{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"半水基注凝成型工艺中由于醇类有机溶剂的加入可以明显防止大尺寸零部件在干燥过程中的开裂问题,但是以醇类有机溶剂代替部分水溶剂来配置料浆必然对料浆的流变特性产生影响;本工作研究了1,3丁二醇、1,4丁二醇、乙二醇和丙三醇四种有机醇溶剂代替部分水配置陶瓷料浆,重点考察不同醇类及其含量对料浆的流变性能的影响规律.实验结果表明,四种有机醇溶剂的加入都使料浆的黏度增加,而且产生不同程度的触变性,其中,以加入30%和40%丙三醇料浆的触变性最明显,而加入10%乙二醇的陶瓷料浆最接近水基料浆的特性,最适合用于半水基注凝工艺.","authors":[{"authorName":"梁艳媛","id":"ea8d5e88-f9db-44e9-9790-447abd936251","originalAuthorName":"梁艳媛"},{"authorName":"陈大明","id":"f3e8ca14-ef27-481e-8927-39d5c794b9b7","originalAuthorName":"陈大明"},{"authorName":"仝建峰","id":"44372bb8-c275-4a63-8e8d-beedac860a0f","originalAuthorName":"仝建峰"},{"authorName":"李宝伟","id":"42d3044f-8722-4203-9288-eefd69c921d6","originalAuthorName":"李宝伟"},{"authorName":"焦春荣","id":"c824f8ca-cdf7-4f55-b432-6c80ebceb2ea","originalAuthorName":"焦春荣"}],"doi":"10.3969/j.issn.1001-4381.2010.z2.073","fpage":"260","id":"c22dbb24-a308-4522-b0a6-ac8d1fb1218d","issue":"z2","journal":{"abbrevTitle":"CLGC","coverImgSrc":"journal/img/cover/CLGC.jpg","id":"9","issnPpub":"1001-4381","publisherId":"CLGC","title":"材料工程"},"keywords":[{"id":"aefcff1c-db0b-4859-a7b8-7aad85ca0ab7","keyword":"半水基","originalKeyword":"半水基"},{"id":"c3b1eb55-c253-4f2d-8e38-e9ef69ad48a1","keyword":"流变性能","originalKeyword":"流变性能"},{"id":"d56a7bac-a802-4790-b3ae-1bf77295e4f4","keyword":"凝胶注模","originalKeyword":"凝胶注模"},{"id":"357edc10-75ce-490b-98bb-8b90aa5306d7","keyword":"陶瓷料浆","originalKeyword":"陶瓷料浆"}],"language":"zh","publisherId":"clgc2010z2073","title":"半水基料浆的流变性能研究","volume":"","year":"2010"},{"abstractinfo":"采用不同工艺制备BSAS(BaO‐SrO‐Al2 O3‐SiO2)喷涂粉体。研究喷涂粉体特性及其对等离子喷涂工艺制备的环境障涂层结构和性能的影响。结果表明:粉体造粒工艺制备的BSAS喷涂粉体颗粒不均匀,流动性差。制备的涂层粗糙,孔隙率高,结合强度为24.1M Pa;造粒烧结工艺制备的BSAS喷涂粉体表面圆滑,流动性好,沉积效率高。制备的涂层结构均匀,少孔隙,无裂纹,结合强度达到29.8M Pa ,涂层中BSAS相保留率最高,达到53.2%;熔融破碎工艺制备的BSAS粉体呈致密不规则块状,虽然流动性好沉积效率高,制备的涂层光滑且孔隙极少,但微裂纹较多,结合强度仅为14.2M Pa ,粉体经喷涂后发生相结构重组,BSAS相保留率为20.5%,对涂层的高温性能不利。分析认为,造粒烧结工艺制备BSAS粉体具有工艺过程简化、粉体质量好、相稳定性高等优点,更适合于等离子喷涂的要求。","authors":[{"authorName":"焦春荣","id":"2e79c6b0-a257-41b1-8a29-7d9797188468","originalAuthorName":"焦春荣"},{"authorName":"焦健","id":"8135d861-51c9-4b09-93bf-0829f4383c85","originalAuthorName":"焦健"},{"authorName":"陈大明","id":"5d4adf1f-7061-42c6-b5b8-745e036146a1","originalAuthorName":"陈大明"},{"authorName":"王岭","id":"b7da545c-9449-44d5-b750-8ad24ecc9e62","originalAuthorName":"王岭"}],"doi":"10.11868/j.issn.1001-4381.2016.08.009","fpage":"51","id":"f407a663-0967-4b9b-9970-5c0a20ea41e8","issue":"8","journal":{"abbrevTitle":"CLGC","coverImgSrc":"journal/img/cover/CLGC.jpg","id":"9","issnPpub":"1001-4381","publisherId":"CLGC","title":"材料工程"},"keywords":[{"id":"ce6572e8-480e-4c59-b9c4-3f1c074f6554","keyword":"等离子喷涂","originalKeyword":"等离子喷涂"},{"id":"2ef57741-6949-4f11-8f34-9ad77cbaae99","keyword":"BSAS粉体","originalKeyword":"BSAS粉体"},{"id":"864275e3-f6e0-4d2b-9ff5-29c7d825a0ac","keyword":"环境障涂层","originalKeyword":"环境障涂层"}],"language":"zh","publisherId":"clgc201608010","title":"BSAS 喷涂粉体制备工艺及其对涂层性能的影响","volume":"44","year":"2016"},{"abstractinfo":"采用等离子喷涂工艺在SiC陶瓷表面制备了BSAS环境障涂层,分析研究了环境障涂层的微观结构、结合强度、长期抗氧化性能、抗热震性能和抗高温水氧腐蚀性能。结果表明: BSAS环境障涂层的结合强度为29 MPa,内部结构均匀,无贯穿裂纹和连通气孔;涂层热震30次开始有微裂纹,热震50次后出现贯穿裂纹失效;涂层于空气中1200℃/200 h氧化后增重0?24%,内部氧化不明显;在1 atm、1200℃、50%H2 O-50%O2、0?4 m/s高温水氧环境中腐蚀150 h后,涂层保护试样失重0?87 mg/cm2,涂层表面腐蚀厚度小于10μm,无涂层保护的试样失重3?4 mg/cm2。","authors":[{"authorName":"焦春荣","id":"5de38cb4-f7c9-4bbe-95b5-6c279a714027","originalAuthorName":"焦春荣"},{"authorName":"王岭","id":"743e9b14-d70a-4662-b68b-09aee2be01c5","originalAuthorName":"王岭"},{"authorName":"杨金华","id":"aacc1983-8533-4773-a2ee-86006126cf24","originalAuthorName":"杨金华"},{"authorName":"刘善华","id":"a5283057-7485-4cc4-933b-ffd5bfc2cc82","originalAuthorName":"刘善华"}],"doi":"10.7502/j.issn.1674-3962.2016.06.11","fpage":"466","id":"d001be16-649e-4aa1-92e8-f26b374fc386","issue":"6","journal":{"abbrevTitle":"ZGCLJZ","coverImgSrc":"journal/img/cover/中国材料进展.jpg","id":"80","issnPpub":"1674-3962","publisherId":"ZGCLJZ","title":"中国材料进展"},"keywords":[{"id":"b5de91bd-4d85-48b3-a68e-c2e5268eb39b","keyword":"等离子喷涂","originalKeyword":"等离子喷涂"},{"id":"d0f50307-6d58-484b-90a5-85e2d49df8ca","keyword":"BSAS粉体","originalKeyword":"BSAS粉体"},{"id":"6f42c137-32d8-4e2b-baf6-a1eaed420472","keyword":"环境障涂层","originalKeyword":"环境障涂层"}],"language":"zh","publisherId":"zgcljz201606013","title":"等离子喷涂 BSAS环境障涂层性能研究","volume":"35","year":"2016"},{"abstractinfo":"采用Chiralpak IC手性柱(250 mm×4.6 mm,5 μm),建立了正相高效液相色谱测定板蓝根中表告依春(R-告依春)和告依春(S-告依春)含量的方法.考察了流动相组成、流速和柱温对分离度的影响.经优化后的实验条件:以正己烷-异丙醇(体积比为90∶10)为流动相,流速为0.8 mL/min;检测波长为245 nm,柱温为20 ℃.在此优化条件下,表告依春和告依春分离度为3.4,检出限为2.0 mg/L,在0.02~2.0 g/L 范围内有良好的线性关系,平均回收率为101% ,相对标准偏差(RSD)小于3.0%(n=6).