{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"用电阻测定及X射线衍射法研究了共晶成分Au-Si合金快速凝固箔带在等温时效时的相变过程,提出了由非晶态至平衡态的四阶段转变顺序,分析了各亚稳相的结构和电子浓度特征,说明在等温时效过程中亦可生成Hume-Rothery电子化合物及尺寸因素化合物。","authors":[{"authorName":"李松瑞","id":"eda1e050-2e94-448c-ad39-eab5ca66d5ee","originalAuthorName":"李松瑞"},{"authorName":"高世谷","id":"48292fe8-9db5-4d89-97ac-a300fb1b0f5d","originalAuthorName":"高世谷"},{"authorName":"高秀娟","id":"0f1b8d07-bccf-439a-8158-9c2920d83d69","originalAuthorName":"高秀娟"}],"categoryName":"|","doi":"","fpage":"407","id":"5dd1680b-5e4f-4ac0-9e47-198f6a2fb5f0","issue":"5","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[{"id":"23ff69ea-e4ff-4ed3-baa6-362ae190940a","keyword":"Au-Si非晶态","originalKeyword":"Au-Si非晶态"},{"id":"1f80f5f4-850b-40a7-b281-02dfeeeb5419","keyword":"isothermal phase transformation","originalKeyword":"isothermal phase transformation"},{"id":"f1441f8e-f823-4717-89ac-2e477426dc8a","keyword":"null","originalKeyword":"null"}],"language":"zh","publisherId":"0412-1961_1988_5_22","title":"Au-Si非晶态合金的恒温相变","volume":"24","year":"1988"},{"abstractinfo":"研究了将谷朊粉溶解于水的方法和其在水性建筑涂料中的应用.谷朊粉的耐水性差,不能用作建筑涂料的主要基料,但其具有良好的粘结性、流动性和流平性,可用在合成树脂乳液内墙涂料中,作增稠剂使用,使涂料具有良好的流平性和涂膜外观,而成本与常用的增稠剂相差不大.","authors":[{"authorName":"徐峰","id":"0c879c81-d169-4d44-b81a-5e306a3215de","originalAuthorName":"徐峰"},{"authorName":"张玉林","id":"8dc4a181-30ea-4b74-b95d-37c6158a63d3","originalAuthorName":"张玉林"}],"doi":"10.3969/j.issn.0253-4312.2004.05.017","fpage":"56","id":"34a60df7-9680-439b-a2fc-fedbad6e77cf","issue":"5","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业 "},"keywords":[{"id":"5e763c91-7c2a-4ab8-915b-5e5e9c21d1d6","keyword":"谷朊粉","originalKeyword":"谷朊粉"},{"id":"3bee3ea1-081f-4e5f-9329-f9f0f07eb050","keyword":"水性涂料","originalKeyword":"水性涂料"},{"id":"3152e260-c2c2-4806-8742-0eb537a9e158","keyword":"建筑涂料","originalKeyword":"建筑涂料"},{"id":"3b7d2a6f-2bf4-493e-ae55-1ea787a09e39","keyword":"涂膜外观","originalKeyword":"涂膜外观"},{"id":"dbfdc095-7edc-474a-b6a5-2c292cda911c","keyword":"增稠剂","originalKeyword":"增稠剂"}],"language":"zh","publisherId":"tlgy200405017","title":"谷朊粉在水性建筑涂料中的应用","volume":"34","year":"2004"},{"abstractinfo":"采用液相还原法制备了介孔碳(CMC)担载的Pd催化剂,用于β-谷甾醇加氢制备β-谷甾烷醇反应.