{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"本文采用化学沉积的方法,在板状基体上成功的制备纳米晶Co-Fe-P合金涂层.运用TEM、XRD等分析手段对[Fe2+]对Co-Fe-P合金成分、结构、性能的影响进行分析研究.结果表明合适工艺参数的调整选择,可获得表面光亮致密与基体结合良好的纳米晶Co-Fe-P化学沉积膜,且所得纳米晶Co-Fe-P合金具有较低的矫顽力和较高的矩形比,可以用作软磁材料.","authors":[{"authorName":"马杰","id":"0b19cb36-02bf-43b7-bfef-f3de16694847","originalAuthorName":"马杰"},{"authorName":"吴玉程","id":"8ddf8a1c-84df-4143-b206-438818f629b4","originalAuthorName":"吴玉程"},{"authorName":"张勇","id":"23304850-45d9-4fd8-b270-4bb898156012","originalAuthorName":"张勇"},{"authorName":"王文芳","id":"81c66c28-fb22-4ddb-baff-71665825c22a","originalAuthorName":"王文芳"},{"authorName":"乔祎","id":"68216b24-0528-4b05-8973-241777f8e5c4","originalAuthorName":"乔祎"},{"authorName":"郑玉春","id":"3ce43753-2ce1-493c-b6b5-5bff1facf062","originalAuthorName":"郑玉春"},{"authorName":"刘玉","id":"023f5d02-cab5-44c8-81cc-6cb27a000d97","originalAuthorName":"刘玉"},{"authorName":"黄新民","id":"ec36a882-c8b1-4695-95dd-dc479e1277e3","originalAuthorName":"黄新民"},{"authorName":"李广海","id":"20595ff9-e76c-4ff2-b668-8606a425e7bf","originalAuthorName":"李广海"},{"authorName":"张立德","id":"711edbb5-a18d-4b23-89ce-c2c03f77ee04","originalAuthorName":"张立德"}],"doi":"10.3969/j.issn.1005-8192.2004.01.002","fpage":"4","id":"bb1c058f-947e-4f2e-9bd1-ab25f3edd785","issue":"1","journal":{"abbrevTitle":"JSGNCL","coverImgSrc":"journal/img/cover/JSGNCL.jpg","id":"46","issnPpub":"1005-8192","publisherId":"JSGNCL","title":"金属功能材料"},"keywords":[{"id":"c30122fc-9c79-4686-a2d8-2e688e649729","keyword":"化学沉积","originalKeyword":"化学沉积"},{"id":"ad88b5f2-8656-45d3-a046-cf5af5f61839","keyword":"Co-Fe-P合金","originalKeyword":"Co-Fe-P合金"},{"id":"c9572fe1-541e-4ab0-a437-cb6fc2689ab9","keyword":"纳米晶","originalKeyword":"纳米晶"},{"id":"bcc5e7ba-0180-44f5-ba8a-6fc7238d530f","keyword":"组织结构","originalKeyword":"组织结构"},{"id":"a444332b-4351-4dfb-87f1-344c95fcadd7","keyword":"磁学性能","originalKeyword":"磁学性能"}],"language":"zh","publisherId":"jsgncl200401002","title":"化学沉积Co-Fe-P纳米涂层结构与磁学性能研究","volume":"11","year":"2004"},{"abstractinfo":"化学沉积是制备纳米材料的一种良好方法,通过控制溶液组份和操作条件可以获得不同尺度的纳米晶.在化学沉积钴硼、钴磷合金纳米晶涂层制备工艺的基础上,制备了钴镍硼、钴镍磷纳米晶合金涂层,研究了三元纳米晶合金的沉积速率和显微组织结构.结果表明:当CCo2+/CNi2+=3:2时,pH值7.2,温度80℃,负载因子0.4 dm2/L,可以获得钴镍硼合金纳米晶.