{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"通过阳极氧化法在钛箔上制备了TiO2纳米管阵列, 在不同热处理工艺下使其晶化. 利用扫描电子显微镜(SEM)和X射线衍射(XRD)对TiO2纳米管阵列的形貌和结构进行了表征. 结果表明, 阳极氧化法制备的TiO2纳米管经450~750℃热处理后为纳米晶结构, 平均晶粒尺寸随退火温度升高而增大, 相同温度下氮气气氛中热处理的TiO2平均晶粒尺寸小于空气气氛中热处理的TiO2. 氮气气氛下退火可拓宽TiO2由锐钛矿型(Anatase)向金红石型(Rutile)结构转变的热处理温度范围, 650℃以上退火处理后, TiO2纳米管中掺杂有少量的氮. 光照开路电位测试和稳态极化曲线测试结果表明, 在氮气气氛中、经650℃退火处理2 h制备的TiO2纳米管阵列电极光电响应性能最佳, 此时TiO2为锐钛矿型和金红石型的混晶结构.","authors":[{"authorName":"","id":"c1146e24-102e-49d6-8829-df50c5e60f6a","originalAuthorName":"金冲"},{"authorName":"张卫国","id":"aeb0a863-08ec-457f-81b1-cf91da054f82","originalAuthorName":"张卫国"},{"authorName":"姚素薇","id":"6841a4d7-a348-4c33-b01a-f5120cd5e9a4","originalAuthorName":"姚素薇"},{"authorName":"王宏智","id":"0fe016a0-78d0-43f1-8d72-7d6f66cb83d5","originalAuthorName":"王宏智"}],"categoryName":"|","doi":"10.3724/SP.J.1077.2012.00054","fpage":"54","id":"416b486e-defe-405c-a6b6-f57ad12cd647","issue":"1","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"308d6f66-fd3e-49dc-b4ea-4f2b0462dc11","keyword":"TiO2纳米管","originalKeyword":"TiO2纳米管"},{"id":"ba1c3305-5849-47b2-b95f-a93def3dcfe3","keyword":" anneal","originalKeyword":" anneal"},{"id":"b5101f72-bda6-4774-b42a-f3cf2b4ce251","keyword":" crystal structure","originalKeyword":" crystal structure"},{"id":"99a6306c-f509-491a-8b6b-fa27e96d8027","keyword":" photoelectric response","originalKeyword":" photoelectric response"}],"language":"zh","publisherId":"1000-324X_2012_1_2","title":"热处理工艺对TiO2纳米管阵列结构及其光电性能的影响","volume":"27","year":"2012"},{"abstractinfo":"通过阳极氧化法在钛箔上制备了TiO2纳米管阵列,在不同热处理工艺下使其晶化,利用扫描电子显微镜(SEM)和X射线衍射(XRD)对TiO2纳米管阵列的形貌和结构进行了表征.结果表明,阳极氧化法制备的TiO2纳米管经450~750℃热处理后为纳米晶结构,平均晶粒尺寸随退火温度升高而增大,相同温度下氮气气氛中热处理的TiO2平均晶粒尺寸小于空气气氛中热处理的TiO2.氮气气氛下退火可拓宽TiO2由锐钛矿型(Anatase)向金红石型(Rutile)结构转变的热处理温度范围,650℃以上退火处理后,TiO2纳米管中掺杂有少量的氮.光照开路电位测试和稳态极化曲线测试结果表明,在氮气气氛中、经650℃退火处理2h制备的TiO2纳米管阵列电极光电响应性能最佳,此时TiO2力锐钛矿型和金红石型的混晶结构.","authors":[{"authorName":"","id":"b5ad9e3b-e660-406a-8028-38075b0c144b","originalAuthorName":"金冲"},{"authorName":"张卫国","id":"8a9ed9a8-6547-46fe-8360-a2ffaec82e8b","originalAuthorName":"张卫国"},{"authorName":"姚素薇","id":"c2486936-f29b-4baa-8e5f-2260f2a462e9","originalAuthorName":"姚素薇"},{"authorName":"王宏智","id":"781b561e-5f91-422f-994e-74bf2927ecba","originalAuthorName":"王宏智"}],"doi":"10.3724/SP.J.1077.2012.00054","fpage":"54","id":"9805cecf-500e-4286-8c6b-05877adbb891","issue":"1","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"acedda73-153d-4f58-a16b-ed74cbcc6956","keyword":"TiO2纳米管","originalKeyword":"TiO2纳米管"},{"id":"36032b5f-d553-4961-bcfa-577ecb3a8b11","keyword":"退火","originalKeyword":"退火"},