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Studies of Correlations between Surface Composition Changes and Ion Bombardment Fluences of Multicomponent Materials

Liping ZHENG Xiqing XIA Mingyao LI Shanghai Institute of Nuclear Research , Academia Sinca , Shanghai , 201800 , ChinaRisheng LI Lab.of Atomic Imaging of Solids , Institute of Metal Research , Academia Sinica , Shenyang , 110015 , China

材料科学技术(英文)

Correlations between surface composition changes and ion bombardment fluences were studied for multicomponent materials by using a dynamic Monte Carlo program,including the preferential sputtering and bombardment-induced Gibbsian segregation (BIGS) processes.For the case of 1 keV KR-~(10)B_(0.02)~(11)B_(0.08) (the most simple multicomponent material system),it is found that the ~(10)B composition enriches at the surface at low fluences but depletes at the surface at high fluences.For the case of 1 keV Ar-Pt_(0.5)Cu_(0.5).it is found that the Cu composition at the topmost surface is always under the bulk composition between zero and high fluences,but the evident composition gradient of Cu(the segregation species) exists in the surface at low fluences.The effects of the preferential sputtering and BIGS processes on above two surface composition profiles are also discussed.

关键词: implantation , null , null

MICROSTRUCTURE AND PROPERTIES OF SiC_w/6061Al COMPOSITE The Author is now with Institute of Metal Research,Academia Sinica,China

MA Zongyi YAO Zhongkai Harbin Institute of Technology , Harbin , China

金属学报(英文版)

The SiC_w/Al composite prepared by squeeze casting has a combination of superior room temperature specific strength and modulus together with excellent thermal properties.The extrusion can make an improvement on the strength and ductility of the composite from 582 MPa as squeeze casted up to 639 MPa,and on the transformation from isotropic to the anisotropic structure.This seems to be explained by the orientation of whiskers and the densification of dislocations in matrix.TEM observation indicates that the stacking fault is the usual planar defect on the SiC_w surface. composite;;SiC whisker;;Al alloy;;microstructure

关键词: composite , null , null , null

CRYOGENIC MECHANICAL BEHAVIOUR OF MARAGING STEEL CONTAINING HYDROGEN

LIU Zhonghao CHEN Lian Institute of Metal Research , Academia Sinica , Shenyang , China

金属学报(英文版)

Within the range of 77 to 295 K,the strength and plastieity of 18Ni maraging steel increase with decreasing temperature and decrease with increasing hydrogen content.The susceptibility to hydrogen embrittlement of the maraged specimens is superior to solid solution ones.The dislocations after plastically deforming will tangle into dislocation cells which reduce thermselves in size as the temperature decreases,and coarsen as the hydrogen content in- creases.No cryogenie deformation twin was found.The tensile fracture surfaces of the solu- tion and maraged specimens containing 5.90 ppm hydrogen under 295 to 223 K are revealed as quasi-cleavage and intergranular features respectively and as transgranular ones under other experimental conditions.The influence of hydrogen on the mechanical behaviour of steel and the mechanism of hydrogen induced deformation and fracture are discussed. Research Assistant, Institute of Metal Research,Academia Sinica, Shenyang 110015,China

关键词: maraging steel , null , null , null

SYNTHESIS OF TiN FILM WITH ION BEAM ENHANCED DEPOSITION AND ITS PROPERTIES

ZHOU Jiankun LIU Xianghuai CHEN Youshan WANG Xi ZHENG Zhihong HUANG Wei ZOU Shichang Shanghai Institute of Metallurgy , Academia Sinica , Shanghai , China

金属学报(英文版)

The TiN films were synthesized with an alternate process of depositing titanium from a E-gun evaporation source and 40 keV N~+ bombarding onto the target.It is shown from the composi- tion analysis and structure investigations using RBS,AES,TEM,XPS and X-ray diffraction spectrum that the formed fihns are mainly composed of TiN phase with grain size of 30—40 nm and without preferred orientation,the nitrogen content in the film is much less than that in case without N~+ bombarding,and an intermixed region about 40 nm thick exists between the film and the substrate.The films exhibt high microhardness and low friction. ZHOU Jiankun,Ion Beam Laboratory,Shanghai Institute of Metallurgy,Academia Sinica, Shanghai 200050,China

关键词: TiN film , null

METALLOGRAPHIC STUDY ON SEGREGATION BEHAVIOUR OF P IN COLD-ROLLED Fe-P ALLOYS DURING ANNEALING

NING Hua ZHANG Lixin Institute of Corrosion and Protection of Metals , Academia Sinica , Shenyang , China

金属学报(英文版)

The segregation behaviour of P and its effect on structure of 70%-reduction cold rolled Fe-P alloys containing different contents of P,e.g.,0.007,0.06 and 0.09% P,during annealing at 200-700℃ under vacuum have been studied by means of metallography and EPMA.The P was found to segregate preferentially along dislocation line during recovery annealing.The P-riched dislocation densing region,the P-depleted region and the sub-grain-like boundary thus formed.The nuclei grow preferentially during recrystallization in such region that the P segregation is more evident and the residual strain by dislocation densing increases to large extent.After recrystallizing,the P segregates along grain boundaries and makes the grains in alloy fine. Engineer,Institute of Corrosion and Protection of Metals,Academia Sinica,Shenyang 110015,China

关键词: P , null , null , null

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