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STUDY ON THE TENSILE FATIGUE DAMAGE OF QUASI—ISOTROPIC COMPOSITE LAMINATES

I.G.Kim , I.S.Kim

金属学报(英文版)

Quasi-isotropic laminates have isotropic elastic properties in all yn-plane directions.Therefore,this kind of laminate is widely used for structural elements.The simplest stacking sequence of quasi-isotropic laminates is[0/-60/60]s.When the direction of applied axial lood to[0/-60/60]s laminate is inclined at a 30-degree angle,we have the other quasi-isotropic laminate [30/-30/90]s under axial load.The failure mecha-nisms of these two lamibnates are,however,entirely different from each other because these two laminates have different distribution of the interlaminar stresses.It was confirmed by tensile fatigue tests that the [0/-60/60]s laminate does not show any vis-ible fatigue damage,but the[30/-30/90]s laminate develops edge-delamination

关键词: composite , null , null

Microstructural Evolution in Directionally Solidified Ni-Base Superalloy IN792+Hf

S.M.Seo , I.S.Kim , J.H.Lee , C.Y.Jo , H.Miyahara , K.Ogi

材料科学技术(英)

Microstructural evolution during directional solidification (DS) of Ni-base superalloy IN792+Hf has been investigated with an emphasis on the γ′ precipitates and MC-type carbides. The quantitative image analyses revealed that the increase in the solidification rate up to 100 μm/s at constant thermal gradient of 178 K/cm resulted in a fine and uniform distribution of γ′ precipitates. The relationship between the as-cast γ′ size and cooling rate was also determined for DS IN792+Hf. In the mean time, the MC carbide size was found to be dependent both on the solidification rate and the S/L interface morphology while the area fraction of MC carbide was significantly influenced by the S/L interface morphology.

关键词: IN792 , null , null , null

Fe-Ti-N合金α相区淬火的S-I交互内耗峰

葛庆麟 , 施天生 , 陈廷国 , 陈源 , 吴自良

金属学报

四种不同Ti浓度的Fe-Ti合金,加氮到N/Ti>1之后,发现有两个内耗峰,并且随氮浓度之增加而同时升高。20℃处的峰是氮的Snoek峰,160℃附近的是s-i峰。s-i峰的峰高和Ti浓度成线性关系,表明起峰的反应只涉及孤立的Ti原子,与Ti-Ti原子对或杂质原子团都无关系。 提出了产生s-i峰的二种缺陷中心——Ti-N对缺陷和N-Ti-N仨缺陷——的模型(图7)。氮占Ti位就构成对缺陷,其中的Ti,N原子亲和力很强,只要合金中尚存有自由Ti原子,就不可能存有自由氮原子,因此N/Ti≤1以下,不会出现Snoek峰或s-i峰。N/Ti>1之后,多余氮原子要在对缺陷的OⅡ位和T_3位之间以约1:10的比例进行分配,直到绝大部分的对缺陷转化为仨缺陷。N/Ti(?)2以后,几乎所有的多余氮都进入了仨缺陷的OⅡ位,此时s-i峰的弛豫强度突然增加10倍。 淬火时冻结在α-Fe基体中的过饱和氮、要扩散到OⅡ位(扩散距离~10(?)),以期达到室温下的再分配,因此引起Snoek峰室温下的迅速衰减。s-i峰的形状,只取决于多余氮的浓度,与淬火温度、冷却速度无关。

关键词:

Xe I原子6s[3/2]2亚稳态寿命的理论研究

董晨钟 , 颉录有 , Stephan Fritzsche

原子核物理评论 doi:10.3969/j.issn.1007-4627.2002.02.001

利用多组态Dirac-Fock(MCDF)理论方法, 系统地研究了延迟和相关效应对中性XeI原子5p56s[3/2]2-5p6 1S0(M2)辐射跃迁的影响, 给出了亚稳态6s[3/2]2的辐射寿命. 与最新的磁光阱实验观测结果比较, 目前的计算不仅大大提高了理论计算的精度, 而且解释了实验和以往理论偏差非常大的原因.

关键词: MCDF方法 , 延迟和相关效应 , 辐射寿命

Er3+掺杂的 MFT玻璃材料2H11/2、4S3/2→4I15/2荧光性质

陈宝玖 , 吕少哲 , 黄世华

无机材料学报 doi:10.3321/j.issn:1000-324X.2001.02.006

计算了Er3+掺杂的氟氧化物玻璃材料MFT的J-O参数,进而获得了一些能级间跃迁的跃迁几率、分支比、及寿命等数据.测量了室温下Er3+的较强的两个绿色发射2H11/2、4S3/2→4I15/2及红色发射4F9/2→4I15/2的激发光谱,观测了2H11/2、4S_3/2→4I15/2跃迁荧光强度随着温度的变化,测量了室温下这两个跃迁衰减曲线,计算了这两个能级的无辐射跃迁几率及量子效率.

