{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":2,"startPagecode":1},"records":[{"abstractinfo":"将精确测定点阵参数的单波双线和双波双线法用于符合Vegard定理的连续固溶体和有限固溶体的组分测量。推导了立方晶系连续固溶体中一种组分x与双线衍射角差δ_x的关系 x≈(δ_x-δ_0)/(δ_1-δ_0)其中δ_1,δ_0,δ_x分别为x=1,C,x时双线Bragg角的差,并从典型例子和实验上验证了这个理论方程。对偏离上述线性关系的情形,引入修正项△x,其满足抛物线方程,故最后得 x≈(δ_x-δ_0)/(δ_1-δ_0)+Δx最大4((δ_x-δ_0)(δ_1-δ_x))/(δ_1-δ_0)~2这样就消除了线性近似引入的误差。最后,简要讨论了两种方法的误差。由于整个实验只要求测量衍射角差,消除了零位和试样偏心的影响,因此方法简便、迅速、具有一定的适用性。","authors":[{"authorName":"杨传铮","id":"58297855-97df-4bdb-8316-30c97834b426","originalAuthorName":"杨传铮"},{"authorName":"<span style=\"color:red\">姜</span><span style=\"color:red\">小龙</span>","id":"62abed3b-6ea6-4c91-a8f6-3a67f69bc9dd","originalAuthorName":"姜小龙"}],"categoryName":"|","doi":"","fpage":"196","id":"93262621-2b1c-40db-918a-eab546964504","issue":"2","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[],"language":"zh","publisherId":"0412-1961_1981_2_14","title":"立方晶系固溶体组分测量的X射线双衍射线法","volume":"17","year":"1981"},{"abstractinfo":"用超临界CO2萃取生姜根茎中的<span style=\"color:red\">姜</span>油树脂,并用气相色谱-质谱联用技术对其进行了成分分析.从<span style=\"color:red\">姜</span>油树脂中分析出77种化合物,其中挥发油成分50种,主要是α-<span style=\"color:red\">姜</span>烯(22.29%)、β-倍半水芹烯(8.58%)、α-法尼烯(3.93%)、β-没药烯(3.87%)和α-姜黄烯(2.63%)等倍半萜类化合物;<span style=\"color:red\">姜</span>辣素成分27种,主要成分为6-<span style=\"color:red\">姜</span>酚(9.38%)、6-<span style=\"color:red\">姜</span>烯酚(7.59%)和分析过程中由<span style=\"color:red\">姜</span>酚类或<span style=\"color:red\">姜</span>烯酚类化合物受热分解而形成的<span style=\"color:red\">姜</span>油酮(9.24%).在<span style=\"color:red\">姜</span>辣素成分中,6-异<span style=\"color:red\">姜</span>酚、(Z)-10-异<span style=\"color:red\">姜</span>烯酚和(E)-10-异<span style=\"color:red\">姜</span>烯酚3种化合物是新发现的未见报道的化合物.实验中对这3种新化合物进行了质谱裂解分析.","authors":[{"authorName":"战琨友","id":"18029250-7538-4dbd-a479-4a7c758cfe80","originalAuthorName":"战琨友"},{"authorName":"王超","id":"e25f333c-dd8d-45ed-9015-ba6126bcf7cd","originalAuthorName":"王超"},{"authorName":"徐坤","id":"e8424cb6-b0d4-46ed-8fa2-c673af3ec31c","originalAuthorName":"徐坤"},{"authorName":"尹洪宗","id":"ec76914e-8f6c-4f7e-afaf-bbc7cda8c69f","originalAuthorName":"尹洪宗"}],"doi":"10.3321/j.issn:1000-8713.2008.06.009","fpage":"692","id":"42c1bbc0-652a-433f-8e34-86f30b7f6523","issue":"6","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"e53773ad-891b-403b-8b22-f5b0686630e3","keyword":"超临界萃取","originalKeyword":"超临界萃取"},{"id":"286cbdc0-600d-40b3-affc-527a1b3253a4","keyword":"气相色谱-质谱联用技术","originalKeyword":"气相色谱-质谱联用技术"},{"id":"7ed48749-e650-4478-96ef-9741cba04e1c","keyword":"<span