材料期刊网

Silicon Pickup of InterstitialFree Steel From MgOSiC Refractories

WEI Yaowu , LI Nan , CHEN Xiaoxia , HU Tieshan , RAO Jiangping , TAO Xiaolin

钢铁研究学报(英文版)

The silicon pickup of interstitialfree steel (IF steel) from resin bonded MgOSiC refractories is studied via a medium frequency induction furnace. Samples of IF steel were heated in MgOSiC crucibles with mould flux cover at 1 600 ℃ for 180 min. The silicon contents of IF steel samples taken from the molten steel in every 30 min were examined and the refractories after heating were investigated by electron probe microanalysis (EPMA) with energy dispersive spectrometer (EDS). The silicon content of steel rapidly increased in the first 90 min of heating, and then decreased because of the formation of liquid layer on the refractory. Liquid layer separated the liquid steel from the bulk refractory and stopped the pickup of silicon. At the same time, desilication via oxygen through the liquid layer and flux started to reduce the silicon content of the liquid steel.

关键词: MgOSiC refractory;silicon carbide;silicon content;steel

116HU聚酯亚胺无挥发浸渍树脂的性能及其在风电上的模拟结构试验

王君 , 邹家桂 , 陈政标 , 高建武 , 刘彦坤 , 张杰元 , 宋莎

绝缘材料

　　为解决苯乙烯和甲基苯乙烯在VPI浸渍树脂应用于风力发电机中的不足，采用不饱和聚酯亚胺、引发剂和无挥发活性稀释剂研制出116HU聚酯亚胺无挥发浸渍树脂，并对其各项性能进行了研究。结果表明：116HU聚酯亚胺无挥发浸渍树脂的常规性能满足风力发电机的要求，其耐热等级可达H级。用该树脂浸渍的风电模拟线棒具有优异的介电性能、耐湿热交变和高低温循环冲击性能及耐盐雾性能等，能满足风力发电机在极端环境运行的要求。

关键词: 聚酯亚胺 , 无挥发 , VPI , 风力发电机 , 耐湿热 , 耐盐雾

基于二氧化碳封存的超临界两相流动的数值研究

高诚 , 胥蕊娜 , 陈黎 , 姜培学

工程热物理学报

格子Boltzmann方法(LBM)在计算复杂结构物理模型时具有独特优势并在模拟两相流动过程中能够高效清晰捕捉相界面.本文介绍了基于Shan-Chen多相模型的格子Boltzmann方法的理论成果以及基于二氧化碳封存的超临界两相流的模拟研究.结果表明,Shan-Chen模型在模拟两相流时符合Laplace定律,且两相层流时的速度分布和相渗曲线均与理论值吻合.二氧化碳封存过程中,较大的注入速率在提高二氧化碳残余俘获量的同时会降低其化学俘获量.

关键词: 二氧化碳封存 , 超临界两相流 , Shan-Chen模型

A Study of the Ni-Cr-Zr System at 900°C

Ximiao PAN , Zhanpeng JIN

材料科学技术（英文）

The phase equilibrium relations of the ternary Ni-Cr-Zr system at 900°C have been investigated by means of diffusion triple and electron probe microanalysis (EMPA) techniques. A series of tie lines and triangles have been determined, and the corresponding tentative isothermal section is presented based on the current information.

关键词: Nickel , null , null , null

SAR图像目标识别新方法

王丽 , 魏巍 , 吴林钢 , 王灿进

液晶与显示 doi:10.3788/YJYXS20142903.0429

提出一种SAR图像目标识别新方法.首次引入BM3D方法,用于滤除原始图像中的相干斑噪声,BM3D结合了空间域和变换域去噪的优势,滤波性能优异.在特征提取步骤,将低阶Hu矩与高阶Zernike矩组合,Hu矩描述目标的粗略信息,高阶Zernike矩描述目标的细节信息,因此组合矩能够更加全面而细致地表达目标特性.使用组合矩特征训练SVM分类器,对含噪的SAR图像进行识别实验.实验结果表明:本文方法的识别率高达98.90％,优于已有的SAR目标识别方法.

关键词: SAR图像 , 目标识别 , BM3D滤波 , 组合矩

Subsolidus phase relations in the ZnO-MoO3-B2O3, ZnO-MoO3-WO3 and ZnO-WO3-B2O3 ternary systems

Journal of Alloys and Compounds

The subsolidus phase relations in the ZnO-MoO3-B2O3, ZnO-MoO3-WO3 and ZnO-WO3-B2O3 ternary systems have been investigated by the means of X-ray powder diffraction (XRD). There is no ternary compound in all the systems. There are five binary compounds and five tie lines in the ZnO-MoO3-B2O3 system. This system can be divided into six 3-phase regions. There are three binary compounds and three tie lines in the ZnO-MoO3-WO3 system. This system can be divided into four 3-phase regions. There are four binary compounds and four tie lines in the ZnO-WO3-B2O3 system. This system can be divided into five 3-phase regions. The possible component regions for ZnO single crystal flux growth were discussed. The phase diagram of Zn3B2O6-ZnWO4 pseudo-binary system has been constructed, and the result reveals this system is eutectic system. The eutectic temperature is 1007 degrees C and eutectic point component is 70 mol% Zn3B2O6. (c) 2007 Elsevier B.V. All rights reserved.

