>(S-告依<span style=\"color:red\">春</span>)含量的方法.考察了流动相组成、流速和柱温对分离度的影响.经优化后的实验条件:以正己烷-异丙醇(体积比为90∶10)为流动相,流速为0.8 mL/min;检测波长为245 nm,柱温为20 ℃.在此优化条件下,表告依<span style=\"color:red\">春</span>和告依春分离度为3.4,检出限为2.0 mg/L,在0.02～2.0 g/L 范围内有良好的线性关系,平均回收率为101% ,相对标准偏差(RSD)小于3.0%(n=6).本方法可将具有抗病毒活性的表告依<span style=\"color:red\">春</span>与其对映体告依<span style=\"color:red\">春</span>基线分离并测定,专属性强,能有效控制板蓝根的质量.","authors":[{"authorName":"聂黎行","id":"fee7f0b1-4bfd-4c4e-9d65-d7f03c2a918a","originalAuthorName":"聂黎行"},{"authorName":"王钢力","id":"ee281225-e77f-4477-a486-a098ca91b1db","originalAuthorName":"王钢力"},{"authorName":"戴忠","id":"813e1426-d061-4e41-9723-d75cfa16968e","originalAuthorName":"戴忠"},{"authorName":"林瑞超","id":"3034f33a-eaf2-4665-8751-f5ef70c65379","originalAuthorName":"林瑞超"}],"doi":"10.3724/SP.J.1123.2010.01001","fpage":"1001","id":"32355b8f-ccce-4726-b210-eaacc0917986","issue":"10","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"5c41c71f-d053-43ba-8aa9-32ad96d3cca4","keyword":"手性高效液相色谱法","originalKeyword":"手性高效液相色谱法"},{"id":"e26a591e-56ec-4bb4-acfd-5d5f7ad919ea","keyword":"表告依<span style=\"color:red\">春</span>(R-告依<span style=\"color:red\">春</span>)","originalKeyword":"表告依春(R-告依春)"},{"id":"1e32ab35-876b-46d9-9898-47fb5c40d701","keyword":"告依<span style=\"color:red\">春</span>(S-告依<span style=\"color:red\">春</span>)","originalKeyword":"告依春(S-告依春)"},{"id":"8c1b4600-8fac-47f6-98f6-6670e2a0daa9","keyword":"板蓝根","originalKeyword":"板蓝根"}],"language":"zh","publisherId":"sp201010018","title":"手性高效液相色谱法测定板蓝根中表告依<span style=\"color:red\">春</span>和告依<span style=\"color:red\">春</span>含量","volume":"28","year":"2010"},{"abstractinfo":"单轴、双轴和三轴<span style=\"color:red\">徐</span>变试验结果表明,混凝土的<span style=\"color:red\">徐</span>变与弹性变形一样具有空间特性,但根据单轴<span style=\"color:red\">徐</span>变试验得到的<span style=\"color:red\">徐</span>变系数、<span style=\"color:red\">徐</span>变泊松比以及采用叠加原理计算的双轴、三轴应力状态下的空间<span style=\"color:red\">徐</span>变与实际情况存在较大偏差.为了准确计算不同应力状态下混凝土的空间<span style=\"color:red\">徐</span>变,介绍了应力组合对有效<span style=\"color:red\">徐</span>变泊松比的影响和基于有效<span style=\"color:red\">徐</span>变泊松比的空间<span style=\"color:red\">徐</span>变计算方法.另外,根据应力张量的弹性力学意义,引入了球应力<span style=\"color:red\">徐</span>变系数(ψ)m和偏应力<span style=\"color:red\">徐</span>变系数(ψ) d,提出了基于这两个<span style=\"color:red\">徐</span>变系数的空间<span style=\"color:red\">徐</span>变计算统一表达式,可计算混凝土在单轴、双轴和三轴等不同应力状态下的空间<span