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Element Analysis of Instrumented Sharp Indentations into Pressure-sensitive Materials

Minh-Quy LE , Seock-Sam KIM

材料科学技术(英文)

Finite element analysis was carried out to investigate the conical indentation response of elastic-plastic solids within the framework of the hydrostatic pressure dependence and the power law strain hardening. A large number of 40 different combinations of elasto-plastic properties with n ranging from 0 to 0.5 and σy/E ranging from 0.0014 to 0.03 were used in the computations. The loading curvature C and the average contact pressure pave were considered within the concept of representative strains and the dimensional analysis. Dimensionless functions associated with these two parameters were formulated for each studied value of the pressure sensitivity. The results for pressure sensitive materials lie between those for Von Mises materials and the elastic model.

关键词: Finite element analysis , null , null , null

Finite Element Analysis of Ceramic Coatings under Spherical Indentation with Metallic Interlayer: Part I Uncracked Coatings

Minh-Quy LE , Seock-Sam KIM

材料科学技术(英文)

Spherical indentation of ceramic coatings with metallic interlayer was performed by means of axisymmetric finite element analysis (FEA). Two typical ceramic coatings with relatively high and low elastic modulus deposited on aluminum alloy and carbon steel were considered. Various combinations of indenter radius-coating thickness ratios and interlayer thickness-coating thickness ratios were used in the modeling. The effects of the interlayer, the coating and the substrate on the indentation behavior, such as the radial stress distribution along the coating surface as well as the coating interface, and the plastic deformation zone evolution in the substrate were investigated in connection with the above mentioned ratios. The coating cracking dominant modes were also discussed within the context of the peak tensile stresses on the coating surface and on the coating interface.

关键词: Finite element analysis , null , null , null

Effect of Doping and High-Temperature Annealing on the Structural and Electrical Properties of Zn1-XNiXO(0≤X≤0.15) Powders

Hakan Colak

材料科学技术(英文)

This paper reported the synthesis, crystal structure and electrical conductivity properties of Ni-doped ZnO powders (i.e. Zn1-XNiXObinary system, X=0, 0.0025, 0.005, 0.0075 and in the range 0.01≤X≤0.15). I-phase samples, which were indexed as single phase with a hexagonal (wurtzite) structure in the Zn1-XNiXObinary system, were determined by X-ray diffraction (XRD). The widest range of the I-phase was determined as 0≤X≤0.03 at 1200°C; above this range the mixed phase was observed. The impurity phase was determined as NiO when compared with standard XRD data, using the PDF program. We focused on single I-phase ZnO samples which were synthesized at 1200°C because of the widest range of solubility limit at this temperature. It was observed that the lattice parameters a and c of the I-phase decreased with Ni doping concentration. The morphology of the I-phase samples was analyzed with a scanning electron microscope. The electrical conductivity of the pure ZnO and single I-phase samples were studied by using the four-probe dc method at temperatures between 100 and 950°C in air atmosphere. The electrical conductivity values of pure ZnO and 3 mol% Ni-doped ZnO samples at 100°C were 2×10-6 and 4.8×10-6Ω-1?cm-1, and at 950°C they were 1.8 and 3.6Ω-1?cm-1, respectively. In other words, electrical conductivity increased with Ni doping concentration.

关键词: II-VI semiconductors

Acoustic emission inspection of Portevin-Le Chatelier effect and deformation mechanisms of two Mg-Li-Al alloys

Journal of Materials Science

In this paper, Portevin-Le Chatelier (PLC) effect of LA41 magnesium alloy is reported. With increasing strain rate, both ultimate tensile stresses (sigma(b)) and 0.2% proof (sigma(0.2)) stresses increase, while serrations become less severe. Major acoustic emission (AE) peaks appear at the end of elastic region, and transform to burst type signals in the plastic range. In another alloy containing less Li (LA11), serrations are absent and major AE peak values are considerably lowered. Additionally, PLC effect disappears in LA41 after annealing. The role of twins is discussed in details. Actual causes for AE activity during deformation are also proposed.

