{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"钙、镁、锰是稀土硅铁及镁硅铁合金产品中重要的指标,采用全谱直读等离子光谱法测定稀土硅铁及镁硅铁合金中的钙、镁、锰量,无须基底匹配,采用工作曲线法对多个元素同时测定,结果稳定可靠.相对标准偏差(RSD)小于2.63％,与其他分析方法相对照,测定结果较为吻合.测定范围:Ca:0.50％～6.00％,Mg:0.20％～11.00％,Mn:0.20％ ～4.00％.","authors":[{"authorName":"<span style=\"color:red\">金</span><span style=\"color:red\">斯琴高娃</span>","id":"c339b7b2-4dfa-4c98-a6ca-a9dc701e7736","originalAuthorName":"金斯琴高娃"},{"authorName":"郝茜","id":"81b159f6-bc94-4fe3-982f-df323ac1a605","originalAuthorName":"郝茜"},{"authorName":"李玉梅","id":"7f550760-02b4-4661-8bca-f89fac7e3e6e","originalAuthorName":"李玉梅"},{"authorName":"刘晓杰","id":"3b4ce807-4045-4d1f-8c6a-9de11e156494","originalAuthorName":"刘晓杰"}],"doi":"","fpage":"70","id":"822fc707-79a5-43d0-9c2d-d78f0b389de7","issue":"4","journal":{"abbrevTitle":"XT","coverImgSrc":"journal/img/cover/XT.jpg","id":"65","issnPpub":"1004-0277","publisherId":"XT","title":"稀土"},"keywords":[{"id":"32c967c7-2bba-4333-93d5-8e71e72fc34f","keyword":"稀土硅铁合金及镁硅铁合金","originalKeyword":"稀土硅铁合金及镁硅铁合金"},{"id":"77133762-83a1-4441-83be-d8b4dac94cbb","keyword":"ICP-AES法","originalKeyword":"ICP-AES法"},{"id":"4b9498e3-f96e-4daa-a2c8-dc3a4f96cc7c","keyword":"钙、镁、锰量","originalKeyword":"钙、镁、锰量"}],"language":"zh","publisherId":"xitu201304015","title":"稀土硅铁合金及镁硅铁合金中钙、镁、锰量的分析方法——ICP-AES法","volume":"34","year":"2013"},{"abstractinfo":"研究了以盐酸浸取氟化稀土中硼的浸取条件,考察了浸取酸的用量、浸取的温度及时间、浸取时加入甘露醇的作用以及氟的残留量对实验结果的影响,测定了试样颗粒度对实验结果的影响.确定的实验方案准确可靠,操作简单,重现性好.测定范围:0.005%～2%.","authors":[{"authorName":"崔爱端","id":"a59e76bc-2e50-4e15-b579-c476bde9cc32","originalAuthorName":"崔爱端"},{"authorName":"<span style=\"color:red\">金</span><span style=\"color:red\">斯琴高娃</span>","id":"3a08b4a0-19e4-4ae9-9c15-754473078111","originalAuthorName":"金斯琴高娃"}],"doi":"10.3969/j.issn.1004-0277.2011.01.016","fpage":"72","id":"bee69fe8-2d57-4495-bdba-9240218e691e","issue":"1","journal":{"abbrevTitle":"XT","coverImgSrc":"journal/img/cover/XT.jpg","id":"65","issnPpub":"1004-0277","publisherId":"XT","title":"稀土"},"keywords":[{"id":"1c509356-a5a7-4d79-a4c0-5821dd92744c","keyword":"氟化稀土","originalKeyword":"氟化稀土"},{"id":"3123c0b5-67cf-405e-a0ba-030b76c9b38a","keyword":"硼","originalKeyword":"硼"}],"language":"zh","publisherId":"xitu201101016","title":"ICP-AES法测定氟化稀土中的硼量","volume":"32","year":"2011"},{"abstractinfo":"建立了电感耦合等离子体发射光谱法(ICP-AES)测定稀土矿石中氧化铌、氧化锆、氧化钛的定量分析方法.样品使用氢氧化钠、过氧化钠溶解后,经过强碱分离磷、硅、氟、铝等元素及大量的钠盐,沉淀用盐酸和氢氟酸溶解,于ICP-AES法测定铌、锆、钛量.本方法对影响测定的各种因素进行了详细的研究,包括溶解样品条件、共存元素干扰、回收率试验等.实验根据稀土矿石的特点确定了各元素的测定范围,测定范围为:Nb2O50.07％ ～0.20％;ZrO21％～5％;TiO20.1％～4％,测定结果与ICP-MS法测定相一致.