style=\"color:red\">姜</span>油树脂","originalKeyword":"姜油树脂"},{"id":"bf6fde50-9a7b-42f4-953e-bf1116bcbb98","keyword":"成分分析","originalKeyword":"成分分析"}],"language":"zh","publisherId":"sp200806009","title":"气相色谱-质谱技术分析<span style=\"color:red\">姜</span>油树脂中的挥发性及非挥发性成分","volume":"26","year":"2008"},{"abstractinfo":"招平断裂南段的夏甸-<span style=\"color:red\">姜</span>家窑金矿床受断裂产状变化、断层泥、脉岩、次级断裂复合控制.矿体多赋存于蚀变分带明显、产状由缓变陡处、脉岩的下盘,并具北东侧伏及尖灭再现规律.","authors":[{"authorName":"王慧","id":"7fb4a685-ee01-4317-819a-300c21af4083","originalAuthorName":"王慧"},{"authorName":"丛成双","id":"061afad7-97f4-4639-b4cd-68988fd1f17e","originalAuthorName":"丛成双"},{"authorName":"丛培章","id":"c090b397-22b7-4f56-ba4e-2c18ca877e09","originalAuthorName":"丛培章"}],"doi":"10.3969/j.issn.1001-1277.2003.08.004","fpage":"12","id":"8bf4c3f0-63ec-49ae-a9a0-0667a8411238","issue":"8","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"10e6b959-ddde-4db4-b855-31927c89ad94","keyword":"赋存规律","originalKeyword":"赋存规律"},{"id":"cc25cee2-8e48-436f-99af-04df19dba09c","keyword":"控矿规律","originalKeyword":"控矿规律"},{"id":"6575bbc0-457d-43a2-88fc-6b2f84731b46","keyword":"夏甸-<span style=\"color:red\">姜</span>家窑金矿床","originalKeyword":"夏甸-姜家窑金矿床"}],"language":"zh","publisherId":"huangj200308004","title":"夏甸—<span style=\"color:red\">姜</span>家窑金矿床矿体赋存规律及控矿规律研究","volume":"24","year":"2003"},{"abstractinfo":"<span style=\"color:red\">姜</span>家窑金矿根据国内外矿山竖井提升现状,经过较详细地理论计算,自行设计出提升容器及配套系统,在该矿得到了应用,并取得了竖井小断面(1.8m×2.7m),卷扬机小型号(φ1.2m双卷筒卷扬机)、提升能力大(达到300～470t/d)的可喜成果,为矿山竖井开拓设计和竖井改造提供了一条可借鉴的经验.","authors":[{"authorName":"郭建军","id":"783308e8-87b6-40f3-9c39-7feb3a63137e","originalAuthorName":"郭建军"},{"authorName":"马玉山","id":"b94224e7-ec93-4950-896c-062c77ba65e2","originalAuthorName":"马玉山"},{"authorName":"贾汉义","id":"ada19182-f707-40f2-80b0-796996b18f85","originalAuthorName":"贾汉义"},{"authorName":"李勇","id":"36bfaa12-893d-443b-b747-041645e6db4e","originalAuthorName":"李勇"}],"doi":"10.3969/j.issn.1001-1277.2002.06.007","fpage":"21","id":"321851a5-c603-4614-8ce4-0bd2be6f3478","issue":"6","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"869cd681-9122-4747-ba4f-9ac4614