SONG Ren-bo
,
XIANG Jian-ying
,
HOU Dong-po
钢铁研究学报(英文版)
A comparative study on mechanical properties and microstructure of 316L austenitic stainless steel between solution treated specimen and hot rolled specimen was conducted. After a specimen was subjected to solution treatment at 1050 ℃ for 6 min, its mechanical properties were determined through tensile and hardness tests. Based on the true stress vs true strain and engineering stress vs engineering strain flow curves, the work hardening rate has been explored. The results show that the solution treated specimen has an excellent combination of strength and elongation, and that this steel is easy to work-hardening during deformation. Optical microscope, scanning electron microscope, transmission electron microscope and X-ray diffraction examinations were conducted, these reveal that twins in 316L austenitic stainless steel can be divided into suspended twin and transgranular twin which have different formation mechanisms in growth, and that the deformation induced martensite nucleated and grown in the shear band intersections can be observed, and that the fracture surfaces are mainly composed of dimples and exhibit a tough fracture character.
关键词:
316L
,
mechanical property
,
twin
,
martensite
,
fracture morphology
张麦仓
,
董建新
,
曾燕屏
,
谢锡善
,
罗子健
金属学报
利用热力耦合有限元程序FORMT,对PM René 95合金中等尺寸(外径尺寸约为630 mm)涡轮盘的等温锻造工艺进行了模拟式设计.结果表明,采用TZM钼基合金模具,在1050℃以接近10-3s.的应变速率进行闭式模锻和开式模锻,模具材料均能满足使用要求,且开式模锻设备最大载荷不超过31×103kN;采用K21合金模具,在1000℃以相同条件等温成形,模具材料因变形热效应及边界摩擦引起温升而失效且所需设备吨位相对较大.
关键词:
PM
,
null
,
null
,
null
张麦仓
,
董建新
,
曾燕屏
,
谢锡善
,
罗子健
金属学报
doi:10.3321/j.issn:0412-1961.2002.10.022
利用热力耦合有限元程序FORMT,对PM René 95合金中等尺寸(外径尺寸约为630 mm)涡轮盘的等温锻造工艺进行了模拟式设计.结果表明,采用TZM钼基合金模具,在1050℃以接近10-3s.的应变速率进行闭式模锻和开式模锻,模具材料均能满足使用要求,且开式模锻设备最大载荷不超过31×103kN;采用K21合金模具,在1000℃以相同条件等温成形,模具材料因变形热效应及边界摩擦引起温升而失效且所需设备吨位相对较大.
关键词:
PM René 95合金,等温锻造,热力耦合有限元,模拟式工艺设计
付锐
,
陈希春
,
任昊
,
冯涤
航空材料学报
doi:10.3969/j.issn.1005-5053.2011.3.002
自行设计开发了适合工业化生产高纯净,低偏析,无宏观缺陷铸锭的电渣重熔连续定向凝固技术(ESR-CDS)的设备和工艺,利用该技术成功制备了直径为φ150mm的René88DT合金定向凝周铸锭.采用XRD测试了定向凝固柱状晶的生长取向,结果表明,ESR-CDS René88DT铸锭柱状晶择优生长方向为<100>系晶向;ERS-CDS铸锭与传统ESR铸锭相比,枝晶组织生长方向保持一致,二次枝晶臂均匀细小,元素偏析程度低,且晶间一次析出相呈颗粒状,尺寸细小;等温热压缩实验结果表明,ESR-CDS René88DT合金热压缩试样在1100℃,0.0-50.1s-1应变速率下可达到70%以上压缩变形量并获得均匀细小的动态再结晶组织;ESR-CDS René88DT合金铸锭经等温锻造制备出了φ170mm×73mm的饼坯件,锻压变形量超过70%,饼坯件除上下两端的变形死区外均发生了动态再结晶,晶粒尺寸约50μm.
关键词:
电渣重熔连续定向凝固
,
热变形
,
动态再结晶
李晓
,
董建新
,
张丽娜
,
张麦仓
,
胡尧和
,
谢锡善
,
国为民
金属学报
经不同固溶时效处理的PM René 95合金于650℃分别在蠕变、保载5和90 s疲劳载荷条件下进行了裂纹扩展速率实验.结果表明,相同热处理制度下,疲劳保载时间越长,裂纹扩展速率越高;相同载荷条件下,增加一次高温固溶并缓冷,有利于降低合金的裂纹扩展速率,且固溶温度越高裂纹扩展速率越低;1200℃一次固溶缓冷并于1160℃二次固溶热处理比1140℃一次固溶的裂纹扩展速率约降低一个数量级;基体晶粒尺寸适当加大,强化相粒子γ′c数量增加、形状趋于田字形,有利于降低裂纹扩展速率.
