{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"采用水热辅助表面接枝印迹技术,以Cd（Ⅱ）离子作为模板,巯基丙基三甲氧基硅烷为功能分子,环氧氯丙烷为交联剂,在硅胶表面制备出高容量的Cd（Ⅱ）离子印迹硅胶材料,利用红外光谱仪、扫描电镜、热重分析仪等进行了表征,采用平衡吸附法研究了印迹硅胶材料的吸附性能和选择识别能力。结果表明,印迹硅胶材料和非印迹硅胶材料的最大吸附量分别为42.5和22.1mg/g;印迹硅胶材料对Cd（Ⅱ）离子具有较强的选择识别能力,对Cd（Ⅱ）离子的吸附行为更符合Langmuir模型,20min即可达到吸附平衡,符合准二级动力学方程,pH值在4～8范围内,保持了较好的吸附容量;重复使用时性能较好。","authors":[{"authorName":"<span style=\"color:red\">范</span><span style=\"color:red\">洪涛</span>","id":"320d98ef-291f-4a61-8d8a-970d0dc17b7f","originalAuthorName":"范洪涛"},{"authorName":"李晶","id":"a8895198-f11c-46bc-9401-d15a55ced326","originalAuthorName":"李晶"},{"authorName":"李展超","id":"8fa1dac7-d468-4eb4-b670-77e8cc7819f8","originalAuthorName":"李展超"},{"authorName":"阎峰","id":"0b995d01-11c1-4af1-8b30-4d32555093f6","originalAuthorName":"阎峰"},{"authorName":"孙挺","id":"0ab03c82-87ff-4aa5-b192-e5e605330b49","originalAuthorName":"孙挺"}],"doi":"","fpage":"2060","id":"0509c419-f06a-4c14-9e47-7c87fcfdea93","issue":"15","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"70e42a58-aba1-4778-984b-1ff1cb4e1f57","keyword":"水热辅助","originalKeyword":"水热辅助"},{"id":"8a67a803-17f7-43cf-83cb-fc661621bd72","keyword":"离子印迹","originalKeyword":"离子印迹"},{"id":"c341bd22-baee-4c16-afcd-e0909926f6ea","keyword":"Cd","originalKeyword":"Cd"},{"id":"36c51c5a-5ee0-4398-8973-bfda8957383e","keyword":"巯基丙基三甲氧基硅烷","originalKeyword":"巯基丙基三甲氧基硅烷"},{"id":"223a9199-4014-40a5-a81f-06190f50da00","keyword":"吸附","originalKeyword":"吸附"}],"language":"zh","publisherId":"gncl201215022","title":"水热辅助表面接枝印迹法制备Cd（Ⅱ）离子印迹硅胶及其性能研究","volume":"43","year":"2012"},{"abstractinfo":"采用表面印迹技术和溶胶-凝胶法,以Cd（Ⅱ）离子作为印迹离子,硫氰基丙基三甲氧基硅烷为功能分子,环氧氯丙烷为交联剂,在硅胶表面制备Cd（Ⅱ）离子印迹聚合物（IIP-TCPTS/SiO2）,并利用平衡吸附法研究了聚合物吸附性能和选择识别能力。结果表明,最大吸附量为16.7 mg/g;20 min即可达到吸附平衡;当pH值在5.4-7.8范围内,印迹聚合物保持了较好的吸附容量;印迹聚合物对Cd（Ⅱ）离子具有较强的选择性识别能力;重复使用时性能稳定。","authors":[{"authorName":"陈美希","id":"9e15a962-3c01-43cd-a848-32acc6fc9e9b","originalAuthorName":"陈美希"},{"authorName":"曹晓晴","id":"dde757f9-8f88-40b0-879b-b867c79401a0","originalAuthorName":"曹晓晴"},{"authorName":"余自友","id":"92a2a43e-ef7b-45a4-9f6d-dc8ecae8635b","originalAuthorName":"余自友"},{"authorName":"张岗","id":"1199657a-05bc-49c4-8792-49c87199b1b4","originalAuthorName":"张岗"},{"authorName":"<span style=\"color:red\">范</span><span