bdc37","keyword":"竖井","originalKeyword":"竖井"},{"id":"5d0ede2b-afe1-4b9c-9648-37d619c8edb8","keyword":"提升容器","originalKeyword":"提升容器"},{"id":"43140e8c-cc3b-48d2-aa61-b07004268c15","keyword":"配套系统","originalKeyword":"配套系统"},{"id":"8430467d-ad62-43e8-aea9-26e36a7d5c72","keyword":"研究","originalKeyword":"研究"},{"id":"394bd3ab-4dde-451f-947f-57d830b95fb9","keyword":"应用","originalKeyword":"应用"}],"language":"zh","publisherId":"huangj200206007","title":"<span style=\"color:red\">姜</span>家窑金矿盲竖井提升容器及配套系统的研究与应用","volume":"23","year":"2002"},{"abstractinfo":"夏甸—<span style=\"color:red\">姜</span>家窑测区位于招平断裂带中段. 招平断裂带在该区段大致沿玲珑花岗岩与胶东群变质岩接触带展布,总体走向42°,倾向SE,倾角37°~52°. 主要金矿体赋存于招平断裂带主裂面下盘黄铁绢英岩化碎裂岩和黄铁绢英岩化花岗岩中. 本次地表构造地球化学测量面积约12 .6 km2 ,采集样品352件,测试元素包括Au、Ag、Cu、Pb、Zn、As、Sb、Hg、Mo、Bi、Mn等19种. Au元素异常与Ag和As元素异常有普遍套合性,与Cu、Pb、Zn、Sb元素异常呈局部套合性. 结合多元统计分析,测定针对深部矿体预测的构造地球化学标志Au-Ag-As,元素组合异常以及斜交参考因子得分Y( i,3)异常和Y( i,7)异常. 在现采矿区深、边部所对应的地表区域圈定出深部隐伏矿体找矿靶位4处.","authors":[{"authorName":"阚靖","id":"02776e6c-2d0c-4c48-9b41-3f220a253ca9","originalAuthorName":"阚靖"},{"authorName":"杨欣鹏","id":"1e620d36-2b91-439c-8108-8d9427ea3a83","originalAuthorName":"杨欣鹏"},{"authorName":"向胤合","id":"271df6c2-7de4-4d5b-9d30-39a2d41bd08c","originalAuthorName":"向胤合"},{"authorName":"杨斌","id":"e652f160-2b33-4865-9ec8-cd5b20be1c70","originalAuthorName":"杨斌"},{"authorName":"梁琴琴","id":"379efe08-608a-4ad3-8de7-d34b22d6060a","originalAuthorName":"梁琴琴"},{"authorName":"陈燕","id":"ecc028b7-a4da-442a-8686-2fa957658c26","originalAuthorName":"陈燕"},{"authorName":"刘庚寅","id":"c88839aa-3014-437a-865d-28f32b2129f0","originalAuthorName":"刘庚寅"}],"doi":"10.11792/hj20150504","fpage":"12","id":"75a62c02-8a0a-4531-8687-f60251820855","issue":"5","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"2f556708-0107-46c4-9134-903d60144569","keyword":"找矿预测","originalKeyword":"找矿预测"},{"id":"ea5d46b4-7b4d-453f-a06d-5d2092637c8b","keyword":"构造地球化学","originalKeyword":"构造地球化学"},{"id":"ee6028e8-5ceb-4284-9a19-0c36b7511af1","keyword":"多元统计分析","originalKeyword":"多元统计分析"},{"id":"99bc456f-c949-4921-8d8b-7ca4d12537e3","keyword":"夏甸—<span style=\"color:red\">姜</span>家窑测区","originalKeyword":"夏甸—姜家窑测区"},{"id":"35ec4729-d34c-4d49-bc6b-967a77e01731","keyword":"招平断裂带","originalKeyword":"招平断裂带"}],"language":"zh","publisherId":"huangj201505004","title":"招平断裂带夏甸—<span style=\"color:red\">姜</span>家窑段构造地球化学找矿预测","volume":"36","year":"2015"},{"abstractinfo":"采用压榨和熬煮两种方法从萝卜、香菜、大葱、柚子皮、<span style=\"color:red\">姜</span>中提取制剂,并采用电化学方法研究各种制剂对钢的腐蚀行为的影响,初步探讨制备方法对植物提取物缓蚀作用的影响规律.