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In-situ Observation of Initiation and Propagation of Cleavage Microcrack in TiAl

Kewei GAO , Qizhi CHEN , Wuyang CHU and Chimei Hsiao(Dept.of Materials Physics , University of Science and Technolgy Beijing , Beijing , 100083 , China)

材料科学技术(英文)

Nucleating and propagating of nancrack formed in dislocation free zone (DFZ) for the brittle TiAl alloy has been studied through in-situ tensile test in TEM and analyzed using microfracture mechanics. The resufts show that a lot of dislocations can be emitted from a crack tip when the applied stress intensity Kla i5 larger than the stress intensity for dislocatin emission Kle=1.4 M Pa·m1/2 and a dislocation free zone, which smetimes is a close zone, can form after reaching equilibrium. The DFZ is a elastic zone with large strain and then the stress in the DFZmight equal to the cohesive strength σth because the crack tip is still sharp. When Kla is larger than the stress intensity for nanocrack nucleation Kli =2.4 M Pa·m1/2, the stress within a certain range in the DFZ would equal to σth and then a nanocrack initiates in the DFZ or sometimes at the notch tip. The nanocrack formed in the DFZ is stable and can propagate a small distance in cleavage mode through multiplication and movement of dislocation in the plastic zone, during keeping constant displacement. Increasing Kla can make the crack stably propagate continuously or discontinuously and it means that the stre5s intensity for crack propagation, Klp, is larger than Kli. Therefre, Kle

关键词:

CORRELATION BETWEEN STRESS COMPONENTS AND STRESS CORROSION CRACKS IN BRASS Lecturer,Department of Materials Physics,University of Science and Technology Beijing,Beijing 100083,China

QIAO Lijie LIU Rui XIAO Jimei University of Science and Technology Beijing , Beijing , China

金属学报(英文版)

The effects of stress components on nucleation sites and propagation directions of stress cor- rosion cracks in brass were investigated with specimens under mode Ⅱ and mode Ⅲ loadings. The results indicated that under mode Ⅱ loading,stress corrosion cracks nucleated on the site with maximum normal stress component and propagated along the plane perpendieular to the maximum normal stress,under mode Ⅲ loading,the stress corrosion crack was not evident on the 45°plane due to the general corrosion in aqueous solution with high NH_4OH concentra- tion,while stress corroded in aqueous solution with low NH_4OH concentration, numerous cracks with spacings of 10—150μm were found on the 45°plane with maximum normal stress and no stress corrosion cracks was observed on the plane with maximum shear stress.

关键词: stress corrosion cracking , null , null , null

Stereology in Materials Science

LIU Guoquan Department of Materials Science and Engineering , University of Science and Technology Beijing , 100083 , China.

材料科学技术(英文)

Quantitative analysis of populations having a geometric structure,which has developed into a special scientific subject called microstructology or stereology,is of great importance to the characterization and evaluation of microstructures and their evolution in various processes.This paper, besides a brief discussion on those topics such as the recent developments of computer assisted image analysis,mathematical morphology,and fractal analysis,will mainly focus on the scope,fundamen- tals,present status,and perspectives of classical stereology.Several case examples of its application to materials science will also be given.

关键词: stereology , null , null , null

Laser-Heated Diamond-Anvil Cell (LHDAC) in Materials Science Research

N.V.Ch , ra Shekar , P.Ch.Sahu , K.Govinda Rajan

材料科学技术(英文)

Laser-heated diamond-anvil cell (LHDAC) is emerging as the most suitable, economical and versatile tool for the measurement of a large spectrum of physical properties of materials under extreme pressure and temperature conditions. In this review, the recent developments in the instrumentation, pressure and temperature measurement techniques, results of experimental investigations from the literature were discussed. Also, the future scope of the technique in various avenues of science was explored.

关键词: Laser heating , null , null , null

CURRENT STATUS OF HIGH-RESOLUTION ELECTRON-MICROSCOPY AND ITS APPLICATIONS TO MATERIALS SCIENCE AND CONDENSED MATTER PHYSICS

材料科学技术(英文)

The present paper summarizes the current status of high resolution elect;on microscopy ( HREM) and the applications of HREM to materials science and condensed matter physics. This review recounts the latest development of high resolution electron microscope, progress of HREM and the applications of HREM, including the crystal structure determination of microcrystalline materials and characterization of the local structure of the defects and nanostructured materials as well as qualitative and quantitative analysis of the grain boundaries, interfaces and interfacial reactions in the advanced materials by means of HREM in combination with electron diffraction, subnanometer level analysis, image simulation and image processing.

关键词: juxtaposed pentagonal antiprisms;two-dimensional quasicrystal;domain;boundary structures;close-packed phases;nanocrystalline materials;crystal-structure;copper oxidation;initial-stage;translational;symmetry;rotational symmetry

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