精密度试验结果表明,RSD(n=11)均小于2.80.","authors":[{"authorName":"<span style=\"color:red\">金</span><span style=\"color:red\">斯琴高娃</span>","id":"19cf9e51-a13d-4300-9d05-fb646ae4663d","originalAuthorName":"金斯琴高娃"},{"authorName":"高立红","id":"08aacc8e-7602-4fdf-969b-18e2f1646b2f","originalAuthorName":"高立红"},{"authorName":"张秀艳","id":"5eb535c5-dc91-465b-8179-7a016f8aea05","originalAuthorName":"张秀艳"},{"authorName":"张翼明","id":"fcf8213a-0609-4b75-8a9d-3ac5e5705fd1","originalAuthorName":"张翼明"},{"authorName":"张弘强","id":"1ae54fbe-7d81-41b9-bd07-f0c173862936","originalAuthorName":"张弘强"}],"doi":"10.16533/J.CNKI.15-1099/TF.201602019","fpage":"113","id":"766bc279-4174-487e-9ed0-3c5c48a0f449","issue":"2","journal":{"abbrevTitle":"XT","coverImgSrc":"journal/img/cover/XT.jpg","id":"65","issnPpub":"1004-0277","publisherId":"XT","title":"稀土"},"keywords":[{"id":"a5223286-ce6d-4097-af64-01004253fb50","keyword":"电感耦合等离子体发射光谱法","originalKeyword":"电感耦合等离子体发射光谱法"},{"id":"77cd1c90-de1c-4eb1-bc2f-da95814500da","keyword":"稀土矿石","originalKeyword":"稀土矿石"},{"id":"7d9c0ddc-9931-4d0c-ab9b-b0ada9ac439c","keyword":"氧化铌","originalKeyword":"氧化铌"},{"id":"b39521b6-c6a5-4cff-b514-dc027e607f4a","keyword":"氧化锆","originalKeyword":"氧化锆"},{"id":"e7fa466d-8b44-44f4-bd45-8557d09a03fe","keyword":"氧化钛","originalKeyword":"氧化钛"}],"language":"zh","publisherId":"xitu201602019","title":"电感耦合等离子体发射光谱法测定稀土矿石中氧化铌、氧化锆、氧化钛量","volume":"37","year":"2016"},{"abstractinfo":"采用等离子光谱法测定碳酸稀土、氯化稀土中氧化铕含量,系统考察了不同试样浓度、不同基体配分下共存元素对测定元素的影响,并进行了加料回收及精密度实验,结果稳定可靠,与ICP-MS的对照结果令人满意.测定范围0.01%～0.30%.","authors":[{"authorName":"<span style=\"color:red\">金</span><span style=\"color:red\">斯琴高娃</span>","id":"347ec280-471f-41a0-a7ab-4ade4e5b2745","originalAuthorName":"金斯琴高娃"},{"authorName":"崔爱端","id":"8e7634e4-d551-4931-8734-bb50b2d0a292","originalAuthorName":"崔爱端"},{"authorName":"李玉梅","id":"33062fe7-4ff7-42f4-9257-328413316c03","originalAuthorName":"李玉梅"}],"doi":"10.3969/j.issn.1004-0277.2010.01.018","fpage":"80","id":"b95c2d62-521c-411b-9796-e356932c36f7","issue":"1","journal":{"abbrevTitle":"XT","coverImgSrc":"journal/img/cover/XT.jpg","id":"65","issnPpub":"1004-0277","publisherId":"XT","title":"稀土"},"keywords":[{"id":"353dbe56-f4bc-4527-81ee-982618dcd80c","keyword":"碳酸稀土","originalKeyword":"碳酸稀土"},{"id":"99cdf9e9-30af-4d6e-a5d0-adc6cc2df9a5","keyword":"氯化稀土","originalKeyword":"氯化稀土"},{"id":"3756cda1-4216-4814-ac30-48586be00de7","keyword":"氧化铕","originalKeyword":"氧化铕"}],"language":"zh","publisherId":"xitu201001018","title":"ICP-AES法测定碳酸稀土、氯化稀土中氧化铕量","volume":"31","year":"2010"},{"abstractinfo":"采用电感耦合等离子体原子发射光谱法( ICP - AES)测定镝铁合金中非稀土杂质.并用基体匹配法及氟化分离法以消除干扰.测定范围为AI、Si:0.020％～0.10％；Ca,,Mg,Ni:0.0050％～0.050％；Mo,W:0.030％～0.20％.对样品测定11次,得到相对标准偏差为0.75％～4.95％,加标回收率为97.5％～104％.