关键词: ZnO-MoO3-B2O3;ZnO-MoO3-WO3;ZnO-WO3-B2O3;Zn3B2O6-ZnWO4;phase relation;zno single-crystals;zinc oxide;growth;moo3-wo3

Formation of TiB2 whiskers in laser clad Fe-Ti-B coatings

Surface & Coatings Technology

In order to reduce the high brittleness of laser clad Fe-B coatings, the composite Fe-Ti-B coating was developed by laser cladding with a powder mixture of B4C and Fe-Ti alloy. The microstructure, hardness and cracking resistance of these coatings were investigated in this paper. The experimental work enables the following findings to be reached: (i) the needle-like TIE, whiskers could be synthesized in situ using the laser cladding method in the composite Fe-Ti-B coating. (ii) The size, shape and volume fractions of TiB2 whiskers in the composite coating are greatly dependent upon powder compositions (contents of B, Ti elements and the ratio of B/Ti elements) and the laser energy density used. The average ratio of width/length for the synthesized TiB2 whiskers increases with increasing laser energy density and ratio of B/Ti elements in this coating. (iii) Both the hardness and cracking resistance of the Fe-B laser clad coating could be improved by the formation of TIE, whiskers. (C) 2001 Elsevier Science B.V. All rights reserved.

关键词: TiB2;laser cladding;coating;steel;microstructure;powders

硝酸羟胺的热稳定性评估及热分解机理研究

刘建国 , 安振涛 , 张倩 , 杜仕国 , 姚凯 , 王金

材料导报 doi:10.11896/j.issn.1005-023X.2017.04.030

为评估氧化剂硝酸羟胺的热稳定性,使用标准液体铝皿于3 K/min、4 K/min、5 K/min加热速率下进行热分析.借助非等温DSC曲线的参数值,应用Kissinger法和Ozawa法求得热分解反应的表观活化能和指前因子,根据Zhang-Hu-Xie-Li公式、Hu-Yang-Liang-Xie公式、Hu-Zhao-Gao公式以及Zhao-Hu-Gao公式,计算硝酸羟胺的自加速分解温度和热爆炸临界温度,并对热分解机理函数进行了研究.设计了7条热分解反应路径,采用密度泛函理论B3LYP/6-311++G(d,p)方法对硝酸羟胺的热分解进行了动力学和热力学计算.计算结果表明,硝酸羟胺热分解的自加速分解温度TsADT=370.05 K,热爆炸临界温度Te0=388.68K,Tbp0=397.54 K,热分解最可几机理函数的微分形式为f(a) =17×(1-α)18/17.硝酸羟胺热分解各路径中,动力学优先支持路径Path 6、Path 5、Path 4和Path 1生成NO和NO2,其次是Path 2、Path 7和Path 3生成N2和N2O.温度在373 K以下时,Path 1'反应无法自发进行,硝酸羟胺无法进行自发的热分解.从热力学的角度来看,硝酸羟胺在370.05K以下储存是安全的.

关键词: 硝酸羟胺 , 热分析 , 热稳定性 , 热分解机理 , 密度泛函理论

Measurement of the remnant magnetic-field in Lorentz mode using permalloy

Haihua LIU

金属学报(英文版) doi:10.1016/S1006-7191(08)60120-9

A novel method was reported to measure the remnant magnetic field in Lorentz mode in a FEI Tecnai F20 transmission electron microscope equipped with a Lorentz lens. The movement of the circle Bloch line of the cross-tie wall in Permalloy is used to measure the remnant magnetic field by tilting the specimen and adjusting the objective lens current. The remnant magnetic field is estimated to be about 17 Oe, in a direction opposite to that of the objective lens magnetic field. The remnant magnetic field can be compensated by adjusting the value of the objective lens current.

关键词: Lorentz electron microscopy , Lorentz lens , remnant magnetic field , Permalloy , cross-tie walls

基于格子Boltzmann方法的疏水表面润湿性数值模拟?

黄桥高 , 潘光

功能材料 doi:10.3969/j.issn.1001-9731.2015.10.005

润湿性对固体表面上液体的各种动力学行为具有重要影响，疏水表面的特殊润湿性是其在减阻、降噪、防污等领域有着广泛应用前景的根本原因。基于Shan-Chen模型的格子Boltzmann方法对疏水表面润湿性进行数值模拟，获得了材料属性和微形貌对疏水表面润湿性的影响规律。研究表明，要使疏水表面处于 Cassie-Baxter 润湿状态，微形貌高度必须大于某一临界值，而当疏水表面一旦处于 Cassie-Baxter 润湿状态后，继续增加微形貌高度也不会提高其疏水性能；疏水表面的表观接触角随气液界面分数先增大后减小，且存在一个最佳的气液界面分数使表观接触角达到最大。

关键词: 疏水表面 , 格子Boltzmann方法 , 材料属性 , 微形貌 , 润湿性