F. Zhang1)
,
X. D. Sun1)
,
J. You2)
,
Z. Zhang2)
,
L. X. Ding3)and Y. M. Wang3)1) School of Materials and Metallurgy
,
Northeastern University
,
Shenyang 110006
,
China2) Liaoning Analyzing and Testing Research Center
,
Shenyang 110015
,
China3) Department of Materials
,
School of Mechanical Engineering
,
Shenyang University
,
Shenyang 110044
,
China
金属学报(英文版)
Synthesis of a m m oniu m alu min u m carbonate hydroxide ( A A C H) w as investigated usinga m m oniu m alu min u m sulfate and a m moniu m hydro carbonate as the starting m aterials . Itw as found that A A C Hcan be synthesized by adding a m m oniu m alu m inu m sulfate solution torapidly stirred a m moniu m hydro - carbonate solution at a tem perature of 30 ℃. A A C Hcantransfor m to α Al2 O3 co m pletely by calcining at 1100 ℃ for 1 hour , and the obtained po w ders , with a particle size of 100 n m , can be sintered to 98 99 % relative density at 1500 ℃for 2 hours .
关键词:
a m moniu m alu m inu m carbonate hydroxide
,
null
,
null
,
null
罗湘宁
,
王晶
,
陈赓华
,
杨乾声
,
张利华
低温物理学报
doi:10.3969/j.issn.1000-3258.2000.01.003
本文采用偏置电流反转的频率与磁通调制频率相等的方案,研制了带偏置电流反转的dc SQUID测试系统,明显降低了YBCO双晶结dc SQUID的1/f噪声.在3Hz处,磁通噪声由静态偏置时的降低到.1/f噪声的角频率从1kHz下降到3Hz.前放的设计,采用低噪声集成电路,整个磁通锁定环置于测试杆顶端,简化了电路,提高了测试系统的稳定性.在白噪声区,测得最低磁通噪声为 .前放的噪声系数为1.1dB.
关键词:
Zhiyong Liu
材料科学技术（英）
Here we report the fabrication and superconductivity of the iron-based arsenic oxide SmO1-xFxFeAs compound. X-ray diffraction (XRD) results prove that the lattice parameters a and c decrease systematically with increasing x in between 0<x≤0.35, but when x>0.35 the a and c increase with the decrease of x in
the SmO1-xFxFeAs. The critical temperature (Tc) increases with increasing x in between 0.15≤x≤0.3, while x>0.3 the Tc decreases with the increase of x. It is found that at x=0.3 SmO0.7F0.3FeAs has the highest onset resistivity transition temperature of 55.5 K. The critical current density (Jc) value at 10 K for the obtained SmO0.7F0.3FeAs is 1.3×105 A/cm2 (0 T). Meanwhile one can estimates Hc2(0) from the slope of the Hc2(T) curve at T=Tc (HC2 is the upper critical field), and for the 90% normal-state resistivity (ρn) criterion (Tc=55 K), Hc2(0) is determined to be ~253 T.
关键词:
SmO1-xFxFeAs compound
Superconductor Science & Technology
It is shown that the superconductivity in Ce(1-x)Gd(x)FeAsO(0.84)F(0.16) compounds can be modulated by internal (chemical) pressure. The internal pressure is induced by Gd substitution for Ce in CeFeAsO(0.84)F(0.16), which compresses the crystal lattice. The temperature dependences of resistivity and magnetization show that the superconducting-transition temperature T(c) is enhanced from 40 K for CeFeAsO(0.84)F(0.16) to 47.5 K for Ce(0.6)Gd(0.4)FeAsO(0.84)F(0.16). The increase and subsequent decrease of Tc upon application of external pressure, as observed previously in LaFeAsO(0.89)F(0.11), is entirely confirmed by the modulation of Tc of the Ce(1-x)Gd(x)FeAsO(0.84)F(0.16) superconductors by internal pressure.
关键词:
layered quaternary compound;43 k;iron
李强
,
王其申
量子电子学报
doi:10.3969/j.issn.1007-5461.2007.01.002
针对淹没在1/f分形噪声中的有用信号恢复问题,提出了一种基于小波变换与Kalman滤波的多尺度滤波算法.首先将带有1/f分形噪声的信号分解成多尺度的子带信号,通过小波变换对1/f分形噪声的白化作用,消除了1/f分形噪声的自相似性和长程相关性.然后在小波域内,利用Kalman滤波实现了噪声和有用信号的分离,估计出了各子带中的有用信号.最后进行小波重构,较好地恢复出淹没在1/f分形噪声中的有用信号.仿真实验表明,使用多尺度Kalman滤波器能有效地抑制分形噪声,显著地提高了信噪比.