style=\"color:red\">徐</span>变.","authors":[{"authorName":"黄胜前","id":"f60fe1e8-6699-466b-8f2e-355e391d0c51","originalAuthorName":"黄胜前"},{"authorName":"杨永清","id":"0ad9d4be-4c12-4497-a380-8dee2c8f7ad4","originalAuthorName":"杨永清"},{"authorName":"李晓斌","id":"a5e2e801-c9b9-4f4b-886e-c62ae3c23491","originalAuthorName":"李晓斌"},{"authorName":"陈志伟","id":"db16b3f8-4c53-49d7-bdd3-f6cf5f2247c1","originalAuthorName":"陈志伟"}],"doi":"","fpage":"150","id":"77593762-6ffb-4cfa-913f-f64ffef2186c","issue":"2","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"69ea1570-d4c9-437e-bfef-97ae77a244a5","keyword":"混凝土","originalKeyword":"混凝土"},{"id":"9785e9c9-1fc1-4ea3-ab52-a37f97e3f32e","keyword":"单轴","originalKeyword":"单轴"},{"id":"4565bb1b-db4a-4cd3-8595-f4cc47900c42","keyword":"双轴","originalKeyword":"双轴"},{"id":"59877901-b9f9-4bd2-a23d-bca130502b51","keyword":"三轴","originalKeyword":"三轴"},{"id":"375cdb53-1ae1-4106-b024-cece1bb5b8eb","keyword":"应力状态","originalKeyword":"应力状态"},{"id":"2edbc816-e655-4662-9602-f0529134d608","keyword":"空间<span style=\"color:red\">徐</span>变","originalKeyword":"空间徐变"}],"language":"zh","publisherId":"cldb201302040","title":"不同应力状态下混凝土空间<span style=\"color:red\">徐</span>变的统一表达式","volume":"27","year":"2013"},{"abstractinfo":"为了研究不同配合比设计方法对再生混凝土长期<span style=\"color:red\">徐</span>变性能的影响,分别采用等体积砂浆法(EMV法)与传统替代法配制再生混凝土,测试各组再生混凝土试件28 d龄期后自然条件下持荷的变形值和相同试验条件下试件的收缩值,并计算各组试件的<span style=\"color:red\">徐</span>变度.研究结果表明:两种方法配制的再生混凝土的收缩<span style=\"color:red\">徐</span>变变化规律与对比普通混凝土相似.EMV法可有效改善再生混凝土的<span style=\"color:red\">徐</span>变性能,具有较低的<span style=\"color:red\">徐</span>变度.","authors":[{"authorName":"霍俊芳","id":"55188923-049c-49aa-994c-ac564398860f","originalAuthorName":"霍俊芳"},{"authorName":"李晨霞","id":"8fa10b03-f76b-44b4-97ee-bd67d36d407e","originalAuthorName":"李晨霞"},{"authorName":"侯永利","id":"83d612b7-ba2c-46d3-a2ff-d86f396b5f77","originalAuthorName":"侯永利"},{"authorName":"吕笑岩","id":"98dd9616-8bca-4990-9631-ef1c189dce52","originalAuthorName":"吕笑岩"}],"doi":"","fpage":"723","id":"dc2db04e-0a0c-4741-830f-d84f7a4e5aee","issue":"2","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报   "},"keywords":[{"id":"d2a7136a-24da-4dc5-b2c8-c753ce344b72","keyword":"再生混凝土","originalKeyword":"再生混凝土"},{"id":"46b36702-7dae-4dad-b1c2-1996ae105250","keyword":"配合比","originalKeyword":"配合比"},{"id":"69440820-bb2f-4272-abe2-bdc4edbd2d6e","keyword":"<span style=\"color:red\">徐</span>变","originalKeyword":"徐变"}],"language":"zh","publisherId":"gsytb201702054","title":"再生粗骨料混凝土收缩<span style=\"color:red\">徐</span>变性能试验","volume":"36","year":"2017"},{"abstractinfo":"利用铱催化高碘酸钾氧化丽<span style=\"color:red\">春</span>红G(PG)的褪色反应,建立了测定痕量铱的催化动力学光度法.在硫酸介质和90℃加热15min的条件下,于500nm波长处,采用固定时间法测定丽<span style=\"color:red\">春</span>红G吸收值的降低.Ir(Ⅳ)的浓度在0～1.0μg/25mL范围内与催化反应的速率有良好的线性关系,检出限为1 81 ×10 mg/mL.