style=\"color:red\">洪涛</span>","id":"f8990655-0e3d-479d-b856-59c61a5b6954","originalAuthorName":"范洪涛"},{"authorName":"孙挺","id":"24691ae4-1343-4036-9247-1ffa167169ea","originalAuthorName":"孙挺"}],"doi":"","fpage":"163","id":"57b091c3-0950-4a3b-a7d0-120fcf036d6b","issue":"8","journal":{"abbrevTitle":"GFZCLKXYGC","coverImgSrc":"journal/img/cover/GFZCLKXYGC.jpg","id":"31","issnPpub":"1000-7555","publisherId":"GFZCLKXYGC","title":"高分子材料科学与工程"},"keywords":[{"id":"a7ea677c-b85d-4334-bad3-c9f99809dadf","keyword":"镉","originalKeyword":"镉"},{"id":"0264b3cb-f9f4-4f62-bd63-52b2c7f17e98","keyword":"溶胶-凝胶","originalKeyword":"溶胶-凝胶"},{"id":"32015089-6900-48bb-a632-23d726772d2f","keyword":"硫氰基丙基三甲氧基硅烷","originalKeyword":"硫氰基丙基三甲氧基硅烷"},{"id":"3c93d433-ac11-4876-b925-9f2dc287dc3c","keyword":"离子印迹","originalKeyword":"离子印迹"}],"language":"zh","publisherId":"gfzclkxygc201208041","title":"镉离子印迹硅胶的制备与吸附性能","volume":"28","year":"2012"},{"abstractinfo":"以氨基酸为原料采用一步法合成了3种氨基酸离子液体,将其代替浓H2SO4用于催化乙酸酐和水杨酸的乙酰化反应,清洁合成阿司匹林.考察了离子液体种类及用量、原料配比、反应温度、时间等因素对合成阿司匹林的影响.结果表明,该离子液体对于合成阿司匹林具有良好的催化效果,在水杨酸20mmol、乙酸酐40mmol、谷氨酸硫酸盐离子液体([Glu] HSO4) 2mmol、反应温度70℃、反应时间30min的条件下,阿司匹林分离产率可达84.8％.增大投料量,产率还会进一步升高,并且离子液体可重复使用.","authors":[{"authorName":"王晓丹","id":"a87ba759-80ef-42db-b7fa-a2e3f33b1006","originalAuthorName":"王晓丹"},{"authorName":"<span style=\"color:red\">范</span><span style=\"color:red\">洪涛</span>","id":"c4daa499-bc04-41a3-8bba-ba737943ad88","originalAuthorName":"范洪涛"},{"authorName":"崔天放","id":"2e596300-5b09-48fb-aa5a-b1cf7100bf72","originalAuthorName":"崔天放"},{"authorName":"邓伟荣","id":"1c64d10d-9fa6-4fa1-b249-d4fa3aad59f5","originalAuthorName":"邓伟荣"}],"doi":"","fpage":"81","id":"f1d7e292-b4e0-4f8b-8e74-382670c64ac9","issue":"18","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"a4f32f61-da5b-49fd-8925-c990eecbf5b1","keyword":"离子液体","originalKeyword":"离子液体"},{"id":"c990f73b-d783-40e7-a79f-8456a0dc9765","keyword":"氨基酸","originalKeyword":"氨基酸"},{"id":"72224813-3ecb-43be-9be7-1438d9f00cef","keyword":"催化","originalKeyword":"催化"},{"id":"5d10ddd1-073c-4ace-b994-114b32f685da","keyword":"合成","originalKeyword":"合成"},{"id":"3376a13b-7fc5-489c-9f6e-f28cf4229347","keyword":"阿司匹林","originalKeyword":"阿司匹林"}],"language":"zh","publisherId":"cldb201218022","title":"氨基酸离子液体清洁催化合成阿司匹林","volume":"26","year":"2012"},{"abstractinfo":"利用原位测试系统得到细编穿剌C/C复合材料纤维/基体及纤维束/基体两种不同层次界面的顶出实验数据,然后利用界面弹簧模型对纤维及纤维束的顶出实验过程进行有限元法计算机模拟,编制了分析程序,得到了不同层次界面的剪切强度值.","authors":[{"authorName":"孔宪仁","id":"0ceba95e-1a7b-4efc-b259-c29ea4812365","originalAuthorName":"孔宪仁"},{"authorName":"黄玉东","id":"63f71e38-5a28-4f37-a7be-e25df0548924","originalAuthorName":"黄玉东"},{"authorName":"<span style=\"color:red\">范</span><span style=\"color:red\">洪涛</span>","id":"4849efc2-2339-4fee-8f23-b6d17a8db30e","originalAuthorName":"范洪涛"},{"authorName":"孙文训","id":"d5985a08-189d-4887-abfb-e1e34f96198a","originalAuthorName":"孙文训"}],"doi":"10.3321/j.issn:1000-3851.2001.02.014","fpage":"57","id":"633c9faf-3243-4ade-8f26-214678b70619","issue":"2","journal":{"abbrevTitle":"FHCLXB","coverImgSrc":"journal/img/cover/FHCLXB.jpg","id":"26","issnPpub":"1000-3851","publisherId":"FHCLXB","title":"复合材料学报"},"keywords":[{"id":"9c916962-f915-4c94-9688-9f82a47922f5","keyword":"C/C复合材料","originalKeyword":"C/C复合材料"},{"id":"694c44a3-9e6d-4f65-89d2-956338e1c626","keyword":"纤维/基体界面","originalKeyword":"纤维/基体界面"},{"id":"20243839-adf5-448c-8b0e-7e29eb2cbd46","keyword":"纤维束/基体界面","originalKeyword":"纤维束/基体界面"},{"id":"8bf5dc1d-84e8-48ee-81ee-e938f64abeb2","keyword":"有限元法","originalKeyword":"有限元法"},{"id":"62e4225d-b8e1-4b73-8e82-29d8b57a78be","keyword":"界面剪切强度","originalKeyword":"界面剪切强度"}],"language":"zh","publisherId":"fhclxb200102014","title":"细编穿刺C/C复合材料不同层次界面剪切强度的测试分析","volume":"18","year":"2001"},{"abstractinfo":"以Cr5支承辊用钢为研究材料,采用热模拟实验对单轴应力作用下马氏体相变的相变塑性进行了研究.介绍了从径向膨胀曲线分离出相变塑性应变的数据处理方法,并讨论了该方法带来的误差,分析了马氏体相变动力学对实验结果的影响.实验结果表明,在Cr5支承辊用钢马氏体相变结束时,相变塑性应变与应力成线性关系,Greenwood-Johnson模型中的相变塑性参数是与应力无关的常数.","authors":[{"authorName":"石伟","id":"3c23d496-2409-4316-9d18-97e5f1d8d699","originalAuthorName":"石伟"},{"authorName":"<span style=\"color:red\">范</span><span style=\"color:red\">洪涛</span>","id":"9f56d274-febf-49e4-b17b-1430dd73df5b","originalAuthorName":"范洪涛"},{"authorName":"刘庄","id":"5c44b2bb-f412-4fb9-a18e-30b5eadfe3b8","originalAuthorName":"刘庄"}],"doi":"10.3969/j.issn.1009-6264.2006.05.029","fpage":"122","id":"35e68b9e-83e4-4a8f-baaf-db1de3de09c6","issue":"5","journal":{"abbrevTitle":"CLRCLXB","coverImgSrc":"journal/img/cover/CLRCLXB.jpg","id":"15","issnPpub":"1009-6264","publisherId":"CLRCLXB","title":"材料热处理学报"},"keywords":[{"id":"3462b9e7-af9a-44fb-8964-e68bdc690bc4","keyword":"相变塑性","originalKeyword":"相变塑性"},{"id":"dbb938db-38d7-441b-a406-d7e9d5426656","keyword":"马氏体相变","originalKeyword":"马氏体相变"},{"id":"8a401f35-5f53-4884-a6f6-55cf6a504a24","keyword":"应力影响相变","originalKeyword":"应力影响相变"},{"id":"4e7dbe40-04e2-4c59-991a-1e4f54f65e16","keyword":"支承辊","originalKeyword":"支承辊"}],"language":"zh","publisherId":"jsrclxb200605029","title":"Cr5支承辊用钢马氏体相变的相变塑性研究","volume":"27","year":"2006"},{"abstractinfo":"以N-甲基咪唑为原料合成了室温离子液体1-丁基-3-甲基咪唑氯酸盐（[BMIM]ClO3）,用IR、NMR、DSC-TGA等手段对产物进行了表征,测定了相关物化性能,如密度、表面张力、黏度、电导率和电化学窗口等,并考察了该离子液体的溶剂性能。结果表明,该离子液体作为新型的电解质材料,具有低黏度、高电导率,密度、表面张力、黏度均随温度升高而减小,电导率随温度升高而增大,与温度符合Arrhenius方程。该离子液体与多数常规溶剂互溶,并对某些金属氧化物具有较高的溶解度,为离子液体在选矿、电解金属氧化物等方面的应用奠定了基础。","authors":[{"authorName":"王晓丹","id":"735fb90e-d1a8-4cf1-83da-307183581784","originalAuthorName":"王晓丹"},{"authorName":"<span style=\"color:red\">范</span><span style=\"color:red\">洪涛</span>","id":"8337e387-797b-4403-a21c-d38e42fc3674","originalAuthorName":"范洪涛"},{"authorName":"于秀兰","id":"f9a67943-5e74-41dc-bf80-0037be1afa0f","originalAuthorName":"于秀兰"}],"doi":"","fpage":"2131","id":"59efd65e-905e-4455-923b-94eeaf76bc9d","issue":"16","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"15ec1e2d-c983-4664-bf1e-0ad7d4b6f20c","keyword":"室温离子液体","originalKeyword":"室温离子液体"},{"id":"93c77fb1-4f9e-4637-8c95-20033ff8ebc1","keyword":"[BMIM]ClO3","originalKeyword":"[BMIM]ClO3"},{"id":"0e02fa52-88aa-4451-a390-17f0c7816967","keyword":"电解质材料","originalKeyword":"电解质材料"},{"id":"7ff60312-4f0b-4e90-8259-a1cfb5a582ea","keyword":"物化性能","originalKeyword":"物化性能"},{"id":"6292da05-1da9-46c8-854a-5414302f3a0e","keyword":"溶解度","originalKeyword":"溶解度"}],"language":"zh","publisherId":"gncl201216003","title":"新型电解质材料[BMIM]ClO_3离子液体的合成及其物化性能","volume":"43","year":"2012"},{"abstractinfo":"<span style=\"color:red\">范</span>庄金银多金属矿床位于熊耳山西段，通过对矿床地质特征及化探异常研究，认为本区金银矿脉分布具有分带性，且与异常分布相吻合，受区内拆离断层和北东向脆性断裂控制，矿床类型为构造蚀变岩型矿床，并对区内找矿标志进行了总结，对区内找矿潜力进行了分析。","authors":[{"authorName":"王宏运","id":"cb6f0486-e88e-4ffc-ada1-612027c1bf3d","originalAuthorName":"王宏运"}],"doi":"10.11792/hj20150804","fpage":"18","id":"e985b485-bec5-4d53-9ff4-76ed095e1536","issue":"8","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"5c47ff4e-7c89-4064-91a0-a2195554c193","keyword":"矿床特征","originalKeyword":"矿床特征"},{"id":"77755bca-5957-4677-8c4b-91a7f6253919","keyword":"化探异常","originalKeyword":"化探异常"},{"id":"024c6b84-ff42-425e-85e2-1dbc149c7251","keyword":"金银矿床","originalKeyword":"金银矿床"},{"id":"cdd75c70-b4eb-46d2-a754-94bacac5349c","keyword":"找矿标志","originalKeyword":"找矿标志"},{"id":"af0438d0-15d2-4d9a-aa84-2292140490ef","keyword":"找矿潜力","originalKeyword":"找矿潜力"},{"id":"e4802e29-f15f-4851-8196-299281542751","keyword":"<span