Chuanfang YANG and Jiayong CHEN (Institute of Chemical Metallurgy
,
Chinese Academy of Sciences
,
Beijing
,
100080
,
China)
材料科学技术(英文)
Solvent extraction of Zr(IV) with TBP in kerosene was used to precipitate precursory zirconia which was then processed to produce ultrafine zirconia powders. The powder prepared was examined and characterized with transmission electron microscopy (TEM) and X-ray diffraction (XRD). Effects of the conditions of preparation on powder properties were especially investigated.It was found the preclpitate was gel-like material with heterogeneous porosity. The gel transformed to polycrystalline particles when calcined to ultrafine powder at 600℃. The composition of the loaded organic phase and the conditions of washing the precipitate are two main factors affecting the properties of powder obtained
关键词:
崔秀岭
,
马中华
,
张陆
,
王相润
,
黄桂桥
腐蚀学报(英文)
实海飞溅区低合金钢锈层分析(摘要)崔秀岭,马中华,张陆(冶金部钢铁研究总院,北京100080)王相润,黄桂桥(青岛海洋腐蚀研究所,青岛266071)19种碳钢和低合金钢试样固定在青岛海水飞溅区栅式试验架L,经8年试验后,低合金钢15MnMoVN耐蚀性能明显优于其他十几种钢,为了弄清15MnMoVN锈层的特性,选用A3钢作对比试样,通过多种方法综合测试,研究它们的形貌、物相组成、结构及合金元素分布与耐蚀性的关系.15MnMoVN和A3钢的化学成分见表1.Tab....
关键词: