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EFFECT OF REVERT RECYCLE TIMES ON MICROSTRUCTURE AND FATIGUE PROPERTIES IN COBALT BASE SUPERALLOY K640S

T.L. Wang 1 , 2) , J.T. Guo 1) , D.S. Xia 2) , Y.Wang 1) and H.C. Yang 2) 1) Institute of Metal Research , Chinese Academy of Science , Shenyang 110015 , China 2) Material and Metallurgical Institute Northeastern University , Shenyang 110006 , China

金属学报(英文版)

Effect of revert cycles on microstructure and fatigue properties of cast cobalt base superalloy K640S has been investigated. The results show that: at 70 times of cool heat cycles, there were microcracks found in seven times revert and ten times revert. With the increasing of thermal fatigue cycles, the crack of revert grows a little faster than virgin. When the cycle time reaches 200, the crack length for both virgin and reverts have been as long as 2mm. The low cycle fatigue life has no remarkable change, with the increase of revert cycles at 815℃, 360MPa ,0 5Hz. With the times of cycles increasing, it is found that the content of impurity and gas in alloy change a little, and there is no obvious change for dendrite microstructure.

关键词: revert , null , null , null , null

Guangzhou Institute of Energy Conversion,The Chinese Academy of Sciences,Guangzhou 510070,China

B.W. Wang , H. Shen

金属学报(英文版)

Ni-Cr System solar selective thin solid films were prepared by d.c. magnetron reactivesputtering under the atmosphere of O2 and N2. Ni-Cr alloy was chosen as targetmaterial and copper sheets as substrate. Using SEM, Spectrophotometer and Talystepto analyze the relations between the selective characteristic and the structure, theformation and the thickness of the thin films. The aim is to obtain good solar selectivethin films with high absorptance and low emittance, which is applied to flat plate solarheat collectors.

关键词: solar selective thin film , null , null , null

(alpha-PbO2-type nanophase of TiO2 from coesite-bearing eclogite in the Dabie Mountains, China

American Mineralogist

A natural high-pressure phase of titanium oxide with alpha-PbO2-structure has been found in omphacite from coesite-bearing eclogite at Shima in the Dabie Mountains, China. High-resolution transmission electron microscope observations have revealed an orthorhombic lattice, corresponding to alpha-PbO2-type TiO2, with cell parameters a = 0.461 nm, b = 0.540 nm, c = 0.497 nm and space group Pbcn. It occurs as nanometer-thick (< 2 nm) lamellae between multiple twinned rutile crystals, providing additional evidence of very high-pressure, metamorphism at 7 GPa, 900 degrees C. This implies subduction of continental material to a depth of more than 200 kilometers. alpha-PbO-type TiO2 could be an extremely useful index mineral for ultrahigh-pressure.

关键词: high-pressure phase;ries crater;rutile;polymorph;titanium

ELECTROCHEMICAL MEASUREMENTS OF COMPONENT ACTIVITIES IN METALLURGICAL SLAGS

O. Volkova , P.R.Scheller , D.Janke

金属学报(英文版)

The up-to-date status of FeO, CaO, SiO2, P2O05,Ti2O3 and Cr2O3 activity measurements in metallurgical slags using electrochemical sensors is outlined. A description of theoretical concepts and practical sensors is presented including their determining features.

关键词: electrochemical measurement , null , null

Microstructure and Mechanical Properties of ZrO_2-Ni Functionally Gradient Material

Jingchuan ZHU , Zhongda YIN and Zhonghong LAI(Dept. of Metals and Technology , Harbin Institute of Technology , Harbin , 150001. China)

材料科学技术(英文)

The fabrication. microstructure and mechanical properties of ZrO2-Ni functionally gradient materials (FGM ) have been studied. FGM as well as non-FG M of ZrO2-Ni system was developed by powder metallurgical process. X-ray diffractometer (XRD ). electron probe microanalyzer (EPMA), scanning electron microscope (SEM ) and optical microscope were employed to investigate the crystalline phases. chemical composition and microstructure Experimental results demonstrate that the composition and microstructure of ZrO2-Ni FGM have the expected gradient distribution. There are no distinct interfaces in the FGM due to the gradient change of components. that is, the constituents are continuous in microstructure everywhere. Moreover, Vickers hardness and flexural strength were measured for the common composites as a function of composition. It is made clear that the mechanical properties of the FGM vary corresponding to the constitutional changes as well

关键词:

Tribological behavior of Ti3SiC2-based material

材料科学技术(英文)

The wear and friction properties of Ti3SiC2-based materials were studied using the pin-on-disc method. The friction coefficient of Ti3SiC2-based material was not very sensitive to normal load, the steady state value, p, increased from 0.4 to 0.5 when the normal load increased from 7.7 N to 14.7 N. The wear volume for Ti3SiC2 disc increased with increasing normal load or sliding distance in the tests. The average wear rate of Ti3SiC2-based material was 9.9X10(-5) mm(3)/Nm. The debris on the Ti3SiC2 disc was essentially made up of Ti3SiC2 and steel pin materials, while the debris on the steel sliders was generally pip material. The wear mechanism was concluded as the fracture and delamination of Ti3SiC2-based materials followed by adhesive wear of steel sliders.

关键词: Ti3SiC2;wear and friction;friction coefficient;wear volume;titanium-silicon carbide;friction

Cu/Ti3SiC2 composite: a new electrofriction material

Materials Research Innovations

Cu/Ti3SiC2 composite, a new electrofriction material, was prepared, for the first time, by PM method. The microstructure, mechanical and electrical properties of the Cu/Ti3SiC2 composites were investigated and were compared with those of Cu/graphite composites. The results demonstrated that Cu/Ti3SiC2 composites had superior mechanical properties over Cu/graphite composites. At filer content of less than 20 vol%, the electrical conductivity for Cu/Ti3SiC2 composites was higher than that for Cu/graphite composites; at high filer content, the electrical conductivity for Cu/Ti3SiC2 composites was lower than that for Cu/graphite composites because of the presence of residual pores. It was found that like Cu/graphite composite, Cu/Ti3SiC2 was a self-lubricated material. The compressive yield strength, Brinell hardness, relative ratio of compressive for Cu-30 vol% Ti3SiC2 composites are 307 MPa, 140, 15.7% respectively.

关键词: electronfriction material;copper;Ti3SiC2;graphite;composite;self-lubricating;ti3sic2

Change in Carbon Dioxide (CO2) Emissions From Energy Use in China′s Iron and Steel Industry

SUN Wenqiang , CAI Jiuju , MAO Hujun , GUAN Duojiao

钢铁研究学报(英文版)

As the largest energy consuming manufacturing sector and one of the most important sources of carbon dioxide (CO2) emissions, the China′s iron and steel industry has paid attention to the study of changing trend and influencing factors of CO2 emissions from energy use. The logarithmic mean Divisia index (LMDI) technique is used to decompose total change in CO2 emissions into four factors: emission factor effect, energy structure effect, energy consumption effect, and steel production effect. The results show that the steel production effect is the major factor which is responsible for the rise in CO2 emissions; whereas the energy consumption effect contributes most to the reduction in CO2 emissions. And the emission factor effect makes a weak negative contribution to the increase of CO2 emissions. To find out the detailed relationship between change in energy consumption or steel production and change in CO2 emissions, the correlation equations are also proposed.

关键词: CO2 emissions , energy use , LMDI technique , steel production , energy consumption

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