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MICROSTRUCTURE AND MECHANICAL PROPERTIES OF RAPIDLY SOLIDIFIED Al-Fe BASED ALLOYS

W.J. Park , S. Ahn , R. Schmees , and Nack J. Kim(1)(Center for Advaned Aerospace Materials , POSTECH. Pohang 790-784 , Korea )2)(Research Institute of industrial Science & Technology , Pohang 790-600 , Korea )3)(Pratt and Whitney , West Palm Beach , FL , USA Manuscript received 26 August 1996)

金属学报(英文版)

The effects of additions of Ti and W on microstructure and mechanical properties of rapidly solidified Al-Fe-V-Si alloys were investigated. Alloy powders were produced by the centrifugal rotary atomization process. After atomization, powders were screened to various mesh sizes to see the effect of powder size on the mechanical properties.These Powders were consolidated into billets using conventional powder metallurgy process, and then extruded into bar form.Microstructural analysis shows that the W addition results in the heterogeneous microstructure.On the other hand, the Ti addition refines the microstructure.Alloy containing both Ti and W has the highest thermal stability of the dispersoid. These variations in the microstructure are well reflected in the mechanical properties in that the Ti containtng alloys (with or without W) have the higher strength and ductility than the W containing alloy. It also shows that the alloys made of the coarser powders have better combinations of strength and ductility than those made of the finer powders.

关键词: :rapid solidification , null , null

RECENT DEVELOPMENTS IN AEROSPACE PROPULSION MATERIALS

T. Khan(Onera , B.P. 72 , 92322 Chatillon Cedex , France Manuscript received 26 August 1996)

金属学报(英文版)

This paper describes the key role played by superalloys in aerospace propulsion. Turbopump blades in liquid rocket engines operating under severe thermal and environmental conditions require the development of specific materials.A new superalloy,THYMONEL 8, developed by ONERA in collaboration with SEP is shown to possess a set of properties required for advanced rocket engines. For future civil aircraft engines, the development of compressor and turbine disk materials operating at still higher temperatures requires a greater contrul of the grain size,which has to be increased for improved creep resistance and higher damage tolerance. Work carried out at ONERA emphasizes the importance of high temperature deformation conditions, especially the strain rate, for obtaining a uniform grain growth.

关键词: :superalloy , null , null , null , null

R & D ACTIVITIES ON AEROSPACE MATERIALS IN KOREA

H.M. Kim(Korea Institute of Machinery and Materials , Korea Manuscript received 26 August 1996)

金属学报(英文版)

This paper briefly reviews research and development programs in Korean aerospace industry,with an emphasis on aircraft materials technology. International collaborations in these areas are outlined and the R & D activities are highlighted against the background of the national economy.It is shown that the investment from government agencies and large enterprises has led to healthy development of aerospace materials industries in Korea.

关键词: :R & D , null , null , null

ELIMIMATION OF RANDOM DEFACTS IN AEROSPACE MATERIALS

A. Mitchell Advanced Materials Research Laboratory , University of British Columbia , Vancouver BC , Canada

金属学报(英文版)

In the pastfew years,severalnew melting processeshavebeenindustrialised forthe produc tion ofsuperalloys,titanium alloysand high qualitysteelsfor useintheaero engineindustry.Theseincludeelectron beam , plasma,inductionskull,andthe”triple melt”process( VIM + ESR+ VAR) . These developments have allbeen instituted in responsetothe major per ceived problem oftheindustry ;that oftheincidence of random defectsin the alloys whichcause problemsinregardto predictablelifing ofthefinished partinservice. Thedirectconse quenceofthe uncertaintyislossof revenue due to premature retirement of parts which mayhavecompleted on a fraction oftheir actualservicelife; a conservatism on the partof design parameters whichleadsto uneccesary weightin thepart;and ariskofeitherservicefailuresor partrecalls whichinterruptengine performance. Thebenefitsoftheprocesschangesinrespectoftheproducts’absolute propertiesand alsoonthereproducibility and inspectability ofthose properties have been substantial. Itisclearthattheprocesses offer the industry a solution to the present dilem ma of how to treatthe ”rare”defectsfrom the pointof view of fracture mechanicslifing methodology. The use ofprocesscontrols which guarantee”zero defect”productisdevelopingintoacriticaltoolfortheextension oftherangeof a given alloy’s use. Itislikelyto permit very substantial gainsinboth componentlife and intheallowablestressin rotating parts withoutthe needtointroduce new materials carrying new problems of user confidence, production reliability and data base. Weconcludethatthenew processesareatastageof development wherethey arereadyforwideindustry usein production. They will not add significantly tothecomponentcost andthey willgive a renwed lifespan to the more familiar materials and methodsof aero engineconstruction.

关键词:

Optical absorption and EPR study of the octahedral Fe3+ center in yttrium aluminum garnet

Physical Review B

The optical-absorption and EPR spectra of octahedral Fe3+ center in yttrium aluminum garnet have been studied by diagonalizing the complete energy matrices for a d(5) configuration ion in a trigonal ligand field. It is shown that the local lattice structure around an octahedrally coordinated Fe3+ center has an expansion distortion. The expansion distortion may be attributed to the fact that the radius of Fe3+ ion is larger than that of Al3+ ion, and the Fe3+ ion will push the oxygen ligands outwards. Simultaneously, the local lattice structure distortion parameters Delta R=0.0907 A and Delta theta=1.940 degrees for the octahedral Fe3+ center in the crystal are determined. From optical spectra calculation, we confirm that two strong sharp transitions at 407 and 415 nm, which are apparent in the optical absorption spectra for lightly doped YAG:Fe3+ system, should be ascribed to the tetrahedral Fe3+ center. This is also in accord with the conclusion of Rotman [J. Appl. Phys. 66, 3207 (1989)].

关键词: electron-paramagnetic-resonance;crystals;field;ion;parameters;impurities;fe-3+

应力对1J79软磁合金强场磁导率的影响

尔延徽 , 毛昌辉 , 杨志民 , 杜军

稀有金属 doi:10.3969/j.issn.0258-7076.2007.06.008

采用8232型B-H交流回线仪对受力前后的1J79软磁合金在不同场强和频率下磁导率的变化进行了研究, 通过XRD对材料受力前后微观结构变化进行了分析. 研究表明: 场强在1~10 A·m-1范围内, 直流条件下受应力1J79合金的相对磁导率远低于不受应力1J79合金的相对磁导率; 交流条件(5~30 kHz)下受应力1J79合金的相对磁导率低于不受应力1J79合金的相对磁导率, 但低于直流条件下的降低幅度. 1J79合金受力后, 使有利于磁性能(111)晶面取向大大减少, 是合金受力后相对磁导率下降的主要原因.

关键词: 应力 , 强场 , 1J79软磁合金 , 相对磁导率

深低温条件下1J30的马氏体转变研究及TEM分析

宁波 , 赵宇 , 李春志 , 李波

物理测试

1J30升温和降温过程分析得出,深低温条件下1J30的马氏体转变为不可逆转变。同时,对1J30内马氏体衍射斑点分析得出:有许多平行的极薄的马氏体片生成;马氏体与奥氏体的位相关系符合“西山关系”。对软磁材料中的马氏体研究具有一定的意义。

关键词: 马氏体转变 , crystallographic orientation , twins

深低温条件下1J30的马氏体转变研究及TEM分析

宁波 , 赵宇 , 李春志 , 李波

物理测试

1J30升温和降温过程分析得出,深低温条件下1J30的马氏体转变为不可逆转变.同时,对1J30内马氏体衍射斑点分析得出:有许多平行的极薄的马氏体片生成;马氏体与奥氏体的位相关系符合"西山关系".对软磁材料中的马氏体研究具有一定的意义.

关键词: 马氏体转变 , 位向关系 , 孪晶

数理统计方法在1J85软磁合金生产中的应用

段晓昆 , 姜燕 , 胡军

金属功能材料

本文介绍了利用数理统计方法中的相对频数曲线,统计、分析实际生产中1J85软磁合金主要化学成分的分布情况,找出影响1J85软磁合金初始磁导率的因素,并采取了相应的改进措施,使1J85软磁合金产品的初始磁导率有了显著的提高.

关键词: 数理统计 , 相对频数曲线 , 1J85软磁合金 , 初始磁导率

不同热处理方法对1J50合金软磁性能影响研究

张燕阳 , 王德义 , 詹晓梅 , 谭常灵

材料开发与应用 doi:10.3969/j.issn.1003-1545.2012.02.006

1J50软磁合金良好的磁性能主要是通过合适的热处理工艺方法得到的,用金相显微镜、XRD等对不同热处理工艺的1J50软磁合金的组织结构进行了分析,用MATS - 2010SA软磁测试仪对1J50软磁合金的磁性能进行了检测.结果表明,不同热处理工艺方法得到的1J50软磁合金组织和性能存在比较明显的差异.氢气气氛热处理得到的合金软磁性能优异.

关键词: 热处理 , 1J50合金 , 组织结构 , 性能

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