{"id":"6411ea0a-8dd5-4b96-b0ec-933c287fbfb5","keyword":"晶体结构","originalKeyword":"晶体结构"},{"id":"a6e02cc5-2d90-4b07-a1d1-322dc3d5cd17","keyword":"光电响应","originalKeyword":"光电响应"}],"language":"zh","publisherId":"wjclxb201201009","title":"热处理工艺对TiO2纳米管阵列结构及其光电性能的影响","volume":"27","year":"2012"},{"abstractinfo":"在吸取强力压边精、对向凹模精、振动修边和往复裁等金属塑性加工工艺特点的基础上,首次提出了往复成形精--一种新型的厚板精工艺方法,以突破传统精技术对加工材料的厚度限制.先用数值模拟的方法对新工艺进行了研究,然后研制了用于实现新工艺的模具,该模具由两个凹模,两个凸模组成,其动作比强力压边精更复杂.研究表明,新工艺与传统工艺相比,能够加工更厚的材料,利用新工艺,项目组通过实验获得了直径为Ф30 mm,厚度为12 mm的合格圆形35#钢精件.新工艺突破了传统精工艺对材料厚度的限制,将大大拓展精技术的应用范围.","authors":[{"authorName":"彭群","id":"2b063cf6-3914-4d4e-9f77-e7b44b2e3ccc","originalAuthorName":"彭群"},{"authorName":"李荣洪","id":"2d595d80-f105-4317-9237-d6336097b80d","originalAuthorName":"李荣洪"},{"authorName":"郑鹏飞","id":"ca1fcc04-4011-404b-99ea-53ef48b282e7","originalAuthorName":"郑鹏飞"},{"authorName":"赵彦启","id":"de8da556-6d27-49f5-bdfd-0a5495e083b5","originalAuthorName":"赵彦启"},{"authorName":"陆辛","id":"57df045b-655c-44b2-8ba8-cf7090ae0d84","originalAuthorName":"陆辛"}],"doi":"10.3969/j.issn.1005-0299.2004.04.002","fpage":"342","id":"47e5df43-bfed-4f20-b7a3-eeff257e5d8f","issue":"4","journal":{"abbrevTitle":"CLKXYGY","coverImgSrc":"journal/img/cover/CLKXYGY.jpg","id":"14","issnPpub":"1005-0299","publisherId":"CLKXYGY","title":"材料科学与工艺"},"keywords":[{"id":"029cfae4-739c-4eaf-8012-cdd7847c8044","keyword":"厚板精","originalKeyword":"厚板精冲"},{"id":"d7069a20-9b23-4224-9d99-82ca932f7616","keyword":"往复成形精","originalKeyword":"往复成形精冲"},{"id":"9fc94a99-f4bf-4d15-b32f-40e7a49f1c1b","keyword":"塑性加工","originalKeyword":"塑性加工"},{"id":"0a887e7b-c509-4592-b37c-f01a766a6111","keyword":"厚度限制","originalKeyword":"厚度限制"},{"id":"d898eee5-088d-4ee7-ac3b-23c9d7eb9db6","keyword":"数值模拟","originalKeyword":"数值模拟"}],"language":"zh","publisherId":"clkxygy200404002","title":"厚板精技术的工艺研究","volume":"12","year":"2004"},{"abstractinfo":"深铌带主要应用于电解电容器行业,深铌带不但要满足内部晶粒尺寸的要求,而且要满足其后续加工的力学性能要求.深铌带要经过多次的拉伸,对铌带的生产工艺提出了很高的要求.本文研究了锻造、轧制、热处理3个关键工艺,确定了能够满足电解电容器行业用深铌带的生产加工工艺.","authors":[{"authorName":"朱军","id":"f9ec2e25-0587-43f1-89c3-bd198086e195","originalAuthorName":"朱军"},{"authorName":"张亚军","id":"0d6e675e-3404-4758-bcdf-0b13d58ab99e","originalAuthorName":"张亚军"},{"authorName":"李桂鹏","id":"8bea51e1-9955-4a1d-a86c-f94d24c88ca2","originalAuthorName":"李桂鹏"},{"authorName":"张春恒","id":"fe0ff2de-60c4-44da-a451-bc254512b8d3","originalAuthorName":"张春恒"},{"authorName":"张全","id":"60920be5-583c-4ef7-b2d9-d177a8e40f2e","originalAuthorName":"张全"}],"doi":"","fpage":"22","id":"2b4812d6-efeb-450f-8c24-193b4fb1cd97","issue":"6","journal":{"abbrevTitle":"CLKFYYY","coverImgSrc":"journal/img/cover/CLKFYYY.jpg","id":"10","issnPpub":"1003-1545","publisherId":"CLKFYYY","title":"材料开发与应用"},"keywords":[{"id":"da07b409-7535-4b6b-8c34-3c4268fcd2b2","keyword":"深铌带","originalKeyword":"深冲铌带"},{"id":"c38bff57-5e1a-4706-bb34-65f00fca1692","keyword":"晶粒尺寸","originalKeyword":"晶粒尺寸"},{"id":"d297ff08-9702-4391-a32a-477e100d12cd","keyword":"锻造工艺","originalKeyword":"锻造工艺"},{"id":"7720cf16-1e2e-4791-884b-02b64e2b0abb","keyword":"轧制工艺","originalKeyword":"轧制工艺"},{"id":"4c9bb98e-8e8d-4e97-9cf1-501996c1a789","keyword":"热处理工艺","originalKeyword":"热处理工艺"}],"language":"zh","publisherId":"clkfyyy201206006","title":"深铌带工艺研究","volume":"27","year":"2012"},{"abstractinfo":"攀钢通过优化深钢转炉冶炼、炉外精炼及连铸浇铸等工艺,使其产品夹杂物得到了控制,夹杂废品率降低.","authors":[{"authorName":"唐向东","id":"f2747794-af0b-44ba-ae62-55084c10bcc2","originalAuthorName":"唐向东"}],"doi":"10.3969/j.issn.1005-4006.2005.04.007","fpage":"18","id":"92d04dc9-721b-4b28-91cf-a977638ff6d2","issue":"4","journal":{"abbrevTitle":"LZ","coverImgSrc":"journal/img/cover/LZ.jpg","id":"52","issnPpub":"1005-4006","publisherId":"LZ","title":"连铸"},"keywords":[{"id":"991a53c4-7a8e-45b3-bc7a-b79af3cfd873","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"lz200504007","title":"深钢夹杂物控制研究","volume":"","year":"2005"},{"abstractinfo":"ABS合金化是提高ABS综合性能的有效途径.本研究开发成功ABS/PVC、ABS/PC、ABS/SMA合金,其中ABS/PC合金具有阻燃、耐热、高抗性能.","authors":[{"authorName":"马玫","id":"766607de-49eb-40a9-a796-ac2115106974","originalAuthorName":"马玫"},{"authorName":"刘冠文","id":"1ff7a500-2db0-4bdf-a7f2-858a393bbcf5","originalAuthorName":"刘冠文"},{"authorName":"朱继芳","id":"d6afd505-3494-4e89-b2fb-38abfac3aa44","originalAuthorName":"朱继芳"},{"authorName":"谢春灼","id":"467cb05c-1c85-4f91-a700-a845cace707b","originalAuthorName":"谢春灼"}],"doi":"10.3969/j.issn.1671-5381.2004.01.004","fpage":"11","id":"f28f27bd-e372-4a9b-9cf6-1ef344db2809","issue":"1","journal":{"abbrevTitle":"HCCLLHYYY","coverImgSrc":"journal/img/cover/HCCLLHYYY.jpg","id":"42","issnPpub":"1671-5381","publisherId":"HCCLLHYYY","title":"合成材料老化与应用"},"keywords":[{"id":"3e7f0f78-6dd3-4764-8dbc-028bbd580914","keyword":"ABS合金","originalKeyword":"ABS合金"},{"id":"56a66f9d-d58d-4543-a729-7e2e7fc0e312","keyword":"阻燃","originalKeyword":"阻燃"},{"id":"fdcb98ff-b48e-43b7-a91f-703c9be25c54","keyword":"耐热","originalKeyword":"耐热"},{"id":"9db80c13-681d-47fd-9d59-1d7d2b82f56c","keyword":"抗","originalKeyword":"抗冲"}],"language":"zh","publisherId":"hccllhyyy200401004","title":"阻燃、耐热、高抗ABS合金","volume":"33","year":"2004"},{"abstractinfo":"为了研究管材液压冲孔中头形状对塌陷的影响规律,采用7种不同形状的头进行了液压冲孔实验,分析了头形状对液压冲孔质量的影响.实验结果表明:塌陷深度随着头端面倾斜角度的增大而减小,随着头圆角的增大而增大.