以纳米晶钴磷合金沉积液为基本配方,CCo2+/(CCo2+CNi2+)保持在0.1~0.5之间变化,可获得较好的纳米晶钴镍磷合金沉积层.","authors":[{"authorName":"吴玉程","id":"0fe56625-1013-4ee3-bf0a-b81498e4af8e","originalAuthorName":"吴玉程"},{"authorName":"舒霞","id":"875dcc91-62d6-4315-b95b-9405aae82f39","originalAuthorName":"舒霞"},{"authorName":"张勇","id":"37bad7ed-6388-43c5-9e4e-1e3a7734e74d","originalAuthorName":"张勇"},{"authorName":"郑玉春","id":"afb8cd40-702c-4e75-adfb-958b6ae31eac","originalAuthorName":"郑玉春"},{"authorName":"王文芳","id":"29f99d95-7ba2-4b8a-ae20-23ceb4c1e9fa","originalAuthorName":"王文芳"},{"authorName":"黄新民","id":"9cba4552-f9ca-459f-ac84-edeab61ae6bd","originalAuthorName":"黄新民"},{"authorName":"李广海","id":"a7c01bf4-708e-4c3b-a244-4207bf8fff1d","originalAuthorName":"李广海"},{"authorName":"张立德","id":"1d9873a0-32cc-443d-bf2c-76b04b115b6e","originalAuthorName":"张立德"}],"doi":"10.3969/j.issn.1001-1560.2004.01.014","fpage":"38","id":"609a6dac-bef2-45bc-8ec7-4f429c5019fb","issue":"1","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"b79af913-46ee-4346-bd97-9512d0a208ef","keyword":"钴镍硼合金","originalKeyword":"钴镍硼合金"},{"id":"8cb81077-1e47-43d4-9343-b18737d36f58","keyword":"钴镍磷合金","originalKeyword":"钴镍磷合金"},{"id":"7583e84d-d9eb-4858-ba4a-ea4b7fe08a17","keyword":"化学沉积","originalKeyword":"化学沉积"},{"id":"b3056334-6876-425f-b61b-0a1a0ba3b77f","keyword":"纳米晶","originalKeyword":"纳米晶"},{"id":"3f64409d-aa9c-4ec9-9746-c014e8c9247f","keyword":"合金涂层","originalKeyword":"合金涂层"}],"language":"zh","publisherId":"clbh200401014","title":"化学沉积钴基纳米晶合金涂层工艺","volume":"37","year":"2004"},{"abstractinfo":"通过对合金成分的优化设计,对冶金、铸造、热处理工艺的试验研究,对合金力学性能、组织结构及冲击腐蚀磨损试验等,获得了适合于冶金矿山湿式磨机衬板使用的新型合金.装机试验结果表明,用该合金制作的球磨机衬板在冶金矿山湿式磨机中的使用寿命可以达到高锰钢的2倍以上,其性能明显优于现有各种合金衬板.","authors":[{"authorName":"李先芬","id":"56e94524-a31c-4c8b-8076-0f026bce50ba","originalAuthorName":"李先芬"},{"authorName":"丁厚福","id":"1198fdac-07b3-4860-9824-6f4354daca8d","originalAuthorName":"丁厚福"},{"authorName":"卢书媛","id":"3a3f81bc-8094-4f6b-bfa4-821a5cca2323","originalAuthorName":"卢书媛"},{"authorName":"陈翌庆","id":"84931d59-452d-4052-9ad0-48460052d6dd","originalAuthorName":"陈翌庆"},{"authorName":"黄新民","id":"29c3022a-bb35-478e-848d-2519d7a9b89b","originalAuthorName":"黄新民"},{"authorName":"祖方遒","id":"d4ec27c7-24f9-4bf3-a819-55ca78682769","originalAuthorName":"祖方遒"},{"authorName":"郑玉春","id":"856468ca-dc89-44d2-8bbd-11d157e86df1","originalAuthorName":"郑玉春"},{"authorName":"程和法","id":"ed0354ba-cbc5-4429-8b1e-1ee486463b6a","originalAuthorName":"程和法