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INTERNAL FRICTION AND MODULUS DEFECT ASSOCIATED WITH THE MICROCRACKS IN MATERIALS

Q.F.Fang Laboratory ofInternal Friction and Defectsin Solids , Institute of Solid State Physics , The Chinese Academy of Sciences , Hefei230031 , China

金属学报(英文版)

Inthis paper, theinvestigation of applying internalfriction ( ultrasonic attenuation) andmodulus defect(ultrasonic velocity change) tostudy the variation of dislocation density andlooplength withcycle numberintheearly fatiguestageisreviewed. On this basis,thecon ceptof characterization of fatigue microcrackformation and propagation assessed bythe mea surementofinternalfriction and dynamicalelastic modulusissuggested. Theanalyticalex pressionoftheinternalfriction and modulus defect associated with microcracksiscalculated underthe assumptionthatthe mechanicalenergy dissipation iscaused by the mutualfriction betweentheoppositefacesofthe microcrack.

关键词: internalfriction , null , null

冷轧Q195F钢种退火工艺制度的优化

崔勇 , 李驭 , 佟强

物理测试 doi:10.3969/j.issn.1001-0777.2000.06.007

介绍了从德国引进的全氢罩式退火炉的特点,结合本钢冷轧厂的生产实际情况,分析了影响Q195F钢种退火工艺的多种因素,对主要产品Q195F钢种的退火工艺制度进行了优化。

关键词: 罩式炉 , 退火 , 工艺优化

Relationship between Relaxation Internal Friction Peak at about 200℃(f≈1Hz)and Bainitic Transformation In a CuZnAl Alloy

ZHAO Zengqi CHEN Feixia YANG Dazhi BAO Er ** Physical Laboratory , Baotou Research Institute of Rare Earth , Baotou , 014010 , China*** Dept.of Materials Engineering , Dalian University of Technology , Dalian , 116024 , China**** Dept.of Materials Engineering , Yanshan Uni

材料科学技术(英文)

The present investigation showed that the re- laxation peak at about 200℃ (f≈1Hz) was related to bainitic transformation in a CuZnAl alloy.The peak decreased when bainite precipitated.The activation energy of the peak was the same as the apparent activation energy of bainitic transforma- tion.According to the relations between the peak and the bainitic transformation,the mechanism of the peak has been discussed.

关键词: internal friction , null , null , null

FRACTAL NATURE OF A FRACTURE SURFACE IN LAYERED SOLIDS

Chinese Physics Letters

We study the crack propagation in layered solids and find that when there exists an easy-fractured layer, the fractal surface becomes more rough, which is characterized by larger fractal dimensions.

关键词: dimension

Melting and superheating of crystalline solids: From bulk to nanocrystals

Progress in Materials Science

Melting of solids is a common phenomenon in nature. It is also one of the most important phase transformations in materials science and engineering. In recent years, extensive experimental and theoretical investigations in conjunction with computer simulations on melting of solids, with various geometries ranging from bulk forms to nanometer-sized clusters, have greatly enhanced our understanding of the nature of melting. This paper reviewed the up-to-date research results on this classical and cutting-edge topic. Emphasis was made on melting and superheating of nano-sized particles and thin films including thermodynamic and kinetic analyses of the size effect and the interfacial structure effect on melting processes. (C) 2007 Elsevier Ltd. All rights reserved.

关键词: isolated tin nanoparticles;embedded pb nanoparticles;kinetic stability;limit;energy ion-scattering;equation-of-state;small particles;electron-microscopy;molecular-dynamics;al(110) surface;al matrix

Synthesis of nanocrystalline materials from amorphous solids

Advanced Materials

The key to the formation of nanocrystallites from amorphous solids lies in the annealing temperature. This aspect of the preparation of nanocrystalline materials is covered, as are other attractive features of this method, for example, that it can be applied to most alloy and pure element systems, large quantities of nanocrystalline samples can be produced, and the grain size can be controlled. The properties of these materials are also described and it is concluded that more studies on 3D bulk: porosity-free, and clean samples are needed.

关键词: ultrafine grain-structure;alloys;selenium;sizes

Crystallization kinetics of amorphous solids under pressure

Physical Review B

The pressure effect on crystallization kinetics of amorphous solids was investigated by means of thermodynamic analysis. A model was developed to describe the nucleation process under pressure by considering the crystalline/amorphous (c/a) interface that plays a dominant role in the nucleation process. Applying the model to three types of crystallization process, polymorphous (a-Se), primary (Al89La6Ni5), and eutectic (Ni80P20), we found the calculated results can give reasonable explanations for the experimental observations. The calculation suggests that for a-Se and Ni80P20 amorphous alloy, the initial stage of nucleation is a volume expansion process due to the c/a interface formation, resulting in an increase in the nucleation work with an increment of pressure. Hence the crystallization temperature of the amorphous phase rises when a pressure is applied, while for the Al-La-Ni amorphous alloy, the nucleation barrier decreases at higher pressures. The coincidence between the calculation and the experimental results illustrates that the cia interface formation is the governing factor in the crystallization kinetics of the amorphous solids. [S0163-1829(99)03534-1].

关键词: activation volume;nanocrystalline state;metallic glasses;diffusion;alloy;selenium;phase;se;transformations;microstructure

Quantitative Analysis of Non-Crystalline and Crystalline Solids in Blast Furnace Slag

WANG Haifeng , ZHANG Chunxia , QI Yuanhong

钢铁研究学报(英文版)

China is short of water seriously. But granulation of blast furnace slag (BFS) with water has many disadvantages, such as high water consumption and difficulty in heat recycling. So developing a new dry granulation technique to treat BFS is very important. The applicability of BFS directly depends on the content of non-crystalline solids in the slag after treatment. So it is of theoretical and practical significance to analyze the content of non-crystalline solids in the slag quantitatively and simply. Metallographical test is mainly adopted to quantify the non-crystalline in BFS now with the shortages such as making sample complexly, determining difficultly and personally. For the diffraction intensity of non-crystalline is proportionate to the content of non-crystalline in BFS, X-ray diffraction method was adopted to quantify the non-crystalline and the crystalline solids in BFS. The quantificational coefficient between the crystalline and the non-crystalline solids of BFS is 0.70 whose main composition is: w(CaO)38.2%,w(SiO2)35.7%,w(Al2O3)16.3%,w(MgO)8.3%. The relatively error of using X-ray diffraction instrument to quantitative analyse non-crystalline content of BFS is less than 1%.

关键词: Blast Furnace Slag;Non-Crystalline;Crystalline;Quantificational Analysis

PREPARATION AND REACTIVITIES OF COMPOSITE NANOCRYSTALLINE SOLIDS PREPARED BY MECHANICAL ALLOYING

Journal of Non-Crystalline Solids

The formation of Fe-SiC composite, nanocrystalline solids through ball milling is reported. The effects of mechanical deformation, crystallite size and gaseous elements on the solid state reaction between Fe and SiC are also investigated. The formation of Fe3C after a long milling time is attributed to the kinetics of the reaction between nanocrystalline Fe and SiC.

关键词:

Characterisation of initial atmospheric corrosion carbon steels by field exposure and laboratory simulation

Corrosion Science

The early stages of the evolution of atmospheric corrosion of carbon steels exposed in both a laboratory simulated and a natural atmosphere environment in Shenyang have been observed by in situ scanning electron microscopy. In the case of laboratory cyclic wet-dry tests, even though the chloride content level is very low, filiform corrosion is initiated in the early stage. The filiform corrosion grows in random directions, forming a network of ridges. White nodules nucleate and grow on the ridges during continued corrosion and eventually connect with each other to form the initial corrosion scale. Pits were also found on the surface beneath corrosion products. In the case of a natural atmospheric environment, both filiform corrosion and other localized corrosion, such as pitting and inter-granular attack take place in the initial stage. It is obvious that there is variety of localized corrosion in the initial stage of atmospheric corrosion. (C) 2007 Elsevier Ltd. All rights reserved.

关键词: steel;atmospheric corrosion;initial stage;localized corrosion;in-situ;iron;electrolyte;thickness

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