{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"通过单因素实验研究了黄铜基材无氰镀银预处理浸银液的硝酸银浓度、硫脲浓度、pH等工艺参数对镀银层性能的影响,优化了浸银工艺.结果表明,在100 ～ 180 g/L硫脲,20 ～ 25 g/L硝酸银,pH为1.0 ～2.0,室温,90 ～120s的条件下浸银后,沉积的银层结合力强,且经300℃保温1h除氢处理,镀层无起皮、脱落及起泡现象.","authors":[{"authorName":"邱媛","id":"24155035-0361-4d89-bbac-22b52766f02c","originalAuthorName":"邱媛"},{"authorName":"王春霞","id":"87d18ce1-8684-49cb-8faa-e348aca26021","originalAuthorName":"王春霞"},{"authorName":"于宽深","id":"bffd724a-f3b1-47af-884c-135f893c1354","originalAuthorName":"于宽深"},{"authorName":"<span style=\"color:red\">卢</span><span style=\"color:red\">野</span>","id":"8bb0aa0b-5486-4d8d-958d-501669037848","originalAuthorName":"卢野"},{"authorName":"徐小江","id":"5425b464-639b-48f5-99af-3fc5b8ad90d9","originalAuthorName":"徐小江"}],"doi":"10.3969/j.issn.1001-3849.2015.03.006","fpage":"20","id":"09174ce4-0425-4862-94ea-0bfd35108430","issue":"3","journal":{"abbrevTitle":"DDYJS","coverImgSrc":"journal/img/cover/DDYJS.jpg","id":"20","issnPpub":"1001-3849","publisherId":"DDYJS","title":"电镀与精饰   "},"keywords":[{"id":"e7b907bc-ea21-463d-82b4-766a0b4f8dc4","keyword":"铜合金","originalKeyword":"铜合金"},{"id":"4cfbb3a6-1c32-44d6-acdb-e1bdc488bbec","keyword":"漫银","originalKeyword":"漫银"},{"id":"8492032a-48ff-43e3-a305-cbdf0972bd88","keyword":"脱落","originalKeyword":"脱落"},{"id":"5a2e86aa-c907-45eb-b256-2b757796ab71","keyword":"起泡","originalKeyword":"起泡"},{"id":"0e47c70d-2d0a-4f34-8de5-043f532f8bc5","keyword":"除氢处理","originalKeyword":"除氢处理"}],"language":"zh","publisherId":"ddjs201503006","title":"黄铜基材无氰镀银预处理浸银工艺的优化","volume":"37","year":"2015"},{"abstractinfo":"由于子<span style=\"color:red\">野</span>分割带来的误差,使得调强放疗(Intensity-Modulated Radiation Therapy,简称IMRT)计划系统所制作的计划往往不能满足临床要求.本研究将采用基于共轭梯度法的子<span style=\"color:red\">野</span>权重优化方法来减小此误差,提高制作计划的效率和效果.采用共轭梯度法优化子<span style=\"color:red\">野</span>权重和微调子<span style=\"color:red\">野</span>形状,最终使得子<span style=\"color:red\">野</span>分割前后强度误差最小.在精确放疗系统中对常见的临床病例(鼻咽癌和周围性肺癌)进行测试,通过对比靶区和危及器官的剂量体积直方图以及CT片上的等剂量线,发现子<span style=\"color:red\">野</span>权重优化后靶区的平均剂量分别从87.0%提高到100.2%和从90.0%提高到98.4%,更好地满足临床要求.","authors":[{"authorName":"裴曦","id":"25e9ae0e-f07c-4b3e-9517-1c037262f567","originalAuthorName":"裴曦"},{"authorName":"曹瑞芬","id":"1a5ef92e-b483-4d67-9b34-7fb7c3235ea7","originalAuthorName":"曹瑞芬"},{"authorName":"景佳","id":"31b1e31c-a85f-49e5-af83-6c191ef7a9b9","originalAuthorName":"景佳"},{"authorName":"程梦云","id":"501f1234-a94a-455d-862