"}],"doi":"10.3969/j.issn.1009-6264.2003.03.014","fpage":"61","id":"6bd2ece5-4938-4b03-9813-abfc7594bd1f","issue":"3","journal":{"abbrevTitle":"CLRCLXB","coverImgSrc":"journal/img/cover/CLRCLXB.jpg","id":"15","issnPpub":"1009-6264","publisherId":"CLRCLXB","title":"材料热处理学报"},"keywords":[{"id":"d0aec22e-940a-47e6-b830-3bd0847803ae","keyword":"湿式磨机衬板","originalKeyword":"湿式磨机衬板"},{"id":"57fffd46-5a3b-4226-a7ce-7737418ab8fd","keyword":"使用寿命","originalKeyword":"使用寿命"},{"id":"5322c2f4-df02-4da1-86b9-f3c40c8e23dd","keyword":"合金设计","originalKeyword":"合金设计"},{"id":"53ffc9a6-56ec-4b6d-98a9-c15903134394","keyword":"冲击腐蚀磨损","originalKeyword":"冲击腐蚀磨损"}],"language":"zh","publisherId":"jsrclxb200303014","title":"湿式磨机衬板新合金的研究和应用","volume":"24","year":"2003"},{"abstractinfo":"采用电沉积制备Ni-W合金纳米晶镀层,研究了纳米晶的形成与镀层组织结构和硬度.随着镀液组分的变化,镀层的表面形貌发生变化;X射线衍射结果表明,Ni-W合金的晶粒尺寸在17~30nm之间;镀液组成、pH值、电流密度、温度等因素对Ni-W合金纳米晶沉积层的硬度都有影响,最主要的影响因素是pH值及电流密度.","authors":[{"authorName":"吴玉程","id":"3ae2e76d-435a-419f-ae9d-4e4c7ece0070","originalAuthorName":"吴玉程"},{"authorName":"陈文辉","id":"a2439d96-d3cb-40e4-9ff0-8da25b837c9c","originalAuthorName":"陈文辉"},{"authorName":"舒霞","id":"b32f661a-8ebd-4add-b1cf-c9593c0d605e","originalAuthorName":"舒霞"},{"authorName":"王文芳","id":"9ebda3d5-f641-43ae-9180-13fb0cb1417c","originalAuthorName":"王文芳"},{"authorName":"郑玉春","id":"742365a2-c447-4d9c-87db-0651e2bc9f35","originalAuthorName":"郑玉春"},{"authorName":"张春晓","id":"d140ced8-4c7f-4a92-b5b6-a69253d97cca","originalAuthorName":"张春晓"},{"authorName":"杜燕君","id":"0a50f9bc-995e-496e-a5a3-70f321951f61","originalAuthorName":"杜燕君"}],"doi":"10.3969/j.issn.1005-8192.2005.02.006","fpage":"21","id":"018369e2-5259-497f-876e-fca5403286c7","issue":"2","journal":{"abbrevTitle":"JSGNCL","coverImgSrc":"journal/img/cover/JSGNCL.jpg","id":"46","issnPpub":"1005-8192","publisherId":"JSGNCL","title":"金属功能材料"},"keywords":[{"id":"8e04ae08-dd90-4bd2-bfd2-8b1dc498d284","keyword":"电化学沉积","originalKeyword":"电化学沉积"},{"id":"0a13bc22-0491-4da9-8b43-6ba4caab6246","keyword":"Ni-W合金纳米晶","originalKeyword":"Ni-W合金纳米晶"},{"id":"c5c37943-0ab2-4e04-af91-cd8a8e0fd4f0","keyword":"组织","originalKeyword":"组织"},{"id":"de4f1c03-6765-483a-a9f0-61e9a9e79808","keyword":"显微硬度","originalKeyword":"显微硬度"}],"language":"zh","publisherId":"jsgncl200502006","title":"电化学沉积Ni-W合金纳米晶镀层的组织与硬度研究","volume":"12","year":"2005"},{"abstractinfo":"化学沉积可得到均匀、致密的纳米晶薄膜,是一种较为理想的纳米晶制备方法.