与活性碳担载的Pd催化剂相比,Pd/CMC的活性更高,这归因于该催化剂具有较大的孔径,从而有利于较大分子的催化加氢反应.","authors":[{"authorName":"陈慧","id":"5fc3a732-3094-4b89-bb3d-8d872e7b35eb","originalAuthorName":"陈慧"},{"authorName":"戴乐","id":"22cb9e2f-5030-40f9-8a74-b53ce7fab47e","originalAuthorName":"戴乐"},{"authorName":"谢建新","id":"adb287c7-0e73-474e-bfb5-ecb94020f41c","originalAuthorName":"谢建新"},{"authorName":"白志平","id":"5d9583e0-5cd0-44ff-8731-13a454b51337","originalAuthorName":"白志平"},{"authorName":"贾敏慧","id":"cfe17897-4e4b-4a38-b638-8ebd1fcb9c48","originalAuthorName":"贾敏慧"},{"authorName":"沈俭一","id":"dd21ba71-72d0-49ec-8809-2f70b692d1f4","originalAuthorName":"沈俭一"}],"doi":"10.1016/S1872-2067(10)60294-X","fpage":"1777","id":"66f952b9-1edb-4743-b347-2df6adda67d9","issue":"12","journal":{"abbrevTitle":"CHXB","coverImgSrc":"journal/img/cover/CHXB.jpg","id":"18","issnPpub":"0253-9837","publisherId":"CHXB","title":"催化学报 "},"keywords":[{"id":"12addb2f-a7e9-463f-9bb7-f406dbab1072","keyword":"钯","originalKeyword":"钯"},{"id":"c8fb89d1-2573-42ee-88d4-3a4be9533d29","keyword":"活性碳","originalKeyword":"活性碳"},{"id":"8d322085-d710-48ac-8f6a-e792946170e7","keyword":"负载型催化剂","originalKeyword":"负载型催化剂"},{"id":"45bf4488-d860-448d-88c3-9d34889532cb","keyword":"介孔碳","originalKeyword":"介孔碳"},{"id":"b556aec4-e05b-44a7-8cc2-812c54c08395","keyword":"孔径效应","originalKeyword":"孔径效应"},{"id":"a06decf0-6289-454f-885d-09eee3b3d879","keyword":"微量吸附量热","originalKeyword":"微量吸附量热"},{"id":"3fe9ebd7-86a9-4e4e-9ba7-b22714488ba2","keyword":"β-谷甾醇","originalKeyword":"β-谷甾醇"},{"id":"f512f7b4-e76f-4709-a829-a17ba6f3c3f5","keyword":"加氢","originalKeyword":"加氢"},{"id":"82afe131-f93d-44b7-b8b4-f73045dc76f6","keyword":"β-谷甾烷醇","originalKeyword":"β-谷甾烷醇"}],"language":"zh","publisherId":"cuihuaxb201112001","title":"介孔碳负载的Pd催化剂催化β-谷甾醇加氢制备β-谷甾烷醇","volume":"32","year":"2011"},{"abstractinfo":"为实现对环境及食品样品中黄曲霉毒素B1的高灵敏检测,通过优化一系列试剂盒参数,研制了一步间接竞争ELISA检测试剂盒.优化后的包被缓冲液为90 mmol·L-1、pH 4.6的柠檬酸缓冲液,最佳反应pH值为7.4,抗体包被浓度为0.2μg·mL-1, HRP?BSA?AFB1稀释比为1/4000,标品稀释液为含7%甲醇的PBST溶液.优化后试剂盒IC50值为66 pg·mL-1,检测限为7.6 pg·mL-1,检测线性范围为10—810 pg·mL-1.试剂盒对不同AFB1添加水平(0.5μg·kg-1,1μg·kg-1)的玉米、豆粕和鱼粉样品平均回收率为108.4%—134.8%.对玉米、豆粕和鱼粉样品各20份盲样测试结果表明,试剂盒检测结果与HPLC?MS/MS检测结果吻合.","authors":[{"authorName":"孙清","id":"7c3952a1-ed28-42aa-ac3b-36375413d269","originalAuthorName":"孙清"},{"authorName":"李谷丰","id":"601d124b-ad4b-4b0d-9fec-247a975f9826","originalAuthorName":"李谷丰"},{"authorName":"邓乾民","id":"ae19371f-fb9c-4aca-b27d-0b1b0c765804","originalAuthorName":"邓乾民"},{"authorName":"刘杰民","id":"73684e21-6b8b-457a-9c83-08853e202204","originalAuthorName":"刘杰民"},{"authorName":"时国庆","id":"e173ff6d-5070-4d1a-86e7-32efd0ddb666","originalAuthorName":"时国庆"}],"doi":"10.7524/j.issn.0254-6108.2015.10.2015031001","fpage":"1845","id":"8a1ff06a-ff36-4b00-a602-559a38b37d70","issue":"10","journal":{"abbrevTitle":"HJHX","coverImgSrc":"journal/img/cover/HJHX.jpg","id":"43","issnPpub":"0254-6108","publisherId":"HJHX","title":"环境化学 "},"keywords":[{"id":"d1b1a8d6-4d80-491a-ba27-73c28edb94a8","keyword":"ELISA","originalKeyword":"ELISA"},{"id":"95516de1-9ed5-4e54-add1-f64b0f8f9cf4","keyword":"黄曲霉毒素B1","originalKeyword":"黄曲霉毒素B1"},{"id":"912060f2-2559-434a-9041-a3cc63ed6aa5","keyword":"残留","originalKeyword":"残留"},{"id":"a45ad9a5-cee4-4439-a8a4-3342ff52c4c4","keyword":"试剂盒","originalKeyword":"试剂盒"}],"language":"zh","publisherId":"hjhx201510012","title":"高灵敏黄曲霉毒素B1酶联免疫试剂盒的研制及应用?孙清1,2李谷丰3邓乾民3刘杰民1,2时国庆2??","volume":"","year":"2015"},{"abstractinfo":"以金谷山金矿床的成矿地质特征为基础, 研究了区域地球化学场及异常特征、岩(矿)石微量元素地球化学特征.矿床位于金及其它成矿元素的高背景场中,与成矿有关的元素组合为Au-Sb-As,异常强度高,分带性明显;地层、岩浆岩、构造等地质单元的地球化学特征表明,成岩作用、构造作用与成矿作用关系密切.","authors":[{"authorName":"王建新","id":"069d878e-4d4e-4613-aa5f-ace4d2f828e8","originalAuthorName":"王建新"},{"authorName":"臧兴运","id":"906f5c55-30bf-45e4-b5c7-3dd242097cd7","originalAuthorName":"臧兴运"},{"authorName":"付阳","id":"91bd313b-49c4-465b-96b2-b9fbaf42b18e","originalAuthorName":"付阳"},{"authorName":"王超","id":"9abd56ce-ef54-40dd-8ef8-50cd67c76202","originalAuthorName":"王超"}],"doi":"10.3969/j.issn.1001-1277.2009.12.004","fpage":"14","id":"04f6b089-0ab2-4e19-9484-ef3aab270350","issue":"12","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"9b119e0e-a0cd-42c8-bc5b-e0b440fd7640","keyword":"金谷山金矿床","originalKeyword":"金谷山金矿床"},{"id":"629c67d7-f79e-4411-98dc-71180defc02d","keyword":"地球化学特征","originalKeyword":"地球化学特征"},{"id":"d81d8850-a201-4cbb-b815-838c0d20e571","keyword":"地球化学场","originalKeyword":"地球化学场"},{"id":"4c2d8d2a-fb7a-4406-993c-537133eed093","keyword":"吉林延边","originalKeyword":"吉林延边"}],"language":"zh","publisherId":"huangj200912004","title":"吉林延边金谷山金矿床地球化学特征","volume":"30","year":"2009"},{"abstractinfo":"以谷朊粉为原料,利用谷氨酰胺转氨酶(TGase)的催化作用制备再生谷朊蛋白纤维,讨论了谷朊粉用量、酶浓度、反应时间、反应温度对谷朊蛋白纤维机械性能的影响,以及温度和pH值对成型纤维水解稳定性能的影响.结果表明,当谷朊粉的用量为30%,酶用量为5U/g(谷朊蛋白),反应时间为1h,反应温度为50℃时,制备出的谷朊蛋白纤维具有较好的物理机械性能;所制备的纤维的水解稳定性随温度的升高而降低,随pH值的降低而增加,TGase的催化作用改善了纤维的水解稳定性.","authors":[{"authorName":"毛军","id":"46966283-e8a9-4e51-8697-f76b5759021c","originalAuthorName":"毛军"},{"authorName":"崔莉","id":"3440ed7d-b8be-4bb5-a07f-f53c2493adb3","originalAuthorName":"崔莉"},{"authorName":"范雪荣","id":"037c98b1-b953-4314-b13f-4a21ac62235f","originalAuthorName":"范雪荣"},{"authorName":"王平","id":"50ec5fb6-8a7a-4c5a-98b8-66493ec327be","originalAuthorName":"王平"},{"authorName":"王强","id":"8f357a0b-3f84-4d6c-9513-5446969fdf62","originalAuthorName":"王强"}],"doi":"","fpage":"39","id":"ad26ef37-7dda-4e0c-ad0d-ac74e750269f","issue":"1","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"b9d94630-7a4a-424f-ad00-36298db58175","keyword":"谷氨酰胺转氨酶","originalKeyword":"谷氨酰胺转氨酶"},{"id":"8591770e-46e6-4eaf-954a-743c6c9d48c7","keyword":"谷朊蛋白纤维","originalKeyword":"谷朊蛋白纤维"},{"id":"417c2777-ddb2-4bd9-a212-029705ac751d","keyword":"改性","originalKeyword":"改性"},{"id":"103f6837-ecbe-4716-b36e-d8dbb9d6d44b","keyword":"稳定性","originalKeyword":"稳定性"}],"language":"zh","publisherId":"gncl201301009","title":"基于谷氨酰胺转氨酶(TGase)再生谷朊蛋白纤维的制备及性质研究","volume":"44","year":"2013"},{"abstractinfo":"建立了液相色谱-串联质谱分析多种肉及肉制品中利谷隆及其代谢产物3,4-二氯苯胺残留的方法.样品用丙酮-乙腈(5∶95,v/v)提取,冷冻去脂,经弗罗里硅土固相萃取柱净化后进行液相色谱-串联质谱检测,采用内标法定量.利谷隆及3,4-二氯苯胺在1 ~ 500μg/L范围内呈良好的线性关系,相关系数(r)均大于0.998,方法的定量限(信噪比(S/N)>1 0)为10μg/kg,检出限(S/N>3)为5μg/kg.在各种肉及肉制品基质中添加低、中、高3种不同水平的利谷隆及3,4-二氯苯胺,其回收率范围分别为88.3% ~101.2%和91.6% ~101.6%,相对标准偏差(RSD)分别为4.8% ~ 13.7%和4.7%~11.8%.结果表明所建立的方法可以满足肉及肉制品中利谷隆和3,4-二氯苯胺残留量的检测需要.","authors":[{"authorName":"郭德华","id":"45c2e21e-70bc-4341-9ebc-cea9e57cccc8","originalAuthorName":"郭德华"},{"authorName":"伊雄海","id":"c1b8403a-dd51-44a2-9b58-c020bc70ad85","originalAuthorName":"伊雄海"},{"authorName":"曲栗","id":"9ea961f7-bbea-4f0c-b172-0a7333579f02","originalAuthorName":"曲栗"}],"doi":"10.3724/SP.J.1123.2011.00967","fpage":"967","id":"84174a34-9402-4e82-8e68-2f7cc4eecbd7","issue":"10","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"c045269c-0c04-41be-b3b4-7864c949c166","keyword":"液相色谱-串联质谱","originalKeyword":"液相色谱-串联质谱"},{"id":"d32d173b-c444-41d7-82f7-147774482c4b","keyword":"利谷隆","originalKeyword":"利谷隆"},{"id":"90cd810a-bade-4aab-8291-50aa1f0012fe","keyword":"3,4-二氯苯胺","originalKeyword":"3,4-二氯苯胺"},{"id":"559e034a-ab92-4872-b26a-4979012eabbe","keyword":"肉","originalKeyword":"肉"},{"id":"e135ce63-1d11-4265-83f5-76db35fc9962","keyword":"肉制品","originalKeyword":"肉制品"}],"language":"zh","publisherId":"sp201110005","title":"液相色谱-串联质谱法测定肉及肉制品中利谷隆及其代谢产物3,4-二氯苯胺残留","volume":"29","year":"2011"},{"abstractinfo":"采用廉价可生物降解的小麦谷朊蛋白为原料,经过羟甲基化和阳离子化改性合成类似聚酰胺聚胺环氧氯丙烷(PPE)的纸张增强剂. 经改性后,谷朊蛋白带有氮杂环丁烷结构、表氯醇和环氧基团3种功能基团,可与纤维形成共价键,且能发生自身交联,在纤维周围形成三维交联网络结构,提高纸张干、湿强度. 通过单因素试验,研究了甲醛、甲酸、温度、反应时间和环氧氯丙烷5种反应因素对纸张强度的影响. 优化合成条件下制备改性谷朊蛋白可使纸张干抗张强度提高35%,湿强保留率达20%. 改性后谷朊蛋白显阳离子性,加入纸浆中,可使得浆料体系Zeta电位升高,改善浆料的留着率,明显提高纸张强度. 