b-7639b89892cb","originalAuthorName":"程梦云"},{"authorName":"郑华庆","id":"6294e3ad-8d74-4227-9636-19fe4b183a27","originalAuthorName":"郑华庆"},{"authorName":"李佳","id":"0be38e3f-9d70-4307-9e5f-58f1bd8e750a","originalAuthorName":"李佳"},{"authorName":"黄善清","id":"e1bc2648-7e0f-4a31-a467-167ff6d491c7","originalAuthorName":"黄善清"},{"authorName":"李贵","id":"8b00d15e-37f8-401f-b218-0e9dd0984f9f","originalAuthorName":"李贵"},{"authorName":"宋钢","id":"4bf5f314-223d-4a56-bacf-22a25c6146b5","originalAuthorName":"宋钢"},{"authorName":"汪卫华","id":"ed5d807b-1735-4c84-9c43-967476924d72","originalAuthorName":"汪卫华"},{"authorName":"吴宜灿","id":"84ae1d42-ade3-4b68-b846-a93e5053f191","originalAuthorName":"吴宜灿"},{"authorName":"FDS团队","id":"679e79b8-5a02-438e-be56-3ccabb4c2845","originalAuthorName":"FDS团队"}],"doi":"","fpage":"103","id":"9e81184c-77cb-4fd3-a75e-2aab609b3eaf","issue":"1","journal":{"abbrevTitle":"YZHWLPL","coverImgSrc":"journal/img/cover/YZHWLPL.jpg","id":"78","issnPpub":"1007-4627","publisherId":"YZHWLPL","title":"原子核物理评论   "},"keywords":[{"id":"9d86948b-ee37-4385-8dc0-d75ec475aeb6","keyword":"调强放疗","originalKeyword":"调强放疗"},{"id":"542c4c1d-55aa-442d-bc86-9bc0410f490e","keyword":"共轭梯度法","originalKeyword":"共轭梯度法"},{"id":"8138e813-6293-48b4-9510-43925c790146","keyword":"精确放疗系统","originalKeyword":"精确放疗系统"},{"id":"d1e50397-d152-4764-89e5-9f153386e736","keyword":"子<span style=\"color:red\">野</span>权重优化","originalKeyword":"子野权重优化"}],"language":"zh","publisherId":"yzhwlpl201101016","title":"调强放射治疗子<span style=\"color:red\">野</span>权重优化方法研究","volume":"28","year":"2011"},{"abstractinfo":"在论述重离子治癌照射的基本思想及其特点的基础上, 着重对磁扫描照射<span style=\"color:red\">野</span>形成的两种技术路线--点扫描和栅扫描的优缺点进行了分析阐述. 初步给出了HIRFL上的重离子治癌终端磁扫描相关参数. ","authors":[{"authorName":"温小琼","id":"a639e099-299f-4b51-8493-b5713dc95f94","originalAuthorName":"温小琼"},{"authorName":"李强","id":"92758d05-f503-43c0-88a9-c13d8f3c40b9","originalAuthorName":"李强"},{"authorName":"李文建","id":"e9201d3f-89c4-4b51-8c01-2593256dd782","originalAuthorName":"李文建"},{"authorName":"卫增泉","id":"9c6adebd-a23f-4de2-a340-ffadce74d76a","originalAuthorName":"卫增泉"}],"doi":"10.3969/j.issn.1007-4627.2001.03.011","fpage":"177","id":"8be3bc72-a2c6-4356-b0af-7e68a112cfae","issue":"3","journal":{"abbrevTitle":"YZHWLPL","coverImgSrc":"journal/img/cover/YZHWLPL.jpg","id":"78","issnPpub":"1007-4627","publisherId":"YZHWLPL","title":"原子核物理评论   "},"keywords":[{"id":"0f41b6a6-d676-4304-b981-47d4627963cf","keyword":"重离子治癌","originalKeyword":"重离子治癌"},{"id":"fa23bf9b-faf3-428b-87f4-e842ab6421e9","keyword":"照射<span style=\"color:red\">野</span>均匀度","originalKeyword":"照射野均匀度"},{"id":"b5a6b6b0-9daa-4e12-af16-f9aaef663cdc","keyword":"点扫描","originalKeyword":"点扫描"},{"id":"59b5f9f1-c9aa-4e64-86e9-ca77471d1101","keyword":"栅扫描","originalKeyword":"栅扫描"}],"language":"zh","publisherId":"yzhwlpl200103011","title":"重离子治癌的磁扫描照射<span style=\"color:red\">野</span>形成法","volume":"18","year":"2001"},{"abstractinfo":"采用固体核径迹探测器聚碳酸脂膜,测定了兰州重离子研究装置提供的55 MeV/u 40Ar和80 MeV/u 20Ne离子束经辐照终端束流均匀化扫描装置后照射<span style=\"color:red\">野</span>均匀度与离子通量之间的关系. 结果表明: 对于40Ar和 20Ne离子束,离子通量小于1×106和2×107 ions/cm2时,横向照射<span style=\"color:red\">野</span>均匀度缓慢增加; 当离子通量分别介于1×106-1×107和2×107-1×108 ions/cm2时,40Ar和20Ne离子束照射<span style=\"color:red\">野</span>均匀度逐渐增加; 离子通量达到1×107和1×108 ions/cm2时,40Ar和20Ne离子束照射<span style=\"color:red\">野</span>均匀度分别约为58%和61%. 从而说明,辐照终端束流扫描装置对束流的均匀化程度目前并不能满足辐照生物效应、辐射育种和重离子治癌等研究工作的需要,须对其性能做进一步的提高.","authors":[{"authorName":"李强","id":"29c99ea9-bae9-494a-bab2-6d680aaadb1a","originalAuthorName":"李强"},{"authorName":"颉红梅","id":"a248b853-784e-467b-b68d-b0b1972d53a1","originalAuthorName":"颉红梅"},{"authorName":"李文建","id":"0b41a6b5-1b20-4c3b-8009-4c378ec04b46","originalAuthorName":"李文建"},{"authorName":"党秉荣","id":"88c28084-62da-4ba6-882a-8c2d7b015dcc","originalAuthorName":"党秉荣"},{"authorName":"马秋峰","id":"d153a62b-b2aa-47e1-aa14-1a086ff2bf77","originalAuthorName":"马秋峰"},{"authorName":"卫增泉","id":"87a542c5-c31a-43ff-8d71-99b4e06ee6f4","originalAuthorName":"卫增泉"}],"doi":"10.3969/j.issn.1007-4627.2003.01.009","fpage":"48","id":"26c8333c-2e49-4256-a8bb-45e86e2090da","issue":"1","journal":{"abbrevTitle":"YZHWLPL","coverImgSrc":"journal/img/cover/YZHWLPL.jpg","id":"78","issnPpub":"1007-4627","publisherId":"YZHWLPL","title":"原子核物理评论   "},"keywords":[{"id":"03c7b8cc-e27d-40b9-be74-e4a1197854c6","keyword":"重离子束","originalKeyword":"重离子束"},{"id":"de76e31e-15c4-41f0-90a6-6b16cfbde5fd","keyword":"照射<span style=\"color:red\">野</span>均匀度","originalKeyword":"照射野均匀度"},{"id":"10297f52-333c-4c48-b675-859785564179","keyword":"离子通量","originalKeyword":"离子通量"},{"id":"129f2caf-482d-4605-83cc-b386fb761d9f","keyword":"束流扫描装置","originalKeyword":"束流扫描装置"}],"language":"zh","publisherId":"yzhwlpl200301009","title":"HIRFL辐照终端照射<span style=\"color:red\">野</span>均匀度与离子通量的关系","volume":"20","year":"2003"},{"abstractinfo":"建立了肾复康胶囊中<span style=\"color:red\">野</span>黄芩苷和芦丁的反相高效液相色谱测定方法.