{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"采用N-(4-羧基苯基)马来酰亚胺为单体,四氢呋喃做溶剂,偶氮<span style=\"color:red\">二</span>异丁腈为引发剂,以RAFT试剂<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span><span style=\"color:red\">苯甲酸</span><span style=\"color:red\">苄</span><span style=\"color:red\">酯</span>为链转移剂,成功地进行了N-(4-羧基苯基)马来酰亚胺和苯乙烯的共聚合反应.结果表明,得到的聚合物数均分子量随单体转化率增加而呈线性增加,且聚合物的分子量分布小于1.5,<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span><span style=\"color:red\">苯甲酸</span><span style=\"color:red\">苄</span><span style=\"color:red\">酯</span>显示出对聚合反应的良好控制作用.通过不同反应温度的聚合反应动力学得到共聚合反应的表现活化能为1.39 kJ/mol.","authors":[{"authorName":"卢彦兵","id":"540a3714-0a27-4607-a56d-2b8abaf10ede","originalAuthorName":"卢彦兵"},{"authorName":"孙荣欣","id":"8183fa08-5426-4410-88f8-dad1eaedcf36","originalAuthorName":"孙荣欣"},{"authorName":"孙丽丽","id":"d0f2a909-01c5-495f-a933-b7a84e7cce34","originalAuthorName":"孙丽丽"},{"authorName":"夏新年","id":"32496ce7-2fff-4294-93a8-2ac91f78c577","originalAuthorName":"夏新年"},{"authorName":"徐伟箭","id":"bac5325e-7f97-4985-97c7-afe4973e2826","originalAuthorName":"徐伟箭"}],"doi":"","fpage":"39","id":"9654eafd-2587-4f76-a5ad-837d92b2914e","issue":"3","journal":{"abbrevTitle":"GFZCLKXYGC","coverImgSrc":"journal/img/cover/GFZCLKXYGC.jpg","id":"31","issnPpub":"1000-7555","publisherId":"GFZCLKXYGC","title":"高分子材料科学与工程"},"keywords":[{"id":"87b1f726-9af9-4b37-bcdd-027955b132f8","keyword":"N-(4-羧基苯基)马来酰亚胺","originalKeyword":"N-(4-羧基苯基)马来酰亚胺"},{"id":"ad97fc73-1f04-4cdb-aec5-a3042c4e71f9","keyword":"可控聚合","originalKeyword":"可控聚合"},{"id":"806bafbf-3a2e-4983-ae23-d97af384d008","keyword":"可逆加成断裂链转移聚合(RAFT)","originalKeyword":"可逆加成断裂链转移聚合(RAFT)"},{"id":"8447d1f3-537e-4243-bffb-134a70e88a69","keyword":"<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span><span style=\"color:red\">苯甲酸</span><span style=\"color:red\">苄</span><span style=\"color:red\">酯</span>","originalKeyword":"二硫代苯甲酸苄酯"}],"language":"zh","publisherId":"gfzclkxygc200903011","title":"基于RAFT过程的N-(4-羧基苯基)马来酰亚胺和苯乙烯可控自由基共聚合","volume":"25","year":"2009"},{"abstractinfo":"采用不同结构的可逆加成-断裂链转移聚合(RAFT)试剂,偶氮<span style=\"color:red\">二</span>异丁腈(AIBN)为引发剂,在乙烯基改性SiO2表面进行甲基丙烯酸甲<span style=\"color:red\">酯</span>接枝聚合.RAFT试剂的R基团和Z基团对接枝聚合的影响很大.R基团皆为苄基时,<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span>新戊酸<span style=\"color:red\">苄</span><span style=\"color:red\">酯</span>调控SiO2表面甲基丙烯酸甲<span style=\"color:red\">酯</span>的接枝聚合速率较高;R基团皆为1-苯基乙基时,苯基<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span>乙酸-1-苯乙<span style=\"color:red\">酯</span>调控SiO2表面甲基丙烯酸甲<span style=\"color:red\">酯</span>的接枝聚合速率较大.Z基团皆为苯基时,<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span><span style=\"color:red\">苯甲酸</span>叔丁<span style=\"color:red\">酯</span>调控SiO2表面甲基丙烯酸甲<span style=\"color:red\">酯</span>的接枝聚合速率较高.SiO2-PMMA接枝链末端<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span><span style=\"color:red\">酯</span>基团,可进一步RAFT接枝聚苯乙烯.