关键词: tensile deformation;magnesium alloys;bands;az31

Mathematical Analysis on the Uniqueness of Reverse Algorithm for Measuring Elastic-plastic Properties by Sharp Indentation

Yongli Huang

材料科学技术(英文)

The reverse analysis provides a convenient method to determine four elastic-plastic parameters through an indentation curve such as Young's modulus E, hardness H, yield strength σy and strain hardening exponent n. In this paper, mathematical analysis on a reverse algorithm from Dao model (Dao et al., Acta Mater., 2001, 49, 3899) was carried out, which thought that only when 20&le;E*0:033&le;26and 0.3<n&le;0.5, the reverse algorithm would yield two solutions of n by dimensionless function Π2. It is shown that, however, there are also two solutions of n when 20&le;E*0:033&le;26 and 0&le;n<0.1. A unique n can be obtained by dimensionless function Π3 instead of Π2 in these two ranges. E and H can be uniquely determined by a full indentation curve, and σy can be determined if n is unique. Furthermore, sensitivity analysis on obtaining n from dimensionless function Π3 or Π22 has been made.

关键词: Elastic-plastic properties , null , null , null , null

Mathematical Analysis on the Uniqueness of Reverse Algorithm for Measuring Elastic-plastic Properties by Sharp Indentation

Yongli Huang

材料科学技术(英文)

The reverse analysis provides a convenient method to determine four elastic-plastic parameters through an indentation curve such as Young's modulus E, hardness H, yield strength σy and strain hardening exponent n. In this paper, mathematical analysis on a reverse algorithm from Dao model (Dao et al., Acta Mater., 2001, 49, 3899) was carried out, which thought that only when 20&le;E*0:033&le;26and 0.3<n&le;0.5, the reverse algorithm would yield two solutions of n by dimensionless function Π2. It is shown that, however, there are also two solutions of n when 20&le;E*0:033&le;26 and 0&le;n<0.1. A unique n can be obtained by dimensionless function Π3 instead of Π2 in these two ranges. E and H can be uniquely determined by a full indentation curve, and σy can be determined if n is unique. Furthermore, sensitivity analysis on obtaining n from dimensionless function Π3 or Π22 has been made.

关键词: Elastic-plastic properties , null , null , null , null

(Mg1-xSrx)2Al4Si5O18陶瓷的显微结构与微波介电性能研究

宋开新 , 杨岳强 , 郑鹏 , 徐军明 , 秦会斌

无机材料学报 doi:10.3724/SP.J.1077.2012.00575

采用固相烧结反应法制备(Mg1-xSrx)2Al4Si5O18陶瓷. Sr掺杂促进低温相β-Mg2Al4Si5O18向高温相α-Mg2Al4Si5O18转变, 并拓宽了(Mg1-xSrx)2Al4Si5O18陶瓷的致密化烧结温度范围. X射线衍射结果表明在0&le;x<0.2范围内, (Mg1-xSrx)2Al4Si5O18陶瓷以(Mg,Sr)2Al4Si5O18堇青石固溶体形式存在; 在0.6<x&le;1.0范围内, 以(Sr, Mg)Al2Si2O8固溶体存在. 用扫描电子显微镜观察表明Sr掺杂可以有效地降低Mg2Al4Si5O18陶瓷的气孔率与微裂纹, 促进SrAl2Si2O8锶长石晶粒生长与均匀分布. 在0&le;x&le;0.4范围内, (Mg1-xSrx)2Al4Si5O18陶瓷介电常数基本保持在7.0左右. 在0.6&le;x&le;1.0范围内从7.0增加到8.5. Qf值在0&le;x&le;0.2范围内从24100 GHz显著地提高到   38900 GHz, 然后逐渐降低至SrAl2Si2O8的14500 GHz.

关键词: Mg2Al4Si5O18; SrAl2Si2O8; 微波性能

TWIP钢不同温度变形的力学性能变化规律及机理研究

王书晗刘振宇张维娜王国栋

金属学报

通过控温拉伸实验分析了在298, 373, 473和673 K温度下变形时, TWIP钢(Fe--25Mn--3Si--3Al)力学性能和显微组织的变化规律. 结果表明, TWIP钢的强度和延伸率均随温度的升高而降低. 通过热力学公式对不同温度下TWIP钢层错能$\it\Gamma$的估算可以推断, 温度T≥673 K时, Γ≥76 mJ/m2, 滑移为TWIP钢主要的变形机制; 298 K&le; T&le;373 K时,  21 mJ/m2&le;Γ&le;34 mJ/m2, 孪生为TWIP钢主要的变形方式, 此时产生“TWIP”效应, 可获得较高的加工硬化速率, 从而获得高强度及高塑性.

关键词: 形变孪晶 , high temperature deformation , deformation mechanism , stacking fault energy

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