结果表明,各种制剂对钢在酸化盐溶液中的腐蚀均具有一定的缓蚀作用.制备方法对葱、<span style=\"color:red\">姜</span>制剂的缓蚀效果影响较大,葱压榨制剂的缓蚀效果明显高于熬煮制剂的缓蚀效果,而生姜熬煮制剂的缓蚀效果高于压榨制剂的.制备方法对制剂缓蚀效率的影响缘于制备方法对制剂成分的影响.","authors":[{"authorName":"赵卫民","id":"ebe3c495-9b20-4e2d-bf29-736be21d8793","originalAuthorName":"赵卫民"},{"authorName":"于道永","id":"6cbe8e90-e91c-435f-b10c-00b1d25649e9","originalAuthorName":"于道永"}],"doi":"","fpage":"110","id":"58246008-8af2-4008-934d-f6d45dbfd7e2","issue":"2","journal":{"abbrevTitle":"FSYFH","coverImgSrc":"journal/img/cover/FSYFH.jpg","id":"25","issnPpub":"1005-748X","publisherId":"FSYFH","title":"腐蚀与防护"},"keywords":[{"id":"e655c10f-5932-449e-9466-c385d5ce80ef","keyword":"金属腐蚀","originalKeyword":"金属腐蚀"},{"id":"bf3be800-53fd-4a0b-a962-5c94e26c7e99","keyword":"天然植物","originalKeyword":"天然植物"},{"id":"c42c5ebd-5240-4033-a7d8-d9fb07a5da08","keyword":"缓蚀剂","originalKeyword":"缓蚀剂"}],"language":"zh","publisherId":"fsyfh200902011","title":"制备方法对植物提取物缓蚀作用的影响","volume":"30","year":"2009"},{"abstractinfo":"建立了同时测定厚朴温中胶囊中山<span style=\"color:red\">姜</span>素、甘草酸、和厚朴酚、小豆蔻明、木香烃内酯、去氢木香内酯及厚朴酚含量的反相高效液相色谱法.固定相为Scienhome C18柱(250 mm×4.6 mm,5 μm),流动相为甲醇-乙腈-0.06%磷酸溶液(体积比为38:27:35),流速为1.0 mL/min,柱温为30℃,检测波长为235 nm.在上述条件下,山<span style=\"color:red\">姜</span>素、甘草酸、和厚朴酚、小豆蔻明、木香烃内酯、去氢木香内酯及厚朴酚的质量浓度分别在0.885～17.7,107～2 140,8.85～17.7,1.035～20.7,4.85～97,5.9～118和17.5～350 mg/L时与色谱峰面积之间的线性关系良好;回收率分别为96.9%～101.1%,96.0%～100.5%,100.396～100.8%,97.7%～101.4%,100.4%～102.3%,96.0%～102.3%和96.2%～100.6%.该方法简便、快速、准确.可用于厚朴温中胶囊的质量控制.","authors":[{"authorName":"丁晓菊","id":"65660375-6f64-480d-b181-e6b2bec6c0a1","originalAuthorName":"丁晓菊"},{"authorName":"赵云丽","id":"600b90d4-71fa-410f-8946-ea255f1d9fb5","originalAuthorName":"赵云丽"},{"authorName":"高晓霞","id":"e489ddd9-51ed-43f8-a443-47237c1783d0","originalAuthorName":"高晓霞"},{"authorName":"唐倩","id":"63d99122-43e4-4e08-ad86-47c1b82a4f89","originalAuthorName":"唐倩"},{"authorName":"李琳","id":"5aa44d3e-2535-4212-aef7-cd8cdc93c677","originalAuthorName":"李琳"},{"authorName":"于治国","id":"ef4ff73f-cc68-4e79-ad83-7f5279426432","originalAuthorName":"于治国"}],"doi":"10.3321/j.issn:1000-8713.2009.01.021","fpage":"107","id":"47ab76cb-