关键词:
René
,
null
,
null
李晓
,
董建新
,
张丽娜
,
张麦仓
,
胡尧和
,
谢锡善
,
国为民
金属学报
doi:10.3321/j.issn:0412-1961.2001.10.012
经不同固溶时效处理的PM René 95合金于650℃分别在蠕变、保载5和90 s疲劳载荷条件下进行了裂纹扩展速率实验.结果表明,相同热处理制度下,疲劳保载时间越长,裂纹扩展速率越高;相同载荷条件下,增加一次高温固溶并缓冷,有利于降低合金的裂纹扩展速率,且固溶温度越高裂纹扩展速率越低;1200℃一次固溶缓冷并于1160℃二次固溶热处理比1140℃一次固溶的裂纹扩展速率约降低一个数量级;基体晶粒尺寸适当加大,强化相粒子γ′c数量增加、形状趋于田字形,有利于降低裂纹扩展速率.
关键词:
René 95粉末高温合金,裂纹扩展速率,热处理
罗军
,
钟真武
,
范世(马豈)
,
王锦昌
人工晶体学报
doi:10.3969/j.issn.1000-985X.2000.01.005
本文首次报道了Ca4YO(BO3)3(YCOB)晶体的坩埚下降法生长.在1600～1650℃炉温下,固液界面处的纵向温度梯度为40～60℃/cm,以0.2～0.6mm/h的生长速率,在近封闭的Pt坩埚中生长出了直径达25mm、长度超过50mm的完整透明YCOB晶体.介绍了生长工艺和原料制备,观察发现晶体中的主要宏观缺陷是包裹体.分析了包裹体生成的原因.
关键词:
布里奇曼法
,
Ca4YO(BO3)3晶体
,
非线性光学材料
,
包裹体
Physica B-Condensed Matter
Nanocapsules consisting of B2O3/H3BO3 encapsulating Fe-Gd cores have been synthesized by an arc-discharge process using metal-boron alloys as cathode. Most of the nanocapsules have a well-constructed shell/core structure with a uniform B2O3/H3BO3 shell. Heat-treatment induces reactions between the shell and the core, resulting in the formation of a Fe3BO5+GdBO3 matrix embedded with Fe nanoparticles, reduction of the metallic-core size and decrease of the blocking temperature T-B. Above T-B, the magnetization curves plotted vs. H/T overlap and show zero coercivity. Below T-B, the coercivity shows a linear dependence when plotted vs. T-1/2. However, the coercivity-T-1/2 curve below 60 K has a different slope from that above 60 K, indicating the existence of two different magnetic phases in the nanocapsules. Different from bulk Fe3BO5, nanoscale Fe3BO5 particles have a lower transition temperature to the weak-ferromagnetic state. and magnetic hysteresis is absent due to size effects. (C) 2004 Elsevier B.V. All rights reserved.
关键词:
nanocapsules;transmission electron microscopy (TEM);X-ray;photoelectron spectroscopy (XPS);magnetic properties;arc-discharge;boric-acid;boron;carbon;oxide;nanoparticles;particles;diborane;iron
张国春
,
傅佩珍
,
李云阁
,
吴以成
人工晶体学报
doi:10.3969/j.issn.1000-985X.2005.05.001
以Na2CO3-H3BO3为助熔剂,用顶部籽晶法生长出Na3La9O3(BO3)8单晶.测定了Na3La9O3(BO3)8晶体结构,结果表明:该晶体属六方晶系,空间群:P62m,晶胞参数为a=b=0.89229(13)nm,c=O.87366(17)nm,α=β=90°,γ=120°,Z=1,V=0.60240(17)nm3,密度为5.066g/cm3.晶体结构中的硼氧基团是平面的BO3基团,BO3基团相互独立,通过与Na(1)O6、La(1)O9和La(2)O8的配位多面体连结形成层状结构,所有层平行于(001)面.描述了Na3La9O3(BO3)8晶体在非线性光学材料领域的应用前景.
关键词:
Na3La9O3(BO3)8
,
晶体结构
,
倍频效应
