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CHARACTERIZATION OF MECHANICALLY ALLOYED Ni-Al-Ti COMPOUNDS

LIU Zhiguang , GUO Jianting , HU Zhuangqi (National Key Laboratory for RSA and Department of Superalloy and Special Casting , Institute of Metal Research , Chinese Academy of Sciences , Shenyang 110015) , China

金属学报(英文版)

Based on the previous work on the mechanical alloying of Ni-Al-Ti compounds. the mechanically alloyed Ni-Al-Ti compounds was characterized. The results show that with the increase of Ti content. the microhardness of the final products decrease apparently. The thermal behavior of the resultant Ni-Al-Ti compounds shows significant difference, the as-milled powders with different Ti content transform into different products after healing.So the microstructure of the milled alloys could be determined through adequate control of composition and heat treatments.

关键词: : mechanical alloying. Ni-Al-Ti , null

Effect of Casting Modulus on Microstructure and Segregation in K441 Superalloy Casting

Weiguo Jiang

材料科学技术(英文)

Four castings with different modulus have been designed to simulate different thickness sections of a turbine blade during casting process. The microstructure has been observed by optical microscopy (OM) and scanning electron microscopy (SEM). The micro-segregation was tested by energy dispersive spectroscopy (EDS) and the macro-segregation was analyzed by using Metalscan 2500 spectrometers. The experimental results show that the microstructure of casting is affected by modulus apparently. The smaller the modulus, the finer the microstructure. The average grain size of castings with modulus of 0.29, 1.57, 3.16 and 5.0 mm is 0.3, 1.5, 2.7 and 4.3 mm, and the volume fraction of eutectic is 0, 0.1%, 0.2% and 1.0%, respectively. The micro/macro segregation is affected by the modulus apparently. The smaller the modulus, the lower the segregation level. When the modulus of casting increases, the content of Al increases, while the content of W, Cr and Mo decreases both in inner grain and near grain boundary. The content of Al and Mo in inner grain is higher than that near grain boundary, while the content of Cr and W in inner grain is lower than that near grain boundary.

关键词: Superalloy

Effect of Casting Modulus on Microstructure and Segregation in K441 Superalloy Casting

材料科学技术(英文)

Four castings with different modulus have been designed to simulate different thickness sections of a turbine blade during casting process. The microstructure has been observed by optical microscopy (OM) and scanning electron microscopy (SEM). The micro-segregation was tested by energy dispersive spectroscopy (EDS) and the macro-segregation was analyzed by using Metalscan 2500 spectrometers. The experimental results show that the microstructure of casting is affected by modulus apparently. The smaller the modulus, the finer the microstructure. The average grain size of castings with modulus of 0.29, 1.57, 3.16 and 5.0 mm is 0.3, 1.5, 2.7 and 4.3 mm, and the volume fraction of eutectic is 0, 0.1%, 0.2% and 1.0%, respectively. The micro/macro segregation is affected by the modulus apparently. The smaller the modulus, the lower the segregation level. When the modulus of casting increases, the content of Al increases, while the content of W, Cr and Mo decreases both in inner grain and near grain boundary. The content of Al and Mo in inner grain is higher than that near grain boundary, while the content of Cr and W in inner grain is lower than that near grain boundary.

关键词: Superalloy;Turbine blade;Casting modulus;Microstructure;Segregation;grain-boundary segregation;single-crystal superalloy;ni-base;superalloy;cooling rate;behaviors

THE CHANGING ROLE OF THE NATIONAL LABORATORIES IN MATERIALS RESEARCH

WADSWORTH Jeffrey and FLUSS Michael(Chemistry and Materials Science Directorate , Lawrence Livermore National Laboratory , Livermore , CA 94551)

金属学报(英文版)

The role of the National Laboratories is summarized from the era of post World War II to the present time. The U.S. federal government policy for the National Laboratories and its influence on their materials science infrastructure is reviewed with respect to .determining overall research strategies, various initiatives to interact with industry (especially in recent years),building facilities that serve the nation, and developing leading edge research in the materials sciences. Despite reductions in support for research in the U.S. in recent years, and uncertainties regarding the specific policies for Research &Development (R&D) in the U.S., there are strong roles for materials research at the National Laboratories. These roles will be centered on the abilities of the National Laboratories to field multidisciplinary teams, the use of unique cutting edge facilities, a focus on areas of strength within each of the labs,increased teaming and partnerships, and the selection of motivated research areas. It is hoped that such teaming opportunities will include new alliances with China, in a manner similar, perhaps, to those recently achieved between the U.S. and other countries.