方法可用于镝铁合金中非稀土杂质的测定.","authors":[{"authorName":"<span style=\"color:red\">金</span><span style=\"color:red\">斯琴高娃</span>","id":"a96d16a7-98ef-4c3f-993d-3fdd0033c049","originalAuthorName":"金斯琴高娃"},{"authorName":"张弘强","id":"634b9000-be30-4369-ac19-0be0d193c7a8","originalAuthorName":"张弘强"},{"authorName":"蒋彩霞","id":"8ca4a8f3-16cf-454d-982b-d87ba1d2995f","originalAuthorName":"蒋彩霞"}],"doi":"10.3969/j.issn.1004-0277.2011.06.018","fpage":"85","id":"c5287218-53e4-49a2-8311-7c6d3c00398b","issue":"6","journal":{"abbrevTitle":"XT","coverImgSrc":"journal/img/cover/XT.jpg","id":"65","issnPpub":"1004-0277","publisherId":"XT","title":"稀土"},"keywords":[{"id":"0580be10-0556-47fb-ba76-10cd7f69cbe3","keyword":"镝铁合金","originalKeyword":"镝铁合金"},{"id":"758fef54-bab3-44e8-a264-6b99fed1cca6","keyword":"非稀土杂质","originalKeyword":"非稀土杂质"},{"id":"cb5972e7-9aa1-446d-a13d-ebeb86dfa00e","keyword":"ICP - AES法","originalKeyword":"ICP - AES法"}],"language":"zh","publisherId":"xitu201106018","title":"电感耦合等离子体发射光谱法测定镝铁合金中非稀土杂质","volume":"32","year":"2011"},{"abstractinfo":"综述了<span style=\"color:red\">金</span>的分离和富集方法,主要包括各种吸附和萃取方法.采用活性炭和泡沫塑料(简称泡塑)吸附分离<span style=\"color:red\">金</span>是传统的分离富集法,有负载活性炭和有负载泡塑可以提高富集<span style=\"color:red\">金</span>的能力.近些年,离子交换树脂和离子交换纤维素在分离富集<span style=\"color:red\">金</span>的应用中,占有相当大的比例.萃取法除了使用传统的MIBK作为萃取剂,又见报道硫醚、亚砜、醇类等作为萃取剂的各种萃取体系.文中引用参考文献107篇.","authors":[{"authorName":"冯月斌","id":"abd62fc7-3872-4461-8d32-6c90e9372e43","originalAuthorName":"冯月斌"},{"authorName":"张锦柱","id":"0bce5201-7889-4749-8883-5693ec2ee81e","originalAuthorName":"张锦柱"}],"doi":"10.3969/j.issn.1001-1277.2003.07.014","fpage":"43","id":"173127e6-9d27-442f-8424-d35c5570e25b","issue":"7","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"45cf7c43-dbbf-4338-838d-efda573d860e","keyword":"<span style=\"color:red\">金</span>","originalKeyword":"金"},{"id":"27e150c8-2163-4424-ac6a-e0b570c5cfb7","keyword":"分离富集","originalKeyword":"分离富集"},{"id":"fc4fe01c-a40d-435f-b67c-80eae942c9be","keyword":"吸附","originalKeyword":"吸附"},{"id":"7bde1e14-8fc6-4035-92f7-c5a6ddf12d82","keyword":"萃取","originalKeyword":"萃取"}],"language":"zh","publisherId":"huangj200307014","title":"<span style=\"color:red\">金</span>的分离富集","volume":"24","year":"2003"},{"abstractinfo":"称取一定量的载<span style=\"color:red\">金</span>炭进行火试<span style=\"color:red\">金</span>配料,经过熔炼、灰吹得到金银合粒,使用硝酸分金得到<span style=\"color:red\">金</span>粒,再通过计算得到载<span style=\"color:red\">金</span>炭中银含量,从而建立了火试<span style=\"color:red\">金</span>重量法测定载<span style=\"color:red\">金</span>炭中银含量的方法.经过试验,确定了火试<span style=\"color:red\">金</span>配料中试样量、氧化铅加入量、灰吹温度等最佳试验条件.根据目前国内载<span style=\"color:red\">金</span>炭的生产水平,在载<span style=\"color:red\">金</span>炭国家标准物质加入一定量的共存元素,进行了银量测定的干扰试验,结果表明载<span style=\"color:red\">金</span>炭中共存元素(Cu、Fe、Pb、Cd、Zn、Bi、Cr、Ca、Mg、As)对银测定无影响.