955a-4af0-8d7d-115e99ec7bad","issue":"1","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"88b2ab6f-704a-4151-bc50-18f3454495a6","keyword":"高效液相色谱法","originalKeyword":"高效液相色谱法"},{"id":"3329ffde-5c5b-4330-8595-d25421851b9d","keyword":"有效成分","originalKeyword":"有效成分"},{"id":"adcfd855-e976-4daa-86a4-1e6da8e32e25","keyword":"厚朴温中胶囊","originalKeyword":"厚朴温中胶囊"}],"language":"zh","publisherId":"sp200901021","title":"高效液相色谱法同时测定厚朴温中胶囊中的7种有效成分","volume":"27","year":"2009"},{"abstractinfo":"为了解煤燃烧过程中温度对超细颗粒物生成的影响和吸附剂抑制超细颗粒物生成的有效性,本文进行了<span style=\"color:red\">小龙</span>潭褐煤的滴管炉燃烧试验.收集的超细颗粒物的尺寸分布已经在不同的操作参数下进行了测量.超细颗粒物主要通过汽化-成核-冷凝机理形成.因为小于100 nm的颗粒物没有得到充分的控制,一种加入蒸汽吸附剂的方法在煤燃烧系统中得到应用,事实证明这种方法可以有效地抑制超细颗粒物的生成.","authors":[{"authorName":"王春梅","id":"f8409f74-1739-4698-bfdc-bf4239a65625","originalAuthorName":"王春梅"},{"authorName":"张军营","id":"5602d2f0-9345-49fe-af90-a2cba36664eb","originalAuthorName":"张军营"},{"authorName":"周英彪","id":"5b6c7b75-33b7-4ff4-87d0-8a2467f140eb","originalAuthorName":"周英彪"},{"authorName":"郑楚光","id":"4ea0d168-9c94-451b-98eb-6f380f29c55a","originalAuthorName":"郑楚光"},{"authorName":"赵永椿","id":"6b458915-a460-452c-a027-58965dcb2403","originalAuthorName":"赵永椿"}],"doi":"","fpage":"1053","id":"25c2ebb5-151f-454a-9c39-021a7d095c76","issue":"6","journal":{"abbrevTitle":"GCRWLXB","coverImgSrc":"journal/img/cover/GCRWLXB.jpg","id":"32","issnPpub":"0253-231X","publisherId":"GCRWLXB","title":"工程热物理学报   "},"keywords":[{"id":"60033ea8-2ac8-4920-864d-9dead54e797d","keyword":"超细颗粒物","originalKeyword":"超细颗粒物"},{"id":"b10189cb-ce24-4e1c-ab17-8f1f8b7ec6a0","keyword":"温度","originalKeyword":"温度"},{"id":"6be01084-e54d-4d3b-80d0-01deae626ca9","keyword":"吸附剂","originalKeyword":"吸附剂"},{"id":"f5c8ed83-4712-48b7-b120-b283a6338e3d","keyword":"煤燃烧","originalKeyword":"煤燃烧"}],"language":"zh","publisherId":"gcrwlxb200406048","title":"煤燃烧超细颗粒物生成和控制的实验研究","volume":"25","year":"2004"},{"abstractinfo":"采用热力学平衡计算方法对<span style=\"color:red\">小龙</span>潭高钙飞灰在燃后区低温烟气下无机元素的迁移转化规律进行了研究.在常压下,常温～1000℃范围内,重点分析了烟气中CO2浓度和SO2对飞灰中无机元素迁移转化规律的影响.