采用正交实验优化了化学沉积纳米晶钴磷合金的工艺配方,研究了正交实验5因素如硫酸钴、柠檬酸三钠、硼酸、次磷酸钠和温度及负载因子、沉积时间对沉积速度的影响.研究获得的优化工艺配方和参数为:0.06~0.12 mol/L CoSO4·7H2O,0.40~0.55 mol/L NaH2PO2·H2O,0.15~0.3 mol/L Na3C6H5O7·2H2O,0.3~0.6 mol/L H3BO3,50~80 ℃,负载因子0.4~0.8 dm2/L.","authors":[{"authorName":"舒霞","id":"f7afc772-7570-4ef0-a372-e7bea6399b28","originalAuthorName":"舒霞"},{"authorName":"吴玉程","id":"e8315501-b975-48ce-ac2a-19ce75ec5da4","originalAuthorName":"吴玉程"},{"authorName":"张勇","id":"64a3caa0-f943-4aa8-81e0-e332d0579024","originalAuthorName":"张勇"},{"authorName":"郑玉春","id":"d3580162-ea9f-484f-84bb-320dc3e24de4","originalAuthorName":"郑玉春"},{"authorName":"王文芳","id":"d6c5b894-2fc1-453f-82e5-4b2d912b09d6","originalAuthorName":"王文芳"},{"authorName":"黄新民","id":"0ee838da-31cd-48d1-a697-ce75c9373c28","originalAuthorName":"黄新民"},{"authorName":"李广海","id":"6c869034-0936-42f0-8d7e-54c0a6dab5fe","originalAuthorName":"李广海"}],"doi":"10.3969/j.issn.1004-227X.2004.05.001","fpage":"1","id":"53214315-eb51-4ed9-a19a-bf2cec9ab33b","issue":"5","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰 "},"keywords":[{"id":"7f3a5c75-abdc-40d9-9a1b-ae1c46f05d1d","keyword":"钴磷合金","originalKeyword":"钴磷合金"},{"id":"6e644590-03db-48cb-a163-96046e537875","keyword":"化学沉积","originalKeyword":"化学沉积"},{"id":"36a7dc04-8c65-4f0a-9eae-bfe17f80809b","keyword":"纳米晶","originalKeyword":"纳米晶"},{"id":"250fe6f6-7ca2-49d9-9848-d0c5957dc32d","keyword":"沉积速率","originalKeyword":"沉积速率"}],"language":"zh","publisherId":"ddyts200405001","title":"化学沉积纳米晶Co-P合金及其沉积速率影响因素的研究","volume":"23","year":"2004"},{"abstractinfo":"选择对Ni-W合金电沉积影响较大的钨酸钠浓度、电流密度、镀液pH值、温度等4个工艺参数进行对比实验,探索了各因素对沉积速率、显微硬度、镀层外观的影响,为制备Ni-W合金纳米晶提供依据,同时制备出了晶粒尺寸为10.09nm的Ni-W合金纳米晶镀层.","authors":[{"authorName":"舒霞","id":"8d1281fe-0107-440b-97db-3cfe7e4c3518","originalAuthorName":"舒霞"},{"authorName":"吴玉程","id":"2b5d520f-2c81-41a9-9a8f-925e092d0c28","originalAuthorName":"吴玉程"},{"authorName":"郑玉春","id":"b6e03115-7857-4d69-a09b-336326deec76","originalAuthorName":"郑玉春"},{"authorName":"王文芳","id":"ff8ecc9a-03dc-403e-aeee-32f71ade3638","originalAuthorName":"王文芳"},{"authorName":"张勇","id":"ffacde39-13c7-4f4e-8fcc-9f9a20443a29","originalAuthorName":"张勇"},{"authorName":"李广海","id":"3ec4e8e7-2d61-4982-b90f-a1e9a42d629b","originalAuthorName":"李广海"},{"authorName":"张立德","id":"02eee9a5-e837-473a-820b-5894e9804f2c","originalAuthorName":"张立德"}],"doi":"","fpage":"413","id":"a6363fab-df86-417e-bd35-ea0ee1237d23","issue":"3","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"75f9a163-be2c-4366-94dc-0671a185f5ec","keyword":"Ni-W合金","originalKeyword":"Ni-W合金"},{"id":"20b40e26-f577-403a-b9ab-1544ccb05ad8","keyword":"电沉积","originalKeyword":"电沉积"},{"id":"21f26268-d930-4dbd-ad5f-c5b1be83aac7","keyword":"纳米晶","originalKeyword":"纳米晶"}],"language":"zh","publisherId":"xyjsclygc200503019","title":"工艺条件对电沉积Ni-W合金纳米晶的影响","volume":"34","year":"2005"},{"abstractinfo":"在镀液中添加铁氧体粒子制备Ni-Fe基磁性复合镀层是电沉积技术一个新的发展方向,目前相关研究不多。采用电沉积法在铜片上制备了Ni—Fe—NiFe2O4复合镀层,用电化学方法、金相显微镜及能谱仪研究了镀液中NiFe2O4含量、电流密度、表面活性剂十六烷基三甲基溴化铵(CTAB)等对复合镀层性能的影响。结果表明:复合镀层硬度随镀液中NiFe2O4含量的增加先增大后减小,含量为15g/L时镀层硬度达370HV,耐蚀性最好;随电流密度增大,沉积速率加快,镀层显微硬度增加,耐蚀性略有提高;加入CTAB能提高镀层中微粒的复合量,可在较低的电流密度下获得孔隙小、致密度高的镀层,显微硬度也有所提高,但耐蚀性略有下降;在温度为60℃,镀液中NiFe2O4含量为15g/L,电流密度为5A/dm2,CTAB含量为0.1%(质量分数)时,可获得性能较好的复合镀层,镀层中NiFe2O4含量较高,均匀致密,微观表面粗糙,无裂纹,与基体结合良好。","authors":[{"authorName":"李燕","id":"1c9f1d33-aa62-47bd-933b-a868db41b619","originalAuthorName":"李燕"},{"authorName":"舒霞","id":"4b38a668-ce03-459b-b539-ef6d13937dae","originalAuthorName":"舒霞"},{"authorName":"黄新民","id":"2980198a-4140-4cd0-9a18-6464dcd4317c","originalAuthorName":"黄新民"},{"authorName":"郑玉春","id":"e971c7b6-78c9-47b7-ba32-d800fc68a414","originalAuthorName":"郑玉春"},{"authorName":"吴玉程","id":"95eb63bb-949f-49f4-aeef-66a2a45999e9","originalAuthorName":"吴玉程"}],"doi":"","fpage":"33","id":"093619d5-2c15-429e-badb-b26c6d4110ca","issue":"8","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"eb321843-1eee-4c3b-b35b-75215b096307","keyword":"复合电沉积","originalKeyword":"复合电沉积"},{"id":"dfe3f222-9469-4229-9e95-cdbfbe482a23","keyword":"Ni-Fe-NiFe2O4沉积层","originalKeyword":"Ni-Fe-NiFe2O4沉积层"},{"id":"d4f8f023-f8cb-49d9-a245-215a49294a12","keyword":"耐蚀性","originalKeyword":"耐蚀性"},{"id":"aa16dcf1-b6b3-45a0-9382-42e02fe3ca9b","keyword":"显微硬度","originalKeyword":"显微硬度"},{"id":"8d8b2f84-ad23-456c-b0db-829a1f7d6fcd","keyword":"结合力","originalKeyword":"结合力"}],"language":"zh","publisherId":"clbh201208013","title":"Ni-Fe-NiFe2O4电沉积层的制备及其性能","volume":"45","year":"2012"},{"abstractinfo":"利用差示扫描量热(DSC)、透射电镜(TEM)和X射线衍射(XRD)技术对快速凝固Al91Ni7Y2合金条带急冷态和不同温度退火态的晶化行为及显微结构演化进行了研究.