将方法用于3个载<span style=\"color:red\">金</span>炭国家标准物质中银的测定,测定值与认定值基本吻合,相对标准偏差(RSD,n=11)为0.82%~4.2%.","authors":[{"authorName":"夏珍珠","id":"ae2def66-61f8-4a33-8789-5dec712b132d","originalAuthorName":"夏珍珠"}],"doi":"10.13228/j.boyuan.issn1000-7571.010052","fpage":"54","id":"4b8246f5-46d3-4c21-add1-aec3ad1a51f6","issue":"2","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"47d546ce-8dc2-4590-a95d-577be2bda394","keyword":"载<span style=\"color:red\">金</span>炭","originalKeyword":"载金炭"},{"id":"d39a523e-9fce-4000-9dc3-679e231f7a0a","keyword":"银","originalKeyword":"银"},{"id":"4fe9ac55-04a7-4da9-9b38-d814d71ea793","keyword":"火试<span style=\"color:red\">金</span>","originalKeyword":"火试金"}],"language":"zh","publisherId":"yjfx201702011","title":"火试<span style=\"color:red\">金</span>重量法测定载<span style=\"color:red\">金</span>炭中银","volume":"37","year":"2017"},{"abstractinfo":"研究了杂质元素对火试<span style=\"color:red\">金</span>重量法测定粗<span style=\"color:red\">金</span>中<span style=\"color:red\">金</span>量的影响,并通过一系列实验分别确定了粗<span style=\"color:red\">金</span>中铜、铁、锌、镍、铂、钯、硒、碲、锑、铋、钛、钨12种杂质元素适用于该方法的上限量值,及杂质元素超上限量值时所采取的措施,保证了方法的适用性,对指导黄金冶炼企业准确测定粗<span style=\"color:red\">金</span>中<span style=\"color:red\">金</span>量具有重要的意义.","authors":[{"authorName":"马丽军","id":"1aea492a-f1cb-4f25-8870-494fbdfac084","originalAuthorName":"马丽军"},{"authorName":"李正旭","id":"bcdcac60-868f-43b0-8ff7-5fd18fdde2ed","originalAuthorName":"李正旭"},{"authorName":"钟英楠","id":"14b7df8e-fde7-400f-9b4c-11ba54563283","originalAuthorName":"钟英楠"},{"authorName":"阚春海","id":"69aab5c5-c343-4999-85bc-aa8f1fab723b","originalAuthorName":"阚春海"},{"authorName":"肖千鹏","id":"4124895c-f61b-457e-b3e1-a05be5a61792","originalAuthorName":"肖千鹏"},{"authorName":"赵可迪","id":"129b9416-e5e1-4289-b9ef-588bfdc3fb62","originalAuthorName":"赵可迪"}],"doi":"10.11792/hj20170419","fpage":"73","id":"46f9af80-ca46-483c-8fe4-9e040e33c937","issue":"4","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"479a91d0-1aef-4dcc-a898-ec7584f07b9c","keyword":"粗<span style=\"color:red\">金</span>","originalKeyword":"粗金"},{"id":"a0e8154d-ba09-4767-a2e9-43c4bda89609","keyword":"火试<span style=\"color:red\">金</span>","originalKeyword":"火试金"},{"id":"83e6efb9-971b-4ca5-80bd-f897fba9014b","keyword":"重量法","originalKeyword":"重量法"},{"id":"5050a2e1-8206-4f61-b38a-326d6b9a783b","keyword":"杂质","originalKeyword":"杂质"},{"id":"938185a1-80ab-4ccd-8a9f-c89967d97758","keyword":"增量","originalKeyword":"增量"}],"language":"zh","publisherId":"huangj201704019","title":"杂质元素对火试<span style=\"color:red\">金</span>重量法测定粗<span style=\"color:red\">金</span>中<span style=\"color:red\">金</span>量影响的探讨","volume":"38","year":"2017"},{"abstractinfo":"分析了化学镀镍浸<span style=\"color:red\">金</span>过程中<span style=\"color:red\">金</span>层厚度不均的现象及其产生的原因.