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In-situ TEM Observation of Dislocation Emission, Multiplication and Motion Induced by Anodic Dissolution in Type 310 Stainless Steel

Yizhong HUANG , Qizhi CHEN and Wuyang CHU (Dept. of Materials Physics , Univrsity of Science and Technology Beijing , Beijing 100083 , China)(To whom correspondence should be addressed)

材料科学技术(英文)

A special constant deflection device for TEM has been designed and then the dislocation configuration change ahead of a loaded crack tip after corrosion or anodic dissolution for some time but before the initiation of SCC can be observed in TEM. The results showed that anodic dissolution during SCC of a type 310 stainless steel in deionized water could promote dislocation emission,multiplication and motion before the initiation of SCC.

关键词:

CURRENT STATUS OF HIGH-RESOLUTION ELECTRON-MICROSCOPY AND ITS APPLICATIONS TO MATERIALS SCIENCE AND CONDENSED MATTER PHYSICS

材料科学技术(英文)

The present paper summarizes the current status of high resolution elect;on microscopy ( HREM) and the applications of HREM to materials science and condensed matter physics. This review recounts the latest development of high resolution electron microscope, progress of HREM and the applications of HREM, including the crystal structure determination of microcrystalline materials and characterization of the local structure of the defects and nanostructured materials as well as qualitative and quantitative analysis of the grain boundaries, interfaces and interfacial reactions in the advanced materials by means of HREM in combination with electron diffraction, subnanometer level analysis, image simulation and image processing.

关键词: juxtaposed pentagonal antiprisms;two-dimensional quasicrystal;domain;boundary structures;close-packed phases;nanocrystalline materials;crystal-structure;copper oxidation;initial-stage;translational;symmetry;rotational symmetry

Current Status of High Resolution Electron Microscopy and Its Applications to Materials Science and Condensed Matter Physics

Douxing LI and Hengqiang YE (Laboratory of Atomic imaging of Solids , Institute of Metal Research , Chinese Academy of Sciences , Shenyang , 110015 , China)

材料科学技术(英文)

The present paper summarizes the current status of high resolution electron microscopy (HREM)and the applications of HREM to materials science and condensed matter physics. This review recounts the latest development of high resolution electron microscope, progress of HREM and the applications of HREM, including the crystal structure determination of microcrystalline materials and characterization of the local structure of the defects and nanostructured materials as well as qualitative and quantitative analysis of the grain boundaries, interfaces and interfacial reactions in the advanced materials by means of HREM in combination with electron diffraction,subnanometer level analysis, image simulation and image processing.

关键词:

DEPT135测定Resol的组成及微细结构参数

杨金瑞 , 余尚先 , 顾江楠

高分子材料科学与工程

通过对resol(羟甲基酚化合物和低分子量羟甲基酚树脂)DEPT135图谱的分析讨论,得到一系列计算resol微细结构参数的经验公式.根据DEPT135图谱可判断是否发生缩聚反应,根据经验公式可计算酚单体各个活性点参与反应百分率或酚羟基导入率、不同类型缩聚所占百分率及低分子量羟甲基酚树脂的平均核体数.

关键词: 羟甲基酚化合物 , 羟甲基酚树脂 , DEPT135 , 结构参数

Chen系统的状态变量周期性反馈控制

李开明 , 李亚洲 , 冯维贵 , 林长

量子电子学报 doi:10.3969/j.issn.1007-5461.2007.05.014

采用非线性反馈控制,用附加了带参数的正弦项对Chen系统进行了有效的控制.随着参数k的逐渐增大,系统的动力学行为呈现出一系列的变化.数值研究结果表明:随控制参数的增大,驱动信号的强度渐大,混沌系统由混沌运动到周期轨道,最终到一相点.