提高内压能够降低塌陷深度,塌陷深度随着管内压力的增大而减小.不同形状头对塌陷的影响不同,斜头冲孔后塌陷较小,圆角头冲孔后塌陷较大.","authors":[{"authorName":"齐延兵","id":"90604e13-e33d-4b34-a4dd-e0d49e5fd1b8","originalAuthorName":"齐延兵"},{"authorName":"林俊峰","id":"ca952055-6945-4a73-98a5-4aaa24eff8d5","originalAuthorName":"林俊峰"},{"authorName":"苏海波","id":"847ee19a-73c7-412f-a612-f1ac05e2dad1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figure"}],"language":"zh","publisherId":"0412-1961_1989_6_4","title":"深汽车簿钢板织构的表述方法","volume":"25","year":"1989"},{"abstractinfo":"济钢1750高炉渣系统由于使用焦化水渣,粒化轮、脱水器内部腐蚀严重,设备维护作业量大、安全施工难度高.为此,对冲渣系统进行无粒化轮渣的工艺和设备改造,实现了渣设备的安全定期检修,大大降低了日常的维护作业量,确保了设备的稳定运行,有效保障了高炉的正常生产.","authors":[{"authorName":"岳岗","id":"8554f626-292a-4149-95d5-c56483cf17d7","originalAuthorName":"岳岗"},{"authorName":"谭昕","id":"9bbdde79-928a-47d1-a4b1-ae298c7e35ff","originalAuthorName":"谭昕"},{"authorName":"张旺","id":"0c8fb590-0175-4f41-b0b2-51b6badce549","originalAuthorName":"张旺"}],"doi":"10.3969/j.issn.1001-7208.2009.05.012","fpage":"56","id":"ef71f470-1def-4279-b585-d34907d83918","issue":"5","journal":{"abbrevTitle":"SHJS","coverImgSrc":"journal/img/cover/SHJS.jpg","id":"59","issnPpub":"1001-7208","publisherId":"SHJS","title":"上海金属"},"keywords":[{"id":"cfe035a4-3759-4b0d-8dc3-79594073e8ac","keyword":"高炉渣系统","originalKeyword":"高炉冲渣系统"},{"id":"abdca93e-11b1-4e4a-9c6a-8c012d643e9c","keyword":"粒化轮","originalKeyword":"粒化轮"},{"id":"8fa9118d-56d2-454b-9fcb-0b034b17ba53","keyword":"脱水器","originalKeyword":"脱水器"},{"id":"647e30ca-b89b-4d9a-a339-41e7b33d2864","keyword":"优化改造","originalKeyword":"优化改造"}],"language":"zh","publisherId":"shjs200905012","title":"济钢1750高炉渣系统的优化改造","volume":"31","year":"2009"},{"abstractinfo":"介绍了攀钢根据DIN EN10142标准开发家电用深光整热镀锌钢板的情况,概述了低碳铝镇静钢和IF钢深热镀锌板的性能及应用情况.","authors":[{"authorName":"郑之旺","id":"840cc895-c1c8-4989-95e3-edb9fe9797b7","originalAuthorName":"郑之旺"}],"doi":"10.3969/j.issn.1004-7638.2002.04.008","fpage":"31","id":"f6fa25b4-a084-4b89-abb5-10d7ea8236f1","issue":"4","journal":{"abbrevTitle":"GTFT","coverImgSrc":"journal/img/cover/gtft1.jpg","id":"28","issnPpub":"1004-7638","publisherId":"GTFT","title":"钢铁钒钛"},"keywords":[{"id":"fdc2862a-c68f-4d18-8d98-b95d047f376d","keyword":"光整热镀 锌板","originalKeyword":"光整热镀 锌板"},{"id":"c891c1c8-4947-4426-a7de-6b8138dfe16f","keyword":"深","originalKeyword":"深冲"},{"id":"5344ca9d-f749-49d8-930f-dd9abbe2f79f","keyword":"低碳铝镇静钢","originalKeyword":"低碳铝镇静钢"},{"id":"f2081a30-2671-42e4-8b70-de67a3059f75","keyword":"IF钢","originalKeyword":"IF钢"}],"language":"zh","publisherId":"gtft200204008","title":"家电用深光整热镀锌钢板开发","volume":"23","year":"2002"}],"totalpage":303,"totalrecord":3030}