对0.3μg/25mLIr(Ⅳ)测定的相对标准偏差为1.61%(n=11).体系至少稳定3.5h.考察了40多种共存离子的影响,大多数常见离子不干扰,方法有较好的选择性.催化反应对Ir(Ⅳ)和丽<span style=\"color:red\">春</span>红G均为一级反应,催化反应的表观活化能为103.66kJ/mol.用于冶金产品及岩矿中铱的测定,结果与推荐值十分吻合.","authors":[{"authorName":"侯能邦","id":"92c62fdf-fec8-4163-aad2-9ed54b7fdce6","originalAuthorName":"侯能邦"},{"authorName":"李祖碧","id":"c4dacfbe-4824-4cbe-a844-91a76be4f69c","originalAuthorName":"李祖碧"},{"authorName":"李崇宁","id":"f7a10f8c-895c-486c-ad99-2b32db2c7164","originalAuthorName":"李崇宁"},{"authorName":"王加林","id":"6d15967f-b1aa-492c-9003-5900696277f5","originalAuthorName":"王加林"},{"authorName":"曹秋娥","id":"b89522cc-6338-40b9-bb28-a8fc73f09d40","originalAuthorName":"曹秋娥"}],"doi":"10.3969/j.issn.1000-7571.2002.05.006","fpage":"17","id":"cf8ee9a7-e782-4fcb-866c-e15d9126e60f","issue":"5","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"3c381e65-e813-4912-b9c8-15299a341a75","keyword":"铱","originalKeyword":"铱"},{"id":"90683ee6-f835-43a8-b573-bc0be1641329","keyword":"丽<span style=\"color:red\">春</span>红G","originalKeyword":"丽春红G"},{"id":"a2a57fdf-fa6d-4d5d-bc97-967b1b2de292","keyword":"高碘酸钾","originalKeyword":"高碘酸钾"},{"id":"4ffcfe3c-3af4-41cd-ae8f-447d4f037585","keyword":"催化光度法","originalKeyword":"催化光度法"}],"language":"zh","publisherId":"yjfx200205006","title":"高碘酸钾氧化丽<span style=\"color:red\">春</span>红G催化光度法测定铱","volume":"22","year":"2002"},{"abstractinfo":"采用砂土作为模拟土壤，通过失重法及电化学方法，研究了土壤盐浓差Ａ３钢的<span style=\"color:red\">宏</span>电池民腐蚀的影响规律。结果表明位于高盐土壤中的试样试验初期为<span style=\"color:red\">宏</span>电池阳极，而在第５天发生了极性逆转。　","authors":[{"authorName":"孙成","id":"fad53d26-8b5f-49e0-833b-04d86bc59f07","originalAuthorName":"孙成"},{"authorName":"李洪锡","id":"d9c6adad-694f-4c0f-bfe1-7b10d99e9dec","originalAuthorName":"李洪锡"},{"authorName":"张淑泉等","id":"318f7173-1276-4af4-93d0-409b388c169f","originalAuthorName":"张淑泉等"}],"categoryName":"|","doi":"","fpage":"101","id":"95a0908c-96bd-4cf5-8373-77ba2eda5a34","issue":"2","journal":{"abbrevTitle":"FSXB","coverImgSrc":"journal/img/cover/腐蚀学报封面.jpg","id":"24","issnPpub":"2667-2669","publisherId":"FSXB","title":"腐蚀学报（英文）"},"keywords":[{"id":"b0cf9065-4aea-40fc-8ba6-085cd4197a44","keyword":"碳钢","originalKeyword":"碳钢"},{"id":"a7ec12b9-aed6-44bf-bdc3-43ea8e43cfc8","keyword":"salt concernation in soil","originalKeyword":"salt concernation in soil"},{"id":"eaa98ff4-1a71-47df-8ad0-8680ec9b8d8e","keyword":"macrocell cornion","originalKeyword":"macrocell cornion"}],"language":"zh","publisherId":"1002-6495_2000_2_5","title":"土壤盐浓差<span style=\"color:red\">宏</span>电池对碳钢的腐蚀","volume":"12","year":"2000"},{"abstractinfo":"采用砂土作为模拟土壤,通过失重法及电化学方法,研究了土壤盐浓差对A3钢的<span style=\"color:red\">宏</span>电池腐蚀的影响规律.