关键词:
图像处理
,
Kalman滤波
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小波变换
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1/f分形噪声
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自相似性
Journal of Applied Physics
Structural parameters have a critical impact on superconductivity in iron-based oxypnictide superconductors. Structural evolution study was performed on Ce(1-x)Gd(x)FeAsO(0.84)F(0.16) superconductors by the analysis of the x-ray diffraction patterns with Rietveld refinement. Substitution of Gd for Ce generates internal pressure that compresses the crystal lattice. The contraction of the c axis is also indicated by the reduction of Ce/Gd-As and Ce/Gd-O/F distances, while there is a slight increase in the As-Fe-As block size, which is compensated by a large reduction in the Ce/Gd-O/F-Ce/Gd block with Gd substitution. The diagonal Fe-As-Fe angle for Ce(0.6)Gd(0.4)FeAsO(0.84)F(0.16), with the highest T(c) among Ce(1-x)Gd(x)FeAsO(0.84)F(0.16) compounds, is 111.13 degrees. It is close to the ideal value of 109.47 degrees for the perfect FeAs tetrahedron, which is situated in the region of Fe-As-Fe bond angles where RFeAsO compounds tend to have the highest T(c). (C) 2011 American Institute of Physics. [doi:10.1063/1.3565408]
关键词:
layered quaternary compound;high-temperature superconductivity
ZHAO Zengqi CHEN Feixia YANG Dazhi BAO Er ** Physical Laboratory
,
Baotou Research Institute of Rare Earth
,
Baotou
,
014010
,
China*** Dept.of Materials Engineering
,
Dalian University of Technology
,
Dalian
,
116024
,
China**** Dept.of Materials Engineering
,
Yanshan Uni
材料科学技术（英）
The present investigation showed that the re- laxation peak at about 200℃ (f≈1Hz) was related to bainitic transformation in a CuZnAl alloy.The peak decreased when bainite precipitated.The activation energy of the peak was the same as the apparent activation energy of bainitic transforma- tion.According to the relations between the peak and the bainitic transformation,the mechanism of the peak has been discussed.
关键词:
internal friction
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null
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null
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null
卓海涛
,
王先友
,
唐安平
,
刘志明
中国有色金属学报
采用高温固相法合成掺杂改性的NaV1-xCrxPO4F(x=0,0.04,0.08)作为钠离子电池正极材料.通过红外光谱(FT-IR)、X射线衍射(XRD)和扫描电镜(SEM)等对材料的晶体结构和形貌进行表征.从材料的晶体结构、恒流充放电测试和循环性能等方面分析掺杂元素Cr在改善材料性能中的作用.结果表明:掺Cr后的材料电化学循环稳定性得到较好的改善,首次放电容量达到83.3 mA·h/g,效率高达90.3%,循环20次后可逆容量保持率仍然有91.4%.
关键词:
钠离子电池
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高温固相法
,
正极材料
,
Cr掺杂
,
氟磷酸化合物
刘志勇
,
索红莉
,
马麟
,
赵俊静
,
倪宝荣
,
郭志超
,
闫镔杰
,
刘敏
,
吴紫平
,
周美玲
稀有金属材料与工程
研究了F掺杂对铁基超导体SmO0.7F0.3FeAs的制备和性能的影响.利用二次固相反应在1120℃保温40h制备出超导临界转变温度(Tc)为56.5 K的SmO0.7F0.3FeAs超导体样品,其临界电流密度Jc为2.4× 105 A/cm2(10 K,0 T).研究发现,SmO1-xFxFeAs样品的Tc受F含量的强烈影响,晶格参数的变化也是诱导SmO1-xFxFeAs超导体的Tc变化的原因之一.在此基础上详细研究了F元素过掺杂对铁基超导体SmO1-xFδFeAs(δ＞x)制备参数和性能的影响.F元素过量时,在不降低SmO1-xFδFeAs超导性能的情况下,F元素过掺杂可以一定程度地降低样品制备时的热处理温度和极大地缩短热处理时间.1100℃时保温20h制备的SmO0.7F0.35FeAs和SmO0.7F04FeAs样品的Tc分别为56和55K;其临界电流密度Jc分别为1.9×105和1.7× 105 A/cm2 (10K,0 T).
关键词:
铁基超导体
,
SmO1-xFδFeAs
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掺杂