本方法可将具有抗病毒活性的表告依春与其对映体告依春基线分离并测定,专属性强,能有效控制板蓝根的质量.","authors":[{"authorName":"聂黎行","id":"fee7f0b1-4bfd-4c4e-9d65-d7f03c2a918a","originalAuthorName":"聂黎行"},{"authorName":"王钢力","id":"ee281225-e77f-4477-a486-a098ca91b1db","originalAuthorName":"王钢力"},{"authorName":"戴忠","id":"813e1426-d061-4e41-9723-d75cfa16968e","originalAuthorName":"戴忠"},{"authorName":"林瑞超","id":"3034f33a-eaf2-4665-8751-f5ef70c65379","originalAuthorName":"林瑞超"}],"doi":"10.3724/SP.J.1123.2010.01001","fpage":"1001","id":"32355b8f-ccce-4726-b210-eaacc0917986","issue":"10","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"5c41c71f-d053-43ba-8aa9-32ad96d3cca4","keyword":"手性高效液相色谱法","originalKeyword":"手性高效液相色谱法"},{"id":"e26a591e-56ec-4bb4-acfd-5d5f7ad919ea","keyword":"表告依春(R-告依春)","originalKeyword":"表告依春(R-告依春)"},{"id":"1e32ab35-876b-46d9-9898-47fb5c40d701","keyword":"告依春(S-告依春)","originalKeyword":"告依春(S-告依春)"},{"id":"8c1b4600-8fac-47f6-98f6-6670e2a0daa9","keyword":"板蓝根","originalKeyword":"板蓝根"}],"language":"zh","publisherId":"sp201010018","title":"手性高效液相色谱法测定板蓝根中表告依春和告依春含量","volume":"28","year":"2010"},{"abstractinfo":"对干法熄焦和稳定熄焦的技术特点和优势进行了分析比较.指出:干法熄焦回收占焦炉能耗的35%~40%的红焦显热是稳定熄焦所不具备的优势;干法熄焦改善焦炭质量是稳定熄焦所无法比拟的;干法熄焦在减少对环境污染方面显著优于稳定熄焦;各国能源情况和能源价格的差异决定了这些国家选择哪一种熄焦方式.","authors":[{"authorName":"郑文华","id":"232bbd03-2f87-44fe-a2b4-3fe561fd7d72","originalAuthorName":"郑文华"},{"authorName":"张晓光","id":"b29c3448-20f9-4a6b-8f4d-bf4c0405b924","originalAuthorName":"张晓光"}],"doi":"","fpage":"70","id":"7dca7c54-37c8-4515-85ce-b6739323c608","issue":"11","journal":{"abbrevTitle":"GT","coverImgSrc":"journal/img/cover/GT.jpg","id":"27","issnPpub":"0449-749X","publisherId":"GT","title":"钢铁"},"keywords":[{"id":"c5065eb8-8d4b-4374-a68a-f940e8d650be","keyword":"干法熄焦","originalKeyword":"干法熄焦"},{"id":"30c03b4a-4710-43b4-ae61-3c192e57cee2","keyword":"稳定熄焦","originalKeyword":"稳定熄焦"},{"id":"ed92f3b0-8758-4ac2-a3b3-5f9633fd2d06","keyword":"比较","originalKeyword":"比较"}],"language":"zh","publisherId":"gt200411018","title":"干法熄焦和稳定熄焦","volume":"39","year":"2004"},{"abstractinfo":"利用铱催化高碘酸钾氧化丽春红G(PG)的褪色反应,建立了测定痕量铱的催化动力学光度法.在硫酸介质和90℃加热15min的条件下,于500nm波长处,采用固定时间法测定丽春红G吸收值的降低.Ir(Ⅳ)的浓度在0~1.0μg/25mL范围内与催化反应的速率有良好的线性关系,检出限为1 81 ×10 mg/mL.对0.3μg/25mLIr(Ⅳ)测定的相对标准偏差为1.61%(n=11).体系至少稳定3.5h.考察了40多种共存离子的影响,大多数常见离子不干扰,方法有较好的选择性.催化反应对Ir(Ⅳ)和丽春红G均为一级反应,催化反应的表观活化能为103.66kJ/mol.用于冶金产品及岩矿中铱的测定,结果与推荐值十分吻合.","authors":[{"authorName":"侯能邦","id":"92c62fdf-fec8-4163-aad2-9ed54b7fdce6","originalAuthorName":"侯能邦"},{"authorName":"李祖碧","id":"c4dacfbe-4824-4cbe-a844-91a76be4f69c","originalAuthorName":"李祖碧"},{"authorName":"李崇宁","id":"f7a10f8c-895c-486c-ad99-2b32db2c7164","originalAuthorName":"李崇宁"},{"authorName":"王加林","id":"6d15967f-b1aa-492c-9003-5900696277f5","originalAuthorName":"王加林"},{"authorName":"曹秋娥","id":"b89522cc-6338-40b9-bb28-a8fc73f09d40","originalAuthorName":"曹秋娥"}],"doi":"10.3969/j.issn.1000-7571.2002.05.006","fpage":"17","id":"cf8ee9a7-e782-4fcb-866c-e15d9126e60f","issue":"5","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析 "},"keywords":[{"id":"3c381e65-e813-4912-b9c8-15299a341a75","keyword":"铱","originalKeyword":"铱"},{"id":"90683ee6-f835-43a8-b573-bc0be1641329","keyword":"丽春红G","originalKeyword":"丽春红G"},{"id":"a2a57fdf-fa6d-4d5d-bc97-967b1b2de292","keyword":"高碘酸钾","originalKeyword":"高碘酸钾"},{"id":"4ffcfe3c-3af4-41cd-ae8f-447d4f037585","keyword":"催化光度法","originalKeyword":"催化光度法"}],"language":"zh","publisherId":"yjfx200205006","title":"高碘酸钾氧化丽春红G催化光度法测定铱","volume":"22","year":"2002"},{"abstractinfo":"为了研究一种脱硫活性好、机械强度大的成型活性焦,用正交试验法制备成型活性焦,并对各因素进行方差分析和效应考察,得到了用榆林废弃的半焦焦粉制备耐压强度高、脱硫效果好的成型活性焦的工艺条件.使用微机控制电子万能试验机进行耐压强度的测量,利用氮气等温吸附方法测量了原料及成品活性焦的孔结构.最优条件下制备的活性焦碘吸附值为304.8mg/g;比表面积为303.6m2/g;孔容为0.229 9mL/g;前5h的脱硫量达到80%以上,满足烧结烟气脱硫的要求.","authors":[{"authorName":"郑亚旭","id":"c8c4daae-4d37-4186-8a01-e2fd3a03ef47","originalAuthorName":"郑亚旭"},{"authorName":"张建良","id":"efeafeb9-e24c-470a-83af-c39eb6601ae5","originalAuthorName":"张建良"},{"authorName":"刘征建","id":"446a1285-9ea0-4514-a9c1-96242374467a","originalAuthorName":"刘征建"},{"authorName":"杨成杰","id":"6876a7ea-0f83-49a5-b3cb-e73deeb2bbbf","originalAuthorName":"杨成杰"},{"authorName":"付亚清","id":"51c00fa7-7c6b-4fb5-96a2-fa67bdb5e0af","originalAuthorName":"付亚清"}],"doi":"","fpage":"11","id":"2021b33d-c32a-4593-9bd6-62fbe3445a0d","issue":"5","journal":{"abbrevTitle":"GTYJXB","coverImgSrc":"journal/img/cover/GTYJXB.jpg","id":"30","issnPpub":"1001-0963","publisherId":"GTYJXB","title":"钢铁研究学报"},"keywords":[{"id":"d5982521-b96b-42d0-9d6a-35dde4c78ff6","keyword":"钢铁冶金","originalKeyword":"钢铁冶金"},{"id":"1ae480b0-4d2d-4447-aace-29af7e2ee70d","keyword":"烧结","originalKeyword":"烧结"},{"id":"95dedeb6-7d67-4a61-a068-4cdf8b0f6a8a","keyword":"半焦","originalKeyword":"半焦"},{"id":"c8985ff0-24b7-4353-bce7-d931acfeec83","keyword":"活性焦","originalKeyword":"活性焦"},{"id":"7c233fa1-3590-4a49-b38a-c9e86ff66b69","keyword":"烟气脱硫","originalKeyword":"烟气脱硫"}],"language":"zh","publisherId":"gtyjxb201005003","title":"半焦制备烧结烟气脱硫用活性焦","volume":"22","year":"2010"},{"abstractinfo":"缚硫焦是在高硫炼焦煤中加入缚硫剂,使之“缚”住其中尽可能多的硫在炼铁时直接进入炉渣,减少生铁中硫的污染。用缚硫焦和高硫焦分别进行炼铁试验,结果表明:用缚硫焦在小高炉中炼出的铸造生铁,其合格率巳达到90%以上,取得的各项炼铁技术经济指标均显示出有一定的优越性。在炼铁试验中,曾分层从高炉中取出焦炭、矿石、熔剂、生铁和炉渣五种炉料的样品,经过大量分析,得出在分别用缚硫焦和高硫焦炼铁期间五种炉料中沿高炉高度方向的含硫量变化,从而比较清楚地掌握了硫在高炉内的活动规律。