style=\"color:red\">范</span>庄金银多金属矿床","originalKeyword":"范庄金银多金属矿床"}],"language":"zh","publisherId":"huangj201508006","title":"洛宁<span style=\"color:red\">范</span>庄金银多金属矿床地质特征及找矿潜力分析","volume":"","year":"2015"},{"abstractinfo":"利用逐步回归分析的方法,确定了40MnBH钢的淬透性与化学成分之间的回归方程,以便分析化学成分对淬透性的影响程度,并应用概率论推导出求解成分内控规范的联立方程,使淬透性合格概率大于97.5%.","authors":[{"authorName":"张海","id":"da88e202-5464-49a6-880a-0a7c077f69ba","originalAuthorName":"张海"},{"authorName":"于辉","id":"6939212b-88bd-4505-8c43-d61130c16022","originalAuthorName":"于辉"},{"authorName":"姚风臣","id":"03bad0cf-522a-43fb-a66d-8a38a782d024","originalAuthorName":"姚风臣"},{"authorName":"刘德富","id":"1e1a7b85-ef86-4c90-9c44-621abf895500","originalAuthorName":"刘德富"}],"doi":"10.3969/j.issn.1000-3738.2001.06.005","fpage":"15","id":"07638a12-2aab-4883-bdd7-cb5c7ca61fc2","issue":"6","journal":{"abbrevTitle":"JXGCCL","coverImgSrc":"journal/img/cover/JXGCCL.jpg","id":"45","issnPpub":"1000-3738","publisherId":"JXGCCL","title":"机械工程材料"},"keywords":[{"id":"90626f1d-edc0-482a-89c9-14201f07dfa2","keyword":"逐步回归","originalKeyword":"逐步回归"},{"id":"0fad2e06-d7b3-460e-91c7-b46e5929dc4d","keyword":"淬透性","originalKeyword":"淬透性"},{"id":"f419a8a8-c285-440b-8c54-1e08ad9f99ea","keyword":"联立方程","originalKeyword":"联立方程"},{"id":"441277b0-b77c-41de-895b-4a95608faf3a","keyword":"概率","originalKeyword":"概率"}],"language":"zh","publisherId":"jxgccl200106005","title":"40MnBH<span style=\"color:red\">范</span>的研究","volume":"25","year":"2001"},{"abstractinfo":"","authors":[],"doi":"","fpage":"16","id":"9aee0c19-b441-45ef-86ee-595d2130c03c","issue":"3","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"53057b4d-208c-4bb4-abb8-06a51caa4f4a","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"clbh199903031","title":"四平师<span style=\"color:red\">范</span>学院科技开发中心系列化学镀镍产品介绍","volume":"32","year":"1999"},{"abstractinfo":"","authors":[],"doi":"","fpage":"6","id":"d9e15af3-593a-4247-ad97-dac7c54e8179","issue":"7","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"559112dd-8f38-4c8c-a60f-2922ca9c125c","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"clbh200007032","title":"四平师<span style=\"color:red\">范</span>学院科技开发中心系列化学镀镍产品介绍","volume":"32","year":"2000"}],"totalpage":6,"totalrecord":59}