关键词: MFT玻璃 , J-O理论 , 量子效率 , 无辐射跃迁

Er3+掺杂的MFT玻璃材料2H11/24S3/24I15/2荧光性质

陈宝玖 , 吕少哲 , 黄世华

无机材料学报

计算了Er3+掺杂的氟氧化物玻璃材料MFT的J-O参数,进而获得了一些能级间跃 迁的跃迁几率、分支比、及寿命等数据.测量了室温下Er3+的较强的两个绿色发射2H11/24S3/24I15/2及红色发射9/215/2的激发光谱,观测2H11/24S3/24I15/2跃迁 荧光强度随着温度的变化,测量了室温下这两个跃迁衰减曲线,计算了这两个能级的无辐射跃 迁几率及量子效率.

关键词: MFT玻璃 , J-O theory , quantum efficiency , non-radiative transition

新型硫卤玻璃GeS2-Ga2S3-AgX(X=Cl,Br,I)中的K+-Ag+离子交换

王德强 , 陈玮 , 程继健

硅酸盐通报 doi:10.3969/j.issn.1001-1625.2006.06.012

以油酸钾为熔盐,GeS2-Ga2S3-AgX(X=Cl,Br,I)玻璃为基玻璃,在270℃的环境温度下,以氮气作为保护气氛,成功地进行了K+-Ag+离子交换.在50GeS2-25Ga2S3-25AgI玻璃中,K+离子的交换深度可达256μm,并对交换深度、离子扩散系数以及离子浓度之间的规律进行了初步研究.通过离子交换研究,为制备硫卤玻璃光波导奠定了基础,并可以进一步拓宽硫卤玻璃的应用前景.

关键词: 硫卤玻璃 , 离子交换 , 光波导 , 浓度分布

从FeSe_(0.5)Te_(0.5)的V~I曲线论磁通动力学的诸模型

左鸣 , 谭舜 , 于一 , 张志涛 , 皮雳 , 张庶元

低温物理学报

高温超导体的发现动摇了支配磁通动力学二十几年的Kim-Anderson模型.于是人们提出了新的涡旋玻璃态模型,集体钉扎模型和U~j对数关系模型来描述高温超导体的磁通动力学.其中,涡旋玻璃态模型已被人们广泛接受.Fe基超导体发现后,人们它行为十分类似于高温超导体.我们实验上仔细研究了FeSe0.5Te0.5单晶的V~I关系曲线,发现上述诸模型均不能很好的解释我们的实验结果,而张的反跳模型恰能很好的拟合实验结果.本文讨论了诸模型对高温超导体磁通动力学描述的适用性并给出合理的解释.

关键词: 高温超导体 , 磁通蠕动 , 涡旋钉扎

Preparation of I_2 Clusters and Their Absorption Spectra

Zhaojun LIN , Zhanguo WANG , Wei CHEN and Lanying LIN(Lab. of Sendconductor Materials Science , Institute of Semiconductors , Chinese Academy of Sciences , Beijing 100083 , China)

材料科学技术(英)

Samples have been prepared at different temperatures by loading I2 molecules into the cages of zeolite 5A, and the measurements of the absorption spectra have been carried out for the prepared samples. It is shown that I2 molecular clusters are formed in the cages of zeolite 5A,and it is also found that moIecuIar clusters which are bonded with intermoIecuIar forces have an important feature, namely, the intermolecular distance in molecular clusters can be changed on different preparing conditions and the blue shift of absorption edges can not be as the criterion of forming molecular clusters.

关键词:

Galvanostatic electrodeposition and microstructure of copper (I) oxide film

Materials Research Innovations

Polycrystalline copper (I) oxide films were deposited on stainless steel substrate by galvanostatic electrodeposition method and were characterized by Xray diffraction and scanning electron microscopy. The effect of bath temperature, bath pH and current density on the compositon, grain size, surface texture and surface morphology of the electrodeposited films were investigated. The films deposited at low bath pH (less than or equal to 7) consisted of copper (I) oxide and metallic copper; while the films deposited at bath pH between 8 and 12 and bath temperature of 60 degrees C were pure copper (I) oxide. The preferred orientation of the copper (I) oxide films depended on the relative growth rate of (111) and (200) faces and could be controlled by adjusting the bath pH and/or the cathodic current density. (100)-oriented copper (1) oxide films could be deposited at pH=9 and current densities in the range of 0.25-1 mA/cm(2) while (111)-oriented films could be prepared at pH=12 or at pH=9 using the current densities between 1.5-2.5 mA/cm(2). Computer simulated crystallite shapes showed that the crystal shape changed from octahedral for (100)-oriented film to trucated pyramids and cubs for (111)-oriented film. And they were approved by scanning electron microscopy.

关键词: copper(I) oxide;electrochemical deposition;thin films;microstructure;electrochemical synthesis;thin-films

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