以甲醇-水为提取溶剂,采用超声提取法对样品进行前处理.以0.02 mol/L磷酸二氢钾缓冲溶液(含1.0%(体积分数)冰醋酸)-甲醇(体积比为63∶37)为流动相,于330 nm波长下检测,肾复康提取液中<span style=\"color:red\">野</span>黄芩苷和芦丁可达基线分离,分析时间在20 min内.<span style=\"color:red\">野</span>黄芩苷和芦丁在10 ～300 mg/L内,其峰面积与浓度之间线性关系良好,目标物的加标回收率大于98%.该方法适用于肾复康胶囊及相关药材中<span style=\"color:red\">野</span>黄芩苷和芦丁黄酮类化合物的测定和质量控制.","authors":[{"authorName":"张文珠","id":"0bf9838c-ec1e-433e-903e-8aa1f99c00ee","originalAuthorName":"张文珠"},{"authorName":"刘霞","id":"77982290-a8f2-47f3-8266-9b20e7d827ec","originalAuthorName":"刘霞"},{"authorName":"温博","id":"38e907ea-641d-4bbb-815f-5bdd9c855e1d","originalAuthorName":"温博"},{"authorName":"蒋生祥","id":"ad098b19-252e-464a-a01a-3f1be415b404","originalAuthorName":"蒋生祥"}],"doi":"10.3321/j.issn:1000-8713.2004.02.011","fpage":"138","id":"4eaa6b83-36ec-4b6f-810b-352133cb35e6","issue":"2","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"210acd98-3bf7-449b-aa78-a21bcd7b7ceb","keyword":"高效液相色谱法","originalKeyword":"高效液相色谱法"},{"id":"8f47169b-f356-4226-87cc-4de1d03e8f84","keyword":"<span style=\"color:red\">野</span>黄芩苷","originalKeyword":"野黄芩苷"},{"id":"5442a88d-3c2f-4476-8c0a-8be450d97f71","keyword":"芦丁","originalKeyword":"芦丁"},{"id":"82770356-cc2e-4410-82f4-a895be14f198","keyword":"肾复康胶囊","originalKeyword":"肾复康胶囊"}],"language":"zh","publisherId":"sp200402011","title":"反相高效液相色谱法测定肾复康胶囊中的<span style=\"color:red\">野</span>黄芩苷和芦丁","volume":"22","year":"2004"},{"abstractinfo":"以<span style=\"color:red\">野</span>燕麦主芒的厚壁纤维细胞为对象,根据其微观组织结构,建立各向异性的纤维缠绕圆管状体力学模型,导出纤维细胞在湿度载荷作用下的本构关系,分析微纤丝角、壁厚和湿度条件对应变和应力分布的影响.结果表明,纤维缠绕结构在湿度变化时的各向异性膨胀将引起管状体的轴向伸长和环向扭转,通过比较这些变形与微纤丝角之间的关系,发现微纤丝角范围为60°～80°时管状体具有稳定的变形能力.","authors":[{"authorName":"李哲","id":"c10b8233-f646-4798-b333-fe38781a60b2","originalAuthorName":"李哲"},{"authorName":"刘溪源","id":"ec88d32a-7d07-43fe-a1a3-4245351ec1ad","originalAuthorName":"刘溪源"},{"authorName":"徐献忠","id":"5d7cb90c-b43c-4ea4-a49e-3460debd958b","originalAuthorName":"徐献忠"}],"doi":"10.13801/j.cnki.fhclxb.20160822.001","fpage":"932","id":"d27c1a09-3735-462e-b3f5-3a47be548192","issue":"4","journal":{"abbrevTitle":"FHCLXB","coverImgSrc":"journal/img/cover/FHCLXB.jpg","id":"26","issnPpub":"1000-3851","publisherId":"FHCLXB","title":"复合材料学报"},"keywords":[{"id":"357cc082-96f1-4ccd-95ed-5bdebeaf7fbc","keyword":"<span