相同聚合条件下,<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span><span style=\"color:red\">苯甲酸</span><span style=\"color:red\">苄</span><span style=\"color:red\">酯</span>调控SiO2-PMMA表面接枝聚苯乙烯的接枝率最高.","authors":[{"authorName":"李德玲","id":"24088679-6571-4a31-8b1d-e6a097cee670","originalAuthorName":"李德玲"},{"authorName":"王丽红","id":"73676008-a0e0-4a9e-995d-6cb67fb99b6b","originalAuthorName":"王丽红"},{"authorName":"马俊霄","id":"bb0410d0-6ca0-4257-89b4-d096feb28442","originalAuthorName":"马俊霄"}],"doi":"","fpage":"38","id":"c3bb67e5-e934-4e9f-98d3-9c4ca063b0af","issue":"8","journal":{"abbrevTitle":"GFZCLKXYGC","coverImgSrc":"journal/img/cover/GFZCLKXYGC.jpg","id":"31","issnPpub":"1000-7555","publisherId":"GFZCLKXYGC","title":"高分子材料科学与工程"},"keywords":[{"id":"41a035e0-db24-4fa4-8d9c-49b5b764a62c","keyword":"可逆加成-断裂链转移聚合","originalKeyword":"可逆加成-断裂链转移聚合"},{"id":"65f88376-82e9-4bf4-8c71-462f01e1529f","keyword":"表面接枝","originalKeyword":"表面接枝"},{"id":"c1c98088-887e-42c7-959f-4653e5bf941a","keyword":"甲基丙烯酸甲<span style=\"color:red\">酯</span>","originalKeyword":"甲基丙烯酸甲酯"},{"id":"6ec6016c-3def-4b57-b097-31c6b5ff1e32","keyword":"<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span><span style=\"color:red\">酯</span>","originalKeyword":"二硫代酯"}],"language":"zh","publisherId":"gfzclkxygc201308010","title":"<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span><span style=\"color:red\">酯</span>对SiO2表面甲基丙烯酸甲<span style=\"color:red\">酯</span>可逆加成-断裂链转移聚合的影响","volume":"29","year":"2013"},{"abstractinfo":"合成了直链淀粉-三(3,5-<span style=\"color:red\">二</span>甲基苯基氨基<span style=\"color:red\">甲酸酯</span>)手性固定相.用该固定相对6种单<span style=\"color:red\">硫</span><span style=\"color:red\">代</span>甘油醚和4 种双<span style=\"color:red\">硫</span><span style=\"color:red\">代</span>甘油醚进行了手性拆分.单<span style=\"color:red\">硫</span><span style=\"color:red\">代</span>甘油醚对映异构体得到了较好的分离, 而双<span style=\"color:red\">硫</span><span style=\"color:red\">代</span>甘油醚完全不能拆分.提出了样品与固定相的作用模式.","authors":[{"authorName":"于兆文","id":"bb596b37-3a75-4517-a48e-c4f7b0f31ffe","originalAuthorName":"于兆文"},{"authorName":"刘霞","id":"d6866a96-9b11-4d7d-8dbd-d1dde7be9ae4","originalAuthorName":"刘霞"},{"authorName":"蒋生祥","id":"82ca506e-1d5f-481b-8097-1afc80b2a460","originalAuthorName":"蒋生祥"},{"authorName":"陈立仁","id":"53f3d204-c15c-4944-bc5b-cef8fc6575f6","originalAuthorName":"陈立仁"}],"doi":"10.3321/j.issn:1000-8713.2000.01.011","fpage