结果表明,在低温烟气区,Ca、Mg组分易发生碳酸化反应.CO2浓度会影响碳酸化反应的进行,而SO2的存在会极大地促进硫酸盐的生成,从而抑制碳酸化反应.","authors":[{"authorName":"伍夷飞","id":"f25b2ac9-fe19-4fe0-bd4c-60f1c0674180","originalAuthorName":"伍夷飞"},{"authorName":"赵永椿","id":"38302ee6-a3b0-4613-b1dc-04ec195dc715","originalAuthorName":"赵永椿"},{"authorName":"张军营","id":"ee53363b-3fe6-4380-a300-f1ab59f6cf6a","originalAuthorName":"张军营"},{"authorName":"郑楚光","id":"7f265bfa-fc73-48fe-8705-9ffe68982f45","originalAuthorName":"郑楚光"}],"doi":"","fpage":"455","id":"a09c9184-7761-4621-81c1-c3334095472a","issue":"2","journal":{"abbrevTitle":"GCRWLXB","coverImgSrc":"journal/img/cover/GCRWLXB.jpg","id":"32","issnPpub":"0253-231X","publisherId":"GCRWLXB","title":"工程热物理学报   "},"keywords":[{"id":"e308e1b3-3c6b-4a29-810f-ef8f12579fe1","keyword":"富氧燃烧","originalKeyword":"富氧燃烧"},{"id":"8fd8776e-57f9-4450-83d5-37539db0b155","keyword":"飞灰","originalKeyword":"飞灰"},{"id":"a8e4989a-eb9d-46aa-b7b5-bd3958ae19ce","keyword":"无机元素","originalKeyword":"无机元素"},{"id":"020ce866-50b1-4542-9868-4d98198f8810","keyword":"迁徙","originalKeyword":"迁徙"}],"language":"zh","publisherId":"gcrwlxb201502050","title":"富氧燃烧气氛下无机元素的迁移转化规律","volume":"36","year":"2015"},{"abstractinfo":"采用反相高效液相色谱法(RP-HPLC),以磺丁基醚-β-环糊精(SBE-β-CD)作为手性流动相添加剂,建立了二氢黄豆苷原(dihydrodaidzein)、雌马酚(equol)和山<span style=\"color:red\">姜</span>素(alpinetin)3种黄酮类化合物的手性拆分方法.考察了环糊精的种类和浓度、有机相的种类和比例、缓冲盐的种类和浓度以及pH对3种化合物手性拆分效果的影响.结果表明:采用Kromasil 100-5C18(250 mm×4.6 mm,5μm)色谱柱,流动相为乙腈-10 mmol/L SBE-β-CD水溶液(含20 mmol/L KH2PO4,pH值到4.0)(体积比为20:80)的条件下,二氢黄豆苷原、雌马酚和山<span style=\"color:red\">姜</span>素的对映体都达到了基线分离,分离度分别为1.8,1.9和1.4.该方法简便,分离效果好,对黄酮类化合物的拆分具有应用价值.","authors":[{"authorName":"孙亚男","id":"bc8be5be-8661-42e0-89e1-6d5346f45d9c","originalAuthorName":"孙亚男"},{"authorName":"李彤","id":"cf5f3b44-e76a-42bc-89f6-ed10eaf0f178","originalAuthorName":"李彤"},{"authorName":"马辰","id":"f245b23c-12a4-4d3f-8c2a-764472ba6d1f","originalAuthorName":"马辰"}],"doi":"10.3724/SP.J.1123.2012.12054","fpage":"447","id":"6b247c22-cf8b-4249-b6ec-0b8ac2d6f462","issue":"5","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"9064f001-01e7-4deb-9dfe-1df149777835","keyword":"手性分离","originalKeyword":"手性分离"},{"id":"5af15d60-aeff-4db9-9109-e5dcca339f7d","keyword":"反相高效液相色谱","originalKeyword":"反相高效液相色谱"},{"id":"ce51b549-cc03-46c9-b689-34147eae07cc","keyword":"磺丁基醚-β-环糊精","originalKeyword":"磺丁基醚-β-环糊精"},{"id":"2b51a8cc-2746-41f9-9c9c-9fdea5e4ed79","keyword":"黄酮类化合物对映体","originalKeyword":"黄酮类化合物对映体"}],"language":"zh","publisherId":"sp201305009","title":"高效液相色谱手性流动相添加剂法分离3种黄酮类化合物对映体","volume":"31","year":"2013"}],"totalpage":2,"totalrecord":20}