style=\"color:red\">野</span>燕麦","originalKeyword":"野燕麦"},{"id":"e4057d24-6d04-40b9-8ebf-44a0d77ba3ef","keyword":"吸湿芒","originalKeyword":"吸湿芒"},{"id":"cd08e419-3d82-4f34-ba4a-b894bd159de5","keyword":"纤维细胞","originalKeyword":"纤维细胞"},{"id":"a0289c9d-90aa-4f03-b049-19f467a5aedb","keyword":"各向异性膨胀","originalKeyword":"各向异性膨胀"},{"id":"30ccb7de-00b9-4c1f-b6e0-9a3d72db5633","keyword":"力学分析","originalKeyword":"力学分析"}],"language":"zh","publisherId":"fhclxb201704030","title":"<span style=\"color:red\">野</span>燕麦主芒纤维细胞吸湿变形的力学分析","volume":"34","year":"2017"},{"abstractinfo":"通过对窟<span style=\"color:red\">野</span>河流域地表水和地下水样品进行水化学分析,探讨了该流域不同水体水化学特征和主要离子来源.结果表明,地表水与地下水均偏弱碱性.河水的水质类型由上游的Na+-Ca2+-HCO3--SO42-型演变为下游的Na+-Ca2+-SO42--HCO3-型.上游矿井水距离河道5 km以内的水化学类型与河水较为相近为Ca2+-Na+-HCO3-型;大于5 km的水化学类型为Ca2+-Mg2+-HCO3-型.随着距离的增大,矿井水与河水的联系减弱.上游生活用水井深小于180 m且距离河道小于1 km的地下水水化学特征与河水较为相似,为Na+-Ca2+-HCO3--SO42-型;井深大于180 m且距离河道大于1 km的水化学类型为Ca2+-Na+-SO42--HCO3-型和Ca2+-Na+-HCO3--Cl-型,与河水有一定的差距.下游灌溉用水水化学类型为Na+-Ca2+-SO24--HCO3-型,与下游河水水质一致.上游河水与地下水,SO42-与Ca2+、Mg2+,Ca2+与Mg2+相关性较强,说明这些离子同源,可能来源于含有碳酸盐、石膏的岩石中,印证了矿物溶解和阳离子交换对水化学演化的影响;下游河水与地下水,K+与SO42-、Cl-相关性较强,且K+、Ca2+、Na+相互间均呈现正相关,这些阳离子可能来源于含长石的砂岩.","authors":[{"authorName":"郭巧玲","id":"cf3e0715-95da-4a4c-8616-ef30984683e2","originalAuthorName":"郭巧玲"},{"authorName":"熊新芝","id":"da354042-ccb3-4a3c-8205-c7d67bc59315","originalAuthorName":"熊新芝"},{"authorName":"姜景瑞","id":"90126f6d-f628-4c28-8801-03f39e902478","originalAuthorName":"姜景瑞"}],"doi":"10.7524/j.issn.0254-6108.2016.07.2015110301","fpage":"1372","id":"3762112f-d0c1-423c-8c7c-245f94a69f83","issue":"7","journal":{"abbrevTitle":"HJHX","coverImgSrc":"journal/img/cover/HJHX.jpg","id":"43","issnPpub":"0254-6108","publisherId":"HJHX","title":"环境化学   "},"keywords":[{"id":"69f6dd8d-864c-47f0-ba1f-755c7c59cdf7","keyword":"水化学","originalKeyword":"水化学"},{"id":"6380c173-6ccd-4179-9ea2-a301415f6202","keyword":"河水","originalKeyword":"河水"},{"id":"44384589-397b-4155-ad1a-bfa8e14c2e44","keyword":"地下水","originalKeyword":"地下水"},{"id":"16a9248c-9607-469f-9191-d39f7d0535fa","keyword":"相关性分析","originalKeyword":"相关性分析"},{"id":"349237fd-65c0-407b-8f06-d00a2fdd1f33","keyword":"窟<span style=\"color:red\">野</span>河流域","originalKeyword":"窟野河流域"}],"language":"zh","publisherId":"hjhx201607006","title":"窟<span style=\"color:red\">野</span>河流域地表水-地下水的水化学特征","volume":"35","year":"2016"},{"abstractinfo":"通过在崤山金矿田黄<span style=\"color:red\">野</span>坪金矿区开展1∶1万土壤地球化学测量，圈定了Au、As、Sb等元素异常。