":"39","id":"6400b1a0-8d67-4b85-bbc6-255070be8482","issue":"1","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"2659cc22-c033-4161-9060-3bf441492573","keyword":"高效液相色谱法","originalKeyword":"高效液相色谱法"},{"id":"cb3664bf-fa01-45cf-a1fd-c81712900fa8","keyword":"手性固定相","originalKeyword":"手性固定相"},{"id":"bf2451ea-6b49-4bb4-8849-74e37de9a025","keyword":"对映体分离","originalKeyword":"对映体分离"}],"language":"zh","publisherId":"sp200001011","title":"单<span style=\"color:red\">硫</span><span style=\"color:red\">代</span>和双<span style=\"color:red\">硫</span><span style=\"color:red\">代</span>甘油醚在直链淀粉-三(3,5-<span style=\"color:red\">二</span>甲基苯基氨基<span style=\"color:red\">甲酸酯</span>)固定相上的手性拆分","volume":"18","year":"2000"},{"abstractinfo":"采用两步法,首次以<span style=\"color:red\">硫</span><span style=\"color:red\">代</span><span style=\"color:red\">苯甲酸</span>合成的Cd(SCOC6H5)2在十六胺(HAD)介质中于120℃热解合成了CdS纳米晶,并采用透射电子显微镜(TEM)、X射线衍射(xRD)、荧光分光光度计(PL)对其进行了表征.结果表明,纳米晶为晶形完美的六方状颗粒,并夹杂有小短棒,六方状颗粒边长约为5nm,小棒的长度为10～25nm.通过X射线衍射(XRD)进一步分析得知,其成分为CdS.选区电子衍射环为多晶环,荧光峰证明出现了蓝移现象,并解释了原因,探讨了形成机理.","authors":[{"authorName":"吕朝霞","id":"6c19ce10-af68-41e4-a920-e81ae6d9d021","originalAuthorName":"吕朝霞"},{"authorName":"刘淑萍","id":"6bd4e223-438a-48e3-b475-206dd9423c0b","originalAuthorName":"刘淑萍"},{"authorName":"刘胜昌","id":"67aef655-9d0b-4a23-b7f8-29dadcf70e7e","originalAuthorName":"刘胜昌"}],"doi":"","fpage":"33","id":"5946bb61-4cb9-4328-9c2b-22e26387480e","issue":"z2","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"8e77f57d-6e7e-48ac-a661-1015ac401094","keyword":"<span style=\"color:red\">硫</span><span style=\"color:red\">代</span><span style=\"color:red\">苯甲酸</span>","originalKeyword":"硫代苯甲酸"},{"id":"e9b77b40-9539-400e-9ccc-9d233e009370","keyword":"<span style=\"color:red\">硫</span><span style=\"color:red\">代</span><span style=\"color:red\">苯甲酸</span>镉","originalKeyword":"硫代苯甲酸镉"},{"id":"d278de01-dd40-4563-91cc-4cba85adf4e4","keyword":"两步法","originalKeyword":"两步法"},{"id":"bfeb96f3-6eed-4c8e-999b-6fd6df459a14","keyword":"CdS纳米晶","originalKeyword":"CdS纳米晶"},{"id":"906a5851-16da-493c-803f-9e3aecc3f4d8","keyword":"形成机理","originalKeyword":"形成机理"}],"language":"zh","publisherId":"cldb2009z2011","title":"<span style=\"color:red\">硫</span><span style=\"color:red\">代</span><span style=\"color:red\">苯甲酸</span>两步合成CdS纳米晶及表征","volume":"23","year":"2009"},{"abstractinfo":"利用三(o-溴苄基)溴化锡与吡咯烷基<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span><span style=\"color:red\">甲酸</span>钠反应,合成了三(o-溴苄基)锡吡咯烷基<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span><span style=\"color:red\">甲酸</span><span style=\"color:red\">酯</span>.