结果表明,经羟甲基化和环氧氯丙烷加成改性的谷朊蛋白可以作为纸张的干强剂和湿强剂.","authors":[{"authorName":"尹覃伟","id":"64c33601-f85f-4091-8a14-dd1d407d1123","originalAuthorName":"尹覃伟"},{"authorName":"付时雨","id":"c9ee94ea-ddf8-4073-be2a-33a57ca317b4","originalAuthorName":"付时雨"},{"authorName":"詹怀宇","id":"75cf45f1-bbc3-49bf-9f95-ae2c58ac071f","originalAuthorName":"詹怀宇"}],"doi":"10.3969/j.issn.1000-0518.2008.01.007","fpage":"27","id":"9dee3fd7-97ea-4ee6-8c86-2a4a51143154","issue":"1","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"3c226e82-3bf4-4e67-8065-cfa9e1b468cf","keyword":"谷朊蛋白","originalKeyword":"谷朊蛋白"},{"id":"401a30c8-20fa-417e-9a22-ab830eefae9d","keyword":"羟甲基化","originalKeyword":"羟甲基化"},{"id":"8e4b1080-56f2-4f7c-b575-bd8dac6b9974","keyword":"环氧氯丙烷","originalKeyword":"环氧氯丙烷"},{"id":"288ac410-16dc-420c-88c0-497197baa6aa","keyword":"湿强剂","originalKeyword":"湿强剂"}],"language":"zh","publisherId":"yyhx200801007","title":"谷朊蛋白的改性及其作为纸张增强剂的性能","volume":"25","year":"2008"},{"abstractinfo":"涂装的质量提高和生产成本的降低,可为机电产品制造领域创造附加值,还可以增加市场竞争力,所以人们对21世纪新型涂料开发、涂装作业方式改变、劳动条件改善、涂装工艺技术装备改进、开发等等都抱有很大的期望.全世界对公害和地球暖化等问题更加关心,环保问题是涂装行业最大的问题.涂料、涂装设备、涂装应用三位一体共同合作,是21世纪达到无公害涂装要取得成效的重要一步.我国机械制造大型企业在加强科研开发力量的同时不要忽视涂装技术这一重要领域.","authors":[],"doi":"","fpage":"65","id":"b1f1f25d-8e1c-4d6a-a107-e2331ba8a316","issue":"1","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"7a805d76-ec46-4830-8ce4-7f34b9ab216d","keyword":"涂料","originalKeyword":"涂料"},{"id":"1785eda3-238e-4b47-ba14-979aa0b2c04d","keyword":"涂装","originalKeyword":"涂装"},{"id":"f9f24383-5eff-4b55-9bc6-5a9d7f83b347","keyword":"装备","originalKeyword":"装备"},{"id":"28f7663e-ee5d-466d-ae50-c1b7704b74cc","keyword":"开发","originalKeyword":"开发"},{"id":"d1c84c05-b0e8-407d-8da2-4453b33856cd","keyword":"展望","originalKeyword":"展望"}],"language":"zh","publisherId":"clbh200001021","title":"21世纪工业涂装展望","volume":"33","year":"2000"},{"abstractinfo":"结合2002年世界钛材市场的四大特点,从世界钛加工材的产量、主要生产企业的经营状况及应用领域等方面回顾了2002年的世界钛加工材市场,对2003年世界钛材市场做了分析.","authors":[{"authorName":"汪小明","id":"056b1720-45dc-4e09-af46-851cb89af8d2","originalAuthorName":"汪小明"},{"authorName":"郝斌","id":"cd0852d3-beaa-4f9d-83d7-43190739aeaf","originalAuthorName":"郝斌"}],"doi":"10.3969/j.issn.1009-9964.2003.04.020","fpage":"78","id":"a25eaed8-09af-4cbb-9ba3-1d7571f5ab67","issue":"4","journal":{"abbrevTitle":"TGYJZ","coverImgSrc":"journal/img/cover/TGYJZ.jpg","id":"60","issnPpub":"1009-9964","publisherId":"TGYJZ","title":"钛工业进展"},"keywords":[{"id":"57e248eb-e656-402e-a695-1a1890ca2691","keyword":"钛材","originalKeyword":"钛材"},{"id":"4d25609f-9313-4a72-b841-f7a6a55544cb","keyword":"市场","originalKeyword":"市场"},{"id":"241a00a6-e62d-4adf-8a67-409ac29c55d5","keyword":"动态","originalKeyword":"动态"}],"language":"zh","publisherId":"tgyjz200304020","title":"2002年世界钛材市场最新动态","volume":"20","year":"2003"}],"totalpage":2273,"totalrecord":22724}