这对进一步研究提高缚硫效果以及生铁的硫化和脱硫机理,有一定的意义。","authors":[{"authorName":"龙世刚","id":"d9558673-995c-482b-a19d-5f46f657e314","originalAuthorName":"龙世刚"}],"categoryName":"|","doi":"","fpage":"169","id":"6f2a962c-4737-4ac4-ba3e-2762e118561f","issue":"3","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[],"language":"zh","publisherId":"0412-1961_1977_3_6","title":"缚硫焦炼铁试验","volume":"13","year":"1977"},{"abstractinfo":"介绍了干熄焦技术的原理和特点,国外干熄焦技术的发展以及国内干熄焦技术的应用现状,并对我国大力发展干熄焦的必要性进行了综述.","authors":[{"authorName":"刘智平","id":"dc022f59-f944-42a0-adef-ebdda62e890b","originalAuthorName":"刘智平"}],"doi":"10.3969/j.issn.1001-1447.2004.01.016","fpage":"58","id":"23593c24-cf70-4023-82ad-d68031a17f38","issue":"1","journal":{"abbrevTitle":"GTYJ","coverImgSrc":"journal/img/cover/GTYJ.jpg","id":"29","issnPpub":"1001-1447","publisherId":"GTYJ","title":"钢铁研究"},"keywords":[{"id":"ca5b42e8-9190-4467-8484-bdf20c07caa8","keyword":"干熄焦","originalKeyword":"干熄焦"},{"id":"afaf127a-3375-4d76-9455-9e85fc5ef54a","keyword":"技术发展及应用","originalKeyword":"技术发展及应用"},{"id":"cbb70d4e-d0d0-4335-b0f9-ca86cc2f4ea0","keyword":"综述","originalKeyword":"综述"}],"language":"zh","publisherId":"gtyj200401016","title":"干熄焦技术及其应用","volume":"32","year":"2004"},{"abstractinfo":"在90 ℃水浴中,Co2+ 能催化铋酸钠氧化丽春红S褪色,据此建立了一种褪色光度法测定Co2+ 的新方法.Co2+在0~50 μg/mL范围内遵守比尔定律,表观摩尔吸光系数为1.814×103 L/(mol*cm),最大吸收波长为520 nm,该方法检出限为0.538 μg/mL.该方法用于测定锡-钴枪黑色合金镀液中钴的含量,结果令人满意.","authors":[{"authorName":"郭振良","id":"584bf7f2-7e7f-4127-ade6-2c272d72dfbf","originalAuthorName":"郭振良"},{"authorName":"唐清华","id":"9ce2a809-b843-4434-8e7c-dac0f58527cb","originalAuthorName":"唐清华"},{"authorName":"牟起娜","id":"d37d8b39-f7ec-454c-a7d0-cf3e62dd6762","originalAuthorName":"牟起娜"},{"authorName":"孙言志","id":"7c0484e8-9cab-4b29-a48b-4bcb2c838cd8","originalAuthorName":"孙言志"}],"doi":"10.3969/j.issn.1004-227X.2005.12.018","fpage":"63","id":"8c6b0946-37e5-47d0-aff4-bf52e1cf4d1a","issue":"12","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰 "},"keywords":[{"id":"f6c28cfe-17af-49c2-b37f-6d1108f657b6","keyword":"丽春红S","originalKeyword":"丽春红S"},{"id":"cde44370-4a27-46a1-9f05-62ccb3d33206","keyword":"褪色光度法","originalKeyword":"褪色光度法"},{"id":"e7ed13de-3a0a-4b14-b563-e2203460d95f","keyword":"合金镀液","originalKeyword":"合金镀液"},{"id":"6cccbb22-6b70-42fd-9eb3-d3701b2868e9","keyword":"钴","originalKeyword":"钴"}],"language":"zh","publisherId":"ddyts200512018","title":"丽春红S褪色光度法测定锡-钴合金镀液中的钴","volume":"24","year":"2005"}],"totalpage":76,"totalrecord":752}