关键词: 混沌 , Chen系统 , 不动点 , Lyapunov指数 , 反馈控制

CORRELATION BETWEEN STRESS COMPONENTS AND STRESS CORROSION CRACKS IN BRASS Lecturer,Department of Materials Physics,University of Science and Technology Beijing,Beijing 100083,China

QIAO Lijie LIU Rui XIAO Jimei University of Science and Technology Beijing , Beijing , China

金属学报(英文版)

The effects of stress components on nucleation sites and propagation directions of stress cor- rosion cracks in brass were investigated with specimens under mode Ⅱ and mode Ⅲ loadings. The results indicated that under mode Ⅱ loading,stress corrosion cracks nucleated on the site with maximum normal stress component and propagated along the plane perpendieular to the maximum normal stress,under mode Ⅲ loading,the stress corrosion crack was not evident on the 45°plane due to the general corrosion in aqueous solution with high NH_4OH concentra- tion,while stress corroded in aqueous solution with low NH_4OH concentration, numerous cracks with spacings of 10—150μm were found on the 45°plane with maximum normal stress and no stress corrosion cracks was observed on the plane with maximum shear stress.

关键词: stress corrosion cracking , null , null , null

Dependence of strength, elongation, and toughness on grain size in metallic structural materials

Journal of Applied Physics

The dependence of yield strength, uniform elongation, and toughness on grain size in metallic structural materials was discussed. The toughness is defined as the product of yield strength and uniform elongation. The yield strength versus grain size can be well described by the Hall-Petch relation; however, the uniform elongation versus grain size is not well understood yet. A simple model involving the densities of geometrically necessary dislocations and statistically stored dislocations was proposed to estimate the uniform elongation versus grain size. Existing data for low carbon steels and aluminum indicate that, in the grain size less than 1 mu m, the materials usually exhibit high strength and low uniform elongation and, in the grain size greater than 10 mu m, the materials usually exhibit low strength and high elongation; in either case the toughness is low. However, in the grain size of several micrometers, the toughness is the highest. It is suggested that we should pay more attention to develop the metallic materials with grain size of several micrometers for structural applications. (c) 2007 American Institute of Physics.

关键词: nanocrystalline copper;nanostructured metal;steels;deformation;ductility;law

Advanced Materials for Energy Storage

Advanced Materials

Popularization of portable electronics and electric vehicles worldwide stimulates the development of energy storage devices, such as batteries and supercapacitors, toward higher power density and energy density, which significantly depends upon the advancement of new materials used in these devices. Moreover, energy storage materials play a key role in efficient, clean, and versatile use of energy, and are crucial for the exploitation of renewable energy. Therefore, energy storage materials cover a wide range of materials and have been receiving intensive attention from research and development to industrialization. In this Review, firstly a general introduction is given to several typical energy storage systems, including thermal, mechanical, electromagnetic, hydrogen, and electrochemical energy storage. Then the current status of high-performance hydrogen storage materials for on-board applications and electrochemical energy storage materials for lithium-ion batteries and supercapacitors is introduced in detail. The strategies for developing these advanced energy storage materials, including nanostructuring nano-/microcombination, hybridization, pore-structure control, configuration design, surface modification, and composition optimization, are discussed. Finally, the future trends and prospects in the development of advanced energy storage materials are highlighted.

关键词: lithium-ion batteries;carbon nanotube electrodes;enhanced hydrogen;storage;metal-organic frameworks;double-layer capacitors;n-h system;carbide-derived carbons;ammonia borane dehydrogenation;ordered;mesoporous carbons;high-rate performance

REVIEW OF THE RESEARCHES ON MAGNETOSTRICTIVE MATERIALS

Y. Li and Chong-Oh Kim(Department of Materials Engineering , Chungnam National University , Taejon 305-764 , Korea)

金属学报(英文版)

The recent evolution in researeh on the magnetostrictive materials is briefly reviewed.A cotnpaboon of the relative preperties between bulk and thin film materialS, and theeNcts of addition of elements on the magnetic properties are alSo given.

关键词: magnetostriction , null , null

Stereology in Materials Science

LIU Guoquan Department of Materials Science and Engineering , University of Science and Technology Beijing , 100083 , China.

材料科学技术(英文)

Quantitative analysis of populations having a geometric structure,which has developed into a special scientific subject called microstructology or stereology,is of great importance to the characterization and evaluation of microstructures and their evolution in various processes.This paper, besides a brief discussion on those topics such as the recent developments of computer assisted image analysis,mathematical morphology,and fractal analysis,will mainly focus on the scope,fundamen- tals,present status,and perspectives of classical stereology.Several case examples of its application to materials science will also be given.

关键词: stereology , null , null , null

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