关键词: : U.S. Materials Science. U.S. National Laboratories and Facilities , null

Key R&D activities for development of new types of wrought magnesium alloys in China

Transactions of Nonferrous Metals Society of China

Many researchers in China are actively engaged in the development of new types of wrought magnesium alloys with low cost or with high-performances and novel plastic processing technologies. The research activities are funded primarily through four government-supported programs: the Key Technologies R&D Program of China, the National Basic Research Program of China, the National High-tech R&D Program of China, and the National Natural Science Foundation of China. The key R&D activities for the development of new wrought magnesium alloys in China are reviewed, and typical properties of some new alloys are summarized. More attentions are paid to high-strength wrought magnesium alloys and high-plasticity wrought magnesium alloys. Some novel plastic processing technologies, emerging in recent years, which aim to control deformation texture and to improve plasticity and formability especially at room temperature, are also introduced.

关键词: wrought magnesium alloy;microstructure;properties;alloy designing;plastic deformation;research projects;y-zr alloys;mechanical-properties;mg-4y-4sm-0.5zr alloy;grain-refinement;rare-earth;microstructure;gd;phase;temperature;evolution

Key Problems in Microforming Processes of Microparts

Chunju WANG , Debin SHAN , Bin GUO , Jian ZHOU , Lining SUN

材料科学技术(英文)

From the viewpoint of production engineering, microforming is considered as an effective process to fabricate various microparts. Several key problems in microforming processes were investigated. A new microforming apparatus with a high stiffness piezoelectric actuator as the punch driver was developed to produce microparts. To improve the forming abilities and locate the billets, a floating microdie was designed. The size effects of the billets and die cavities on the microforming abilities were studied with upsetting and coining tests, respectively. And the isothermal microforming process of microgears was performed with the developed microforming apparatus. Several analysis methods were used to evaluate the forming quality of the microparts.

关键词: Microforming , 尺寸效应 , 微塑性成形设备 , 浮动

Numerical Simulation of Solidification Process on Single Crystal Ni-Based Superalloy Investment Castings

Jing YU

材料科学技术(英文)

Bridgman directional solidification of investment castings is a key technology for the production of reliable and highly efficient gas turbine blades. In this paper, a mathematical model for three-dimensional (3D) simulation of solidification process of single crystal investment castings was developed based on basic heat transfer equations. Complex heat radiation among the multiple blade castings and the furnace wall was considered in the model. Temperature distribution and temperature gradient in superalloy investment castings of single blade and multiple ones were investigated, respectively. The calculated cooling curves were compared with the experimental results and agreed well with the latter. It is indicated that the unsymmetrical temperature distribution and curved liquid-solid interface caused by the circle distribution of multiple turbine blades are probably main reasons why the stray grain and other casting defects occur in the turbine blade.

关键词: Directional solidification , null , null , null

PHYSICAL SIMULATION OF CONTINUOUS ROLL CASTING PROCESS

L.H. Zhan , J. Zhong , X.Q. Li , M.H. Huang

金属学报(英文版)

A series of simulating experimental studies on the rheological behavior and its influential factors of aluminum alloy in continuous roll-casting process have been explored in this paper with a Gleeble-1500 Thermal-Mechanical Simulation Tester and a set of special clamp system. Relevant rheological rules in the process of coupling transient solidification and continuous deformation of roll-casting conditions are obtained. Experimental results indicate that four different characteristic stages exist in the whole rheological process, and relative constitutive models suitable for the given conditions of continuous roll casting process have been established through multivariable linear regression analysis of the experimental data.

关键词: continuous roll-casting , null , null

A special device for viscous pressure forming: Design and implementation

Bin GUO , Xiaodong XING , Huming DAI , Ronghua LUO , Zhongren WANG

材料科学技术(英文)

A flexible special device for viscous pressure forming is designed and implemented. By using three proportional electro-hydraulic relief valves connected to a computer for precise control of releasing pressure of the medium, we can form differential pressure distribution in the die cavity. With the cooperation of programmable logical controller (PLC), computer and sensor modules in control system the device can satisfy all the requirements of the new forming process.

关键词:

Characterisation of initial atmospheric corrosion carbon steels by field exposure and laboratory simulation

Corrosion Science

The early stages of the evolution of atmospheric corrosion of carbon steels exposed in both a laboratory simulated and a natural atmosphere environment in Shenyang have been observed by in situ scanning electron microscopy. In the case of laboratory cyclic wet-dry tests, even though the chloride content level is very low, filiform corrosion is initiated in the early stage. The filiform corrosion grows in random directions, forming a network of ridges. White nodules nucleate and grow on the ridges during continued corrosion and eventually connect with each other to form the initial corrosion scale. Pits were also found on the surface beneath corrosion products. In the case of a natural atmospheric environment, both filiform corrosion and other localized corrosion, such as pitting and inter-granular attack take place in the initial stage. It is obvious that there is variety of localized corrosion in the initial stage of atmospheric corrosion. (C) 2007 Elsevier Ltd. All rights reserved.

关键词: steel;atmospheric corrosion;initial stage;localized corrosion;in-situ;iron;electrolyte;thickness

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