用X射线单晶衍射测定了其晶体结构,化合物为三斜晶系,空间群P1,晶体学参数a=0.91354(11) nm,b=1.07313(13) nm,c=1.52677(18) nm,α =75.440(6)°,β=89.499(6)°,γ=72.515(7)°,V=1.3781(3) nm3,Z=2,Dc=1.868 g/cm3,μ(MoKα) =54.43 cm-1,F(000) =752,R1=0.0320,wR2=0.0765.化合物中的锡原子为四配位畸变四面体构型.对其结构进行量子化学从头计算,探讨了配合物的稳定性、分子轨道能量以及部分前沿分子轨道的组成特征.测定了配合物体外抗癌活性.","authors":[{"authorName":"张复兴","id":"c7f8c1bf-28d1-42c1-8685-946b7ea7c651","originalAuthorName":"张复兴"},{"authorName":"邝<span style=\"color:red\">代</span>治","id":"21741540-47eb-4220-aa7b-494bbed9a919","originalAuthorName":"邝代治"},{"authorName":"冯泳兰","id":"ccc21032-ac7e-48c2-96ba-ac599d93aeff","originalAuthorName":"冯泳兰"},{"authorName":"王剑秋","id":"80672625-d4a3-432f-8a11-fa973f02565b","originalAuthorName":"王剑秋"},{"authorName":"庾江喜","id":"64f956d8-d2e4-4414-b3c9-35480887f3de","originalAuthorName":"庾江喜"},{"authorName":"蒋伍玖","id":"2921ace5-dbc8-412f-98bb-a3f74e6a760f","originalAuthorName":"蒋伍玖"},{"authorName":"朱小明","id":"dd9e8c72-f6a6-4d87-b683-c1811f331795","originalAuthorName":"朱小明"}],"doi":"10.3724/SP.J.1095.2014.30212","fpage":"285","id":"d96cf96c-d55d-47d2-aa84-c65d94e12b7e","issue":"3","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"6ae74c18-396a-4046-b47a-d8d13e747640","keyword":"三(o-溴苄基)锡吡咯烷基<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span><span style=\"color:red\">甲酸</span><span style=\"color:red\">酯</span>","originalKeyword":"三(o-溴苄基)锡吡咯烷基二硫代甲酸酯"},{"id":"02dccdb6-c5c1-4308-a1d7-a5a3ce403f03","keyword":"合成","originalKeyword":"合成"},{"id":"92e267b0-ba44-453f-8ed6-fc39bf301f9e","keyword":"结构","originalKeyword":"结构"},{"id":"9ee97285-09fb-4816-b19e-1c0c9ee17b01","keyword":"抗肿瘤活性","originalKeyword":"抗肿瘤活性"}],"language":"zh","publisherId":"yyhx201403007","title":"三(o-溴苄基)锡吡咯烷基<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span><span style=\"color:red\">甲酸</span><span style=\"color:red\">酯</span>的合成、结构及体外抗癌活性","volume":"31","year":"2014"},{"abstractinfo":"以固载杂多酸盐TiSiW12O40/TiO2为多相催化剂,对以乙醇、丙醇、丁醇和对羟基<span style=\"color:red\">苯甲酸</span>为原料合成对羟基<span style=\"color:red\">苯甲酸</span><span style=\"color:red\">酯</span>的反应条件进行了研究.实验表明:TiSiW12O40/TiO2是合成对羟基<span style=\"color:red\">苯甲酸</span><span style=\"color:red\">酯</span>的良好催化剂,最佳反应条件为:醇酸摩尔比为4:1,催化剂用量为反应物料总量的2%,反应时间为2 h.上述条件下,对羟基<span style=\"color:red\">苯甲酸</span>乙<span style=\"color:red\">酯</span>的产率为87.5%,对羟基<span style=\"color:red\">苯甲酸</span>丙<span style=\"color:red\">酯</span>的产率为89.2%,对羟基<span style=\"color:red\">苯甲酸</span>丁<span