结果表明:急冷态的A191Ni7Y2合金为部分Al粒子均匀分布在非晶基底上的复合材料.从急冷态到高温平衡态有三阶段晶化过程,对所有的晶化温度和晶化相的测量表明,DSC曲线上第一个峰的初始和峰值温度分别为240C和267 C(在加热速率为10C/min条件下),这一相对高的温度表明此复合材料有高的热稳定性.","authors":[{"authorName":"苏勇","id":"11d00bd7-0476-487f-b9d2-7dbf0f913715","originalAuthorName":"苏勇"},{"authorName":"陈翌庆","id":"87343932-bc9f-42c5-9464-cc6fc294ef0e","originalAuthorName":"陈翌庆"},{"authorName":"丁厚福","id":"40a6e097-a449-458e-b38b-6d17c3a3499c","originalAuthorName":"丁厚福"},{"authorName":"郑玉春","id":"b4996134-186c-4aa4-aa2e-4c548d87bcaa","originalAuthorName":"郑玉春"}],"doi":"10.3969/j.issn.1004-244X.2000.04.003","fpage":"12","id":"15fc9128-8a4f-47fe-ad99-31a079588f68","issue":"4","journal":{"abbrevTitle":"BQCLKXYGC","coverImgSrc":"journal/img/cover/BQCLKXYGC.jpg","id":"4","issnPpub":"1004-244X","publisherId":"BQCLKXYGC","title":"兵器材料科学与工程 "},"keywords":[{"id":"3889fc84-1988-44fe-8d95-a37c14e9e07a","keyword":"纳米非晶复合材料","originalKeyword":"纳米非晶复合材料"},{"id":"9188af20-9e20-4c4f-807f-97d2c9f66e7e","keyword":"Al-Ni-Y合金","originalKeyword":"Al-Ni-Y合金"},{"id":"e20bae83-6f33-4941-8909-7b629cea2622","keyword":"晶化","originalKeyword":"晶化"},{"id":"0c99d944-e8bf-478c-b4a1-e61f7930aae3","keyword":"快速凝固","originalKeyword":"快速凝固"}],"language":"zh","publisherId":"bqclkxygc200004003","title":"Al 91Ni 7Y2纳米非晶复合材料晶化的研究","volume":"23","year":"2000"},{"abstractinfo":"采用单辊旋铸法制备Al-8Fe-4Ce(质量分数)合金薄带,利用透射电镜、能谱分析技术研究了该合金的急冷态和退火态组织,测定了合金在不同温度下退火后的显微硬度.急冷合金组织随冷速的不同而不同;300℃退火态组织无明显变化;400℃退火2 h 后,晶界弥散相开始长大、聚集,但初生相变化甚微;450℃退火2 h 后,初生相和晶间弥散相(分别为亚稳相 Al6Fe 和亚稳相 Al20Fe5Ce相)均进一步粗化.通过显微硬度测定可间接确定该合金的软化温度在 300℃以上.","authors":[{"authorName":"陈翌庆","id":"2e20f86b-5f64-4902-a6c9-17a750e75175","originalAuthorName":"陈翌庆"},{"authorName":"苏勇","id":"48665c63-cfd9-4ef2-83dd-41909d358310","originalAuthorName":"苏勇"},{"authorName":"丁厚福","id":"67a50f29-e9a2-48bc-8530-925104e98502","originalAuthorName":"丁厚福"},{"authorName":"郑玉春","id":"affd1c90-79aa-4d38-9523-667f1d3b2d78","originalAuthorName":"郑玉春"}],"doi":"10.3969/j.issn.0258-7076.2000.05.001","fpage":"321","id":"2f0879dd-0b5e-407c-82e9-c3c8446e3ced","issue":"5","journal":{"abbrevTitle":"XYJS","coverImgSrc":"journal/img/cover/XYJS.jpg","id":"67","issnPpub":"0258-7076","publisherId":"XYJS","title":"稀有金属"},"keywords":[{"id":"98213b96-eaaf-4f07-af50-56bef1e59dda","keyword":"快速凝固","originalKeyword":"快速凝固"},{"id":"7ce480dd-fc6e-43d8-bc52-70985d4cec2f","keyword":"Al-Fe-Ce 