在综合分析各异常的元素组合特征、分带性、浓度情况的基础上，对各异常进行了分类和分级，结合异常所处的空间位置，圈定和优选了找矿靶区。针对重点靶区，利用地质测量、工程揭露、深部钻探工程进行了查证，发现了金矿体，取得了较好的找矿效果，并对邻区的金矿找矿工作具有重要的指示意义。","authors":[{"authorName":"张为民","id":"532bc1c2-982f-42dc-b007-5c461f36dc26","originalAuthorName":"张为民"}],"doi":"10.11792/hj20150405","fpage":"18","id":"34ade0b1-bf85-444c-a093-1d6bcefdc9f3","issue":"4","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"f7dd5968-a568-49a7-b300-43e4b64ddad6","keyword":"崤山金矿田","originalKeyword":"崤山金矿田"},{"id":"a024f41b-876c-474c-9da6-ecbd90ee3ceb","keyword":"黄<span style=\"color:red\">野</span>坪金矿区","originalKeyword":"黄野坪金矿区"},{"id":"13095ef0-4d80-4beb-aebb-91ece14af43a","keyword":"土壤地球化学测量","originalKeyword":"土壤地球化学测量"},{"id":"eeb424d0-361e-45ec-b372-51cb9ed8a81d","keyword":"成矿预测","originalKeyword":"成矿预测"},{"id":"01c06694-1c76-4ce0-b29f-c2277527c771","keyword":"工程验证","originalKeyword":"工程验证"}],"language":"zh","publisherId":"huangj201504007","title":"土壤地球化学方法在黄<span style=\"color:red\">野</span>坪金矿区普查中的应用和找矿效果","volume":"","year":"2015"},{"abstractinfo":"采用柱前衍生化高效液相色谱-荧光检测法测定了桑叶中的1-脱氧<span style=\"color:red\">野</span>尻霉素(DNJ).用0.05 mol/L HCl提取桑叶中的DNJ,采用6-氨基喹啉基-N-羟基琥珀酰亚氨基甲酸酯(AQC)试剂在pH 8.5硼酸盐缓冲液下对DNJ进行衍牛化,以0.02 mol/L磷酸二氢钾缓冲液(pH 5.0)-乙腈(体积比为85:15)为流动相,利用C18色谱柱(5μm,250 mm×4.6 mm)分离,在激发波长为250 nm、发射波长为395 nm条件下进行荧光检测,DNJ的AQC衍生物与衍生化试剂的水解产物分离良好.方法的线性范围为0.5～25 mg/L,检出限为0.02 mg/L(S/N=3).实验测得桑叶中DNJ含量为0.12%;回收率为96.1%～98.6%.","authors":[{"authorName":"谢慧明","id":"82d7ea3f-ab76-443e-803a-42f9aaf71464","originalAuthorName":"谢慧明"},{"authorName":"吴方睿","id":"41ed9479-1418-456c-bc6e-456a024aeac1","originalAuthorName":"吴方睿"},{"authorName":"杨毅","id":"1d548b75-e8fc-4784-b241-418408d2df2a","originalAuthorName":"杨毅"},{"authorName":"刘杰","id":"e0d86485-2a95-4ba0-bac0-071ce538214d","originalAuthorName":"刘杰"}],"doi":"10.3321/j.issn:1000-8713.2008.05.022","fpage":"634","id":"ffb82ac4-ff5a-43e7-9037-711d760cadde","issue":"5","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"e98ca716-b44a-480a-821a-0114b0e0e068","keyword":"柱前衍生化","originalKeyword":"柱前衍生化"},{"id":"c179bc2b-adda-41ea-8da2-8e418384fca5","keyword":"高效液相色谱法","originalKeyword":"高效液相色谱法"},{"id":"07ac9750-c1be-4d30-bfa4-a86e7b42fa82","keyword":"荧光检测","originalKeyword":"荧光检测"},{"id":"57cdf765-f6e5-41f3-b889-4e49f1cfa490","keyword":"1-脱氧<span style=\"color:red\">野</span>尻霉素","originalKeyword":"1-脱氧野尻霉素"},{"id":"212ce1d3-2e95-4d92-adb8-69406238d09e","keyword":"桑叶","originalKeyword":"桑叶"}],"language":"zh","publisherId":"sp200805022","title":"柱前衍生化高效液相色谱-荧光检测法测定桑叶中的1-脱氧<span style=\"color:red\">野</span>尻霉素","volume":"26","year":"2008"},{"abstractinfo":"建立了大鼠灌胃麻杏石甘汤后血浆中苦杏仁苷、<span style=\"color:red\">野</span>黑樱苷的定性及定量方法。