style=\"color:red\">酯</span>的产率为91.1%.","authors":[{"authorName":"杨水金","id":"1069a798-ce37-4386-a45e-341325187e7e","originalAuthorName":"杨水金"},{"authorName":"梁永光","id":"eb71bd2a-f6b3-4db4-b131-d42fbfb2f2c9","originalAuthorName":"梁永光"},{"authorName":"孙聚堂","id":"877f155d-a804-4876-828d-3c5995f791df","originalAuthorName":"孙聚堂"}],"doi":"","fpage":"1033","id":"20f606d9-5f53-474c-8626-1b1beb9818ea","issue":"12","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"97f22b1d-7b4c-4e52-8387-597f4fc8e5b1","keyword":"对羟基<span style=\"color:red\">苯甲酸</span><span style=\"color:red\">酯</span>","originalKeyword":"对羟基苯甲酸酯"},{"id":"dc1b0e68-f586-4a29-a36a-f568f0573f58","keyword":"催化剂","originalKeyword":"催化剂"},{"id":"881142db-5d79-440b-9da7-59bd9e5d1621","keyword":"TiSiW12O40/TiO2","originalKeyword":"TiSiW12O40/TiO2"}],"language":"zh","publisherId":"xyjsclygc200312016","title":"对羟基<span style=\"color:red\">苯甲酸</span><span style=\"color:red\">酯</span>的合成","volume":"32","year":"2003"},{"abstractinfo":"以<span style=\"color:red\">二</span>苄基胺、NaOH 和 CS2为原料，四氢呋喃作溶剂合成<span style=\"color:red\">二</span>苄基<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span>氨基<span style=\"color:red\">甲酸</span>钠，再与四甲基氯化铵反应，合成了新型的离子盐促进剂———<span style=\"color:red\">二</span>苄基<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span>氨基<span style=\"color:red\">甲酸</span>四甲基铵。通过红外(FT-IR)、核磁(1 H NMR)、质谱(MS)及元素分析等分析方法确定了产物的结构。为了研究新型促进剂的性能，实验将合成的<span style=\"color:red\">二</span>苄基<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span>氨基酸四甲基铵、<span style=\"color:red\">二</span>硫化四甲基秋兰姆(TMTD)分别添加到天然橡胶中制成胶片，对其进行溶胀指数(SI )和力学性能测试，结果表明合成的<span style=\"color:red\">二</span>苄基<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span>氨基酸四甲基铵具有优异的促进性能，是一种性能优异绿色环保的天然橡胶促进剂。","authors":[{"authorName":"曾燕飞","id":"f434f13b-0182-4b2a-bfb8-9ed0837f39c3","originalAuthorName":"曾燕飞"},{"authorName":"周元林","id":"7bb12aa7-f791-4848-8fd0-0938f02571ce","originalAuthorName":"周元林"},{"authorName":"游兴均","id":"49cb4ffb-d377-466e-8a86-1d28649bac69","originalAuthorName":"游兴均"}],"doi":"10.3969/j.issn.1001-9731.2014.22.011","fpage":"22051","id":"ced4d97b-7670-4a99-a383-e77f67288642","issue":"22","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"9e3e98ef-8731-4684-aa77-8a099b5617ae","keyword":"<span style=\"color:red\">二</span>苄基<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span>氨基<span style=\"color:red\">甲酸</span>钠","originalKeyword":"二苄基二硫代氨基甲酸钠"},{"id":"a82308f0-6db1-4993-97f1-c4850497c5f4","keyword":"离子盐","originalKeyword":"离子盐"},{"id":"f4fe1b7f-77ed-4b67-af93-79fc6fc18ff5","keyword":"<span style=\"color:red\">二</span>苄基<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span>氨基<span style=\"color:red\">甲酸</span>四甲基铵","originalKeyword":"二苄基二硫代氨基甲酸四甲基铵"},{"id":"7f74497b-6d65-4576-8739-c7c631c4dc6c","keyword":"促进剂","originalKeyword":"促进剂"},{"id":"d964b8be-3bc3-46d2-8b98-8eca35d579ec","keyword":"天然橡胶","originalKeyword":"天然橡胶"}],"language":"zh","publisherId":"gncl201422011","title":"<span