合金","originalKeyword":"Al-Fe-Ce 合金"},{"id":"821b3466-170d-41e8-b8b4-538afa159ac5","keyword":"显微组织","originalKeyword":"显微组织"},{"id":"b188a52b-9dda-4f62-ad3a-23a26cd8f9f6","keyword":"退火态组织","originalKeyword":"退火态组织"},{"id":"7c5b8018-71bb-43c2-8ef3-45d88cca1784","keyword":"显微硬度","originalKeyword":"显微硬度"}],"language":"zh","publisherId":"xyjs200005001","title":"快速凝固Al-Fe-Ce合金显微组织及热稳定性的研究","volume":"24","year":"2000"},{"abstractinfo":"目前,常规紫铜无铬转化液主要由苯骈三氮唑(BTA)、配位剂和表面活性剂组成,所得转化膜的耐蚀性较差。在常规无铬转化液中加入钼酸钠和硝酸镧,并确定了一种环保型紫铜表面无铬成膜工艺:12g/L BTA,8g/LNa2MoO4,4g/LLa(NO3)3·6H2O,10g/LC6H807,4g/LC7H606S·2H2O,温度50℃,时间5min。通过中性盐雾试验测试了所得转化膜的耐蚀性;采用极化曲线和交流阻抗谱分析了转化膜在1mol/LHCl中的电化学行为,同时用场发射扫描电镜(FESEM)观察了转化膜的表面形貌。结果表明:本工艺无铬、环保,可在紫铜表面形成完整、致密的转化膜,缓蚀率达98.8%,耐蚀性优于铬酸盐钝化膜和常规无铬钝化膜。","authors":[{"authorName":"郑伟","id":"897cf914-7be6-4a69-9eae-38bbd3982669","originalAuthorName":"郑伟"},{"authorName":"吴玉程","id":"43c1110d-a53b-4585-a057-5fe4ed5d2db7","originalAuthorName":"吴玉程"},{"authorName":"刘万青","id":"b77140e1-3d0e-4a91-b480-867ef2f9893a","originalAuthorName":"刘万青"},{"authorName":"舒霞","id":"0b2e91b1-6f87-4f0d-bdd6-3535fe8bd0e4","originalAuthorName":"舒霞"},{"authorName":"郑玉春","id":"127b566f-c8aa-4186-a572-598dfb7521a5","originalAuthorName":"郑玉春"},{"authorName":"黄新民","id":"5a4fa613-b011-48ed-b2b5-3bd20d578d3d","originalAuthorName":"黄新民"}],"doi":"","fpage":"1","id":"3c46d91d-1e7e-4af3-b3b7-6d0442a22600","issue":"6","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"db7a47f3-4eeb-4ac9-82ae-18940d72475a","keyword":"无铬转化膜","originalKeyword":"无铬转化膜"},{"id":"ac31bb88-6564-4250-9aaf-b253a4388976","keyword":"BTA","originalKeyword":"BTA"},{"id":"86bae38d-e006-4d77-9cf0-bf29fef185b0","keyword":"钼酸钠","originalKeyword":"钼酸钠"},{"id":"2f6a903a-82a7-46b3-b9f2-87b57fe53313","keyword":"硝酸镧","originalKeyword":"硝酸镧"},{"id":"b10e0c66-7a40-45b8-8fb0-46d77a7aaa90","keyword":"紫铜","originalKeyword":"紫铜"},{"id":"f2307334-d3ef-4b82-bd15-2adbd1e66f87","keyword":"电化学行为","originalKeyword":"电化学行为"},{"id":"62f47f17-0b42-496d-9c2f-c775a5905469","keyword":"表面形貌","originalKeyword":"表面形貌"},{"id":"001700c7-8a5e-4517-a334-85db26566d61","keyword":"耐蚀性","originalKeyword":"耐蚀性"}],"language":"zh","publisherId":"clbh201206002","title":"紫铜表面新型无铬转化膜的耐蚀性能","volume":"45","year":"2012"}],"totalpage":10,"totalrecord":96}