结果表明位于高盐土壤中的试样试验初期为<span style=\"color:red\">宏</span>电池阳极,而在第5 天发生了极性逆转.","authors":[{"authorName":"孙成","id":"6de82a3c-7871-46f6-80e2-4cd3ede997d0","originalAuthorName":"孙成"},{"authorName":"李洪锡","id":"5178d6b7-b30b-4d5f-abb8-36d24e0c2d27","originalAuthorName":"李洪锡"},{"authorName":"张淑泉","id":"9ec4e07e-1a37-46ee-a419-15611c940a62","originalAuthorName":"张淑泉"},{"authorName":"高立群","id":"a0520bef-d3fb-41f6-9480-1511ae90f247","originalAuthorName":"高立群"}],"doi":"10.3969/j.issn.1002-6495.2000.02.010","fpage":"101","id":"9584052e-0be4-4bd0-b182-6d32766f1812","issue":"2","journal":{"abbrevTitle":"FSXB","coverImgSrc":"journal/img/cover/腐蚀学报封面.jpg","id":"24","issnPpub":"2667-2669","publisherId":"FSXB","title":"腐蚀学报（英文）"},"keywords":[{"id":"94335ec0-11e8-4b6a-ab8e-a8be9b6685e3","keyword":"碳钢","originalKeyword":"碳钢"},{"id":"98b42eb4-64b9-4a06-a5ce-a907f37ee9b2","keyword":"土壤盐浓差","originalKeyword":"土壤盐浓差"},{"id":"1189b6f3-4a3d-4c81-9f5b-3376383c26dd","keyword":"<span style=\"color:red\">宏</span>电池腐蚀","originalKeyword":"宏电池腐蚀"}],"language":"zh","publisherId":"fskxyfhjs200002010","title":"土壤盐浓差<span style=\"color:red\">宏</span>电池对碳钢的腐蚀","volume":"12","year":"2000"},{"abstractinfo":"本文阐述了FRP应力松弛、<span style=\"color:red\">徐</span>变性能的研究意义,总结了国内外关于应力松弛、<span style=\"color:red\">徐</span>变性能的最新研究成果及主要影响因素,并探讨了应力松弛和<span style=\"color:red\">徐</span>变的计算模型,对未来FRP长期性能研究的发展方向做出了展望.","authors":[{"authorName":"李建辉","id":"0f7148fe-f8bb-4e01-9827-43b6d6088f0a","originalAuthorName":"李建辉"},{"authorName":"邓宗才","id":"734ba4b3-500c-4ca4-adda-8e3a09ca07b3","originalAuthorName":"邓宗才"}],"doi":"10.3969/j.issn.1003-0999.2007.03.016","fpage":"56","id":"59ffbb46-47b1-40d6-8ec4-254b9f0174de","issue":"3","journal":{"abbrevTitle":"BLGFHCL","coverImgSrc":"journal/img/cover/BLGFHCL.jpg","id":"6","issnPpub":"1003-0999","publisherId":"BLGFHCL","title":"玻璃钢/复合材料"},"keywords":[{"id":"3192da00-b6fe-4a92-a3fe-eec5f9cca17e","keyword":"FRP","originalKeyword":"FRP"},{"id":"812f44d9-8adc-47b7-95e7-d14c2fe8670d","keyword":"应力松弛","originalKeyword":"应力松弛"},{"id":"37e0f5f2-7caa-403e-96f9-d45fa60555ee","keyword":"<span style=\"color:red\">徐</span>变","originalKeyword":"徐变"},{"id":"290bc541-6726-480e-a116-34147a7cb2ae","keyword":"前景展望","originalKeyword":"前景展望"}],"language":"zh","publisherId":"blgfhcl200703016","title":"FRP应力松弛及<span style=\"color:red\">徐</span>变性能的研究近展","volume":"","year":"2007"}],"totalpage":24,"totalrecord":240}