样品经液液萃取净化处理，定性采用超高效液相色谱-串联四极杆飞行时间质谱仪（UPLC-QTOF-MS / MS），经 Shim-pack XR-ODS Ⅲ色谱柱（75 mm×2.0 mm，1.6μm）分离，定量采用超高效液相色谱-串联三重四极杆质谱仪（ UPLC-Q-TRAP-MS），经 Agilent C18色谱柱（50 mm×2.1 mm，1.7μm）分离，电喷雾负离子化（ ESI）及 MRM 模式测定，流动相均为乙腈-0.1％（ v /v）甲酸水溶液。结果显示苦杏仁苷、<span style=\"color:red\">野</span>黑樱苷在相应浓度范围内线性关系良好（相关系数分别为0.9990、0.9970），精密度（RSD）小于9.20％，回收率为82.33％~95.25％，检出限（ LOD）约为0.50 ng / mL。本方法快速简便，为血浆样品中苦杏仁苷、<span style=\"color:red\">野</span>黑樱苷的定性和定量分析提供良好参考。","authors":[{"authorName":"高萌","id":"048eb0c6-2e65-49f5-b90f-2dc4e81c6473","originalAuthorName":"高萌"},{"authorName":"王跃生","id":"dffa9ba8-9599-4594-ab04-bb55525ecd10","originalAuthorName":"王跃生"},{"authorName":"魏惠珍","id":"cf1c1cd5-ca8c-4c38-a085-b0daab631a49","originalAuthorName":"魏惠珍"},{"authorName":"欧阳辉","id":"4a87eaf8-9d30-43a3-96f0-0043b40d1b82","originalAuthorName":"欧阳辉"},{"authorName":"何明珍","id":"386528f8-03e5-4338-aca4-0acbafb42b3a","originalAuthorName":"何明珍"},{"authorName":"曾恋情","id":"2a7be482-e6b3-4f28-bb2d-3ed7d8c1b6a6","originalAuthorName":"曾恋情"},{"authorName":"申峰云","id":"8839b301-9799-4c82-93b6-f9cb522638f8","originalAuthorName":"申峰云"},{"authorName":"郭强","id":"608f8516-b54f-4bca-948a-fbba2c346736","originalAuthorName":"郭强"},{"authorName":"饶毅","id":"481f9f4d-ff41-4c9e-b761-4d4a3b20ced8","originalAuthorName":"饶毅"}],"doi":"10.3724/SP.J.1123.2014.01021","fpage":"591","id":"75973389-0e0a-42c6-8d3c-8d7731f6bdde","issue":"6","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"9ceb79ab-5cad-4a81-a07b-cd6c1c028c6a","keyword":"超高效液相色谱-串联四极杆飞行时间质谱","originalKeyword":"超高效液相色谱-串联四极杆飞行时间质谱"},{"id":"7476fec4-8062-4691-95a4-1d2b8299a71f","keyword":"超高效液相色谱-串联三重四极杆质谱","originalKeyword":"超高效液相色谱-串联三重四极杆质谱"},{"id":"0dee5256-b305-4d9f-b92d-c89724606bdd","keyword":"苦杏仁苷","originalKeyword":"苦杏仁苷"},{"id":"abe8d9ea-5440-4562-bffa-30c8a746f3b6","keyword":"<span style=\"color:red\">野</span>黑樱苷","originalKeyword":"野黑樱苷"},{"id":"f3260deb-4178-4a01-87e4-d85cf9b66245","keyword":"大鼠血浆","originalKeyword":"大鼠血浆"}],"language":"zh","publisherId":"sp201406006","title":"超高效液相色谱-串联四极杆飞行时间质谱和超高效液相色谱-串联三重四极杆质谱用于血浆中苦杏仁苷及其代谢产物<span style=\"color:red\">野</span>黑樱苷的定性和定量分析","volume":"","year":"2014"}],"totalpage":5,"totalrecord":43}