style=\"color:red\">二</span>苄基<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span>氨基<span style=\"color:red\">甲酸</span>四甲基铵的合成、表征及性能研究?","volume":"","year":"2014"},{"abstractinfo":"氨基<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span><span style=\"color:red\">甲酸</span>酯类化合物由于其独特的分子结构,使其具有明显的抗肿瘤、抗菌、抗氧化以及杀虫等多种生物活性,已经成为近年来药物化学领域研究的重点.本文评述了近年来文献报道的氨基<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span><span style=\"color:red\">甲酸</span>酯类化合物以及它们的主要生物活性,并对其今后的发展方向、应用前景做出展望.","authors":[{"authorName":"王晓娟","id":"adb737f0-50a6-430e-a723-3b5ac2d85452","originalAuthorName":"王晓娟"},{"authorName":"李高伟","id":"c6c20b9a-1eb2-4e8e-9e57-43a434e2a5c4","originalAuthorName":"李高伟"},{"authorName":"孟团结","id":"955c5a62-8340-4c39-9ba3-d0b957544331","originalAuthorName":"孟团结"},{"authorName":"刘澜涛","id":"7e22020f-7416-451e-a399-414c9c7003c8","originalAuthorName":"刘澜涛"},{"authorName":"赵文献","id":"245c135f-7463-40db-a08f-a456a15b5ad4","originalAuthorName":"赵文献"}],"doi":"10.11944/j.issn.1000-0518.2015.02.140187","fpage":"123","id":"0463f8f8-2240-4a50-90a3-ca9c0e82751c","issue":"2","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"eb08f2c2-67d1-4b5a-a0b3-5b12f16ac7dc","keyword":"氨基<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span><span style=\"color:red\">甲酸</span><span style=\"color:red\">酯</span>","originalKeyword":"氨基二硫代甲酸酯"},{"id":"cb44646b-84ff-4b29-8f93-a993325ab1cd","keyword":"生物活性","originalKeyword":"生物活性"}],"language":"zh","publisherId":"yyhx201502001","title":"氨基<span style=\"color:red\">二</span><span style=\"color:red\">硫</span><span style=\"color:red\">代</span><span style=\"color:red\">甲酸</span>酯类化合物生物活性研究进展","volume":"32","year":"2015"},{"abstractinfo":"采用超声协助甲醇提取、固相萃取净化、气相色谱/选择离子质谱联用法,同时测定化妆品中8种邻苯<span style=\"color:red\">二甲酸</span><span style=\"color:red\">酯</span>和4种对羟基<span style=\"color:red\">苯甲酸</span><span style=\"color:red\">酯</span>.该方法线性范围广、重现性好、快速简便、干扰小.样品的加标回收率为80%～160%;含量检测的相对标准偏差小于10%;方法的检出限为0.1～5.0 μg/kg.用该方法对15种实际样品中的12种残留物进行定量检测,结果表明除了一种样品中不含待测物外,其余样品均检测到3～7种待测物.其中以对羟基<span style=\"color:red\">苯甲酸</span>甲<span style=\"color:red\">酯</span>、对羟基<span style=\"color:red\">苯甲酸</span>丙<span style=\"color:red\">酯</span>、邻苯<span style=\"color:red\">二甲酸</span>丙<span style=\"color:red\">酯</span>、邻苯<span style=\"color:red\">二甲酸</span>环己<span style=\"color:red\">酯</span>和邻苯<span style=\"color:red\">二甲酸</span>乙基庚基<span