试验发现,面积不同的铜面发生电气互联时容易造成<span style=\"color:red\">金</span>厚不均的现象,而无电气互联情况时,<span style=\"color:red\">金</span>厚均匀性比较好.导致<span style=\"color:red\">金</span>厚不均的原因有两种情况,一种是电势影响,二是双极性效应.","authors":[{"authorName":"胡光辉","id":"6105d80e-068e-4e75-a2ed-ffbd282a642b","originalAuthorName":"胡光辉"},{"authorName":"李大树","id":"62e3288a-b103-4eb7-9a99-6ffc789e1d06","originalAuthorName":"李大树"},{"authorName":"黄奔宇","id":"14d8dd8e-c1bd-4ca2-81b3-c545472f67eb","originalAuthorName":"黄奔宇"},{"authorName":"蒙继龙","id":"ff80758f-2722-4115-ac57-6b6a13f75f00","originalAuthorName":"蒙继龙"}],"doi":"10.3969/j.issn.1001-1560.2006.07.019","fpage":"64","id":"f773fb93-647e-4896-8a60-c0873b6988fb","issue":"7","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"a0ce79ec-825f-46c1-b447-ab3e4d597164","keyword":"化学镀镍","originalKeyword":"化学镀镍"},{"id":"e44c5d80-d47d-4fa1-96d8-2aa0b8a4189c","keyword":"浸<span style=\"color:red\">金</span>","originalKeyword":"浸金"},{"id":"1210d68b-2815-4375-b61c-6370035bcfcd","keyword":"双极性效应","originalKeyword":"双极性效应"}],"language":"zh","publisherId":"clbh200607019","title":"化学镀镍浸<span style=\"color:red\">金</span><span style=\"color:red\">金</span>厚不均探究","volume":"39","year":"2006"},{"abstractinfo":"介绍几种<span style=\"color:red\">金</span>基合金电镀的发展历程,比较几种镀液的性能特点并讨论几种<span style=\"color:red\">金</span>合金电镀的现况及未来的发展趋势.","authors":[{"authorName":"郭珊云","id":"fc3518a8-d78c-483e-86e1-3446f8c82f4f","originalAuthorName":"郭珊云"},{"authorName":"周光月","id":"c6c35efa-1cfc-4bba-83ea-a44b38ac31e3","originalAuthorName":"周光月"},{"authorName":"陈志全","id":"2831fb23-fc59-418c-8261-f7629ed22a93","originalAuthorName":"陈志全"},{"authorName":"郑恩华","id":"e49fed41-683c-42a7-a193-138e4c06b1ce","originalAuthorName":"郑恩华"},{"authorName":"胡劲","id":"4c6c1f70-4589-408f-90c9-a296f1ac945c","originalAuthorName":"胡劲"}],"doi":"10.3969/j.issn.1004-0676.1999.01.013","fpage":"53","id":"0320c3a0-d185-4db5-af32-63905d268001","issue":"1","journal":{"abbrevTitle":"GJS","coverImgSrc":"journal/img/cover/GJS.jpg","id":"38","issnPpub":"1004-0676","publisherId":"GJS","title":"贵金属"},"keywords":[{"id":"23453b40-da3e-4c13-bbb4-229e8683de54","keyword":"<span style=\"color:red\">金</span>","originalKeyword":"金"},{"id":"b4d640ca-5afd-42f4-b16a-3c710366061a","keyword":"合金","originalKeyword":"合金"},{"id":"e761404b-52d9-41b6-b774-3cb6259cd5ab","keyword":"电镀","originalKeyword":"电镀"}],"language":"zh","publisherId":"gjs199901013","title":"<span style=\"color:red\">金</span>合金电镀的发展","volume":"","year":"1999"}],"totalpage":256,"totalrecord":2553}