style=\"color:red\">酯</span>为主.","authors":[{"authorName":"沈昊宇","id":"c426d70a-92fb-4d84-af1a-04841ca7d388","originalAuthorName":"沈昊宇"},{"authorName":"应丽艳","id":"b794d6e0-a7b7-4841-893d-cdc94591fae3","originalAuthorName":"应丽艳"},{"authorName":"曹云峰","id":"b67d38af-f534-4b47-97f3-db21c1a8a6c0","originalAuthorName":"曹云峰"},{"authorName":"潘刚","id":"37ce31da-5590-461c-b99b-0978e3deb2a6","originalAuthorName":"潘刚"},{"authorName":"周鹿","id":"e55f370a-2d97-4efa-8571-8d5f9cb7a6ea","originalAuthorName":"周鹿"}],"doi":"10.3321/j.issn:1000-8713.2007.02.032","fpage":"272","id":"87a2968c-9342-491f-a104-6cfe8e34c01b","issue":"2","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"ce747f0b-3b3f-427b-b3a3-bc76ca5a6460","keyword":"气相色谱/质谱法","originalKeyword":"气相色谱/质谱法"},{"id":"2958a551-b2a9-4b8f-bfdf-0ffa6f715d1e","keyword":"固相萃取","originalKeyword":"固相萃取"},{"id":"e1db940c-6bd0-4fd4-b807-8996c4c890e0","keyword":"邻苯<span style=\"color:red\">二甲酸</span><span style=\"color:red\">酯</span>","originalKeyword":"邻苯二甲酸酯"},{"id":"918b819c-fa5a-4172-a50e-423afa876f58","keyword":"对羟基<span style=\"color:red\">苯甲酸</span><span style=\"color:red\">酯</span>","originalKeyword":"对羟基苯甲酸酯"},{"id":"1abb9b20-0411-4440-858d-622f5f6580b8","keyword":"化妆品","originalKeyword":"化妆品"}],"language":"zh","publisherId":"sp200702032","title":"固相萃取-气相色谱/质谱法同时测定化妆品中的邻苯<span style=\"color:red\">二甲酸</span><span style=\"color:red\">酯</span>和对羟基<span style=\"color:red\">苯甲酸</span><span style=\"color:red\">酯</span>","volume":"25","year":"2007"},{"abstractinfo":"以淀粉和3,5-<span style=\"color:red\">二</span>硝基苯甲酰氯为原料合成了一种淀粉衍生物--3,5-<span style=\"color:red\">二硝基苯甲酸</span>淀粉<span style=\"color:red\">酯</span>(DNBZ-ST),采用红外光谱、元素分析、核磁、热重等手段对产物结构进行了表征,确定了合成DNBZ-ST的最佳条件. DNBZ-ST对肌酐有较好的吸附性能,在肌酐溶液浓度为100 mg/L、吸附温度为37 ℃、介质pH=7的条件下,DNBZ-ST(取代度DS=2.09)对肌酐的最大吸附量达25 mg/g.","authors":[{"authorName":"于九皋","id":"0266759c-b95f-4c04-af3b-c94a1458b415","originalAuthorName":"于九皋"},{"authorName":"杨冬芝","id":"8f5eff15-6a77-4bf7-8358-cf21d1ecc93f","originalAuthorName":"杨冬芝"}],"doi":"10.3969/j.issn.1000-0518.2002.09.009","fpage":"858","id":"a3a6feb3-b532-4e30-9025-a642345c30b0","issue":"9","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"074ca076-8bad-4380-9e71-38edae474144","keyword":"淀粉","originalKeyword":"淀粉"},{"id":"b416cf68-3905-4f3d-ac06-aac5b1340808","keyword":"<span style=\"color:red\">二硝基苯甲酸</span>淀粉<span style=\"color:red\">酯</span>","originalKeyword":"二硝基苯甲酸淀粉酯"},{"id":"ddd212af-99fb-44f0-8967-6ddde8a0c6e3","keyword":"合成","originalKeyword":"合成"},{"id":"e59979f2-8506-43ef-98a8-00662691f71f","keyword":"高分子吸附剂","originalKeyword":"高分子吸附剂"}],"language":"zh","publisherId":"yyhx200209009","title":"3,5-<span style=\"color:red\">二硝基苯甲酸</span>淀粉<span style=\"color:red\">酯</span>的合成及应用","volume":"19","year":"2002"}],"totalpage":3831,"totalrecord":38304}