{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"利用数字散斑相关方法计算在不同温度下聚酰亚胺无机纳米杂化膜的变形量,并以此计算出聚酰亚胺无机纳米杂化膜的热膨胀系数.实验中同时测量了掺杂有不同浓度粘土、云母和二氧化硅类无机物的聚酰亚胺薄膜的热膨胀系数,并对实验结果进行了分析.","authors":[{"authorName":"毕博","id":"2ae9a5ae-c48b-4c24-8c0a-0337ea080e67","originalAuthorName":"毕博"},{"authorName":"高志敖","id":"d67e1af6-5b2b-4516-8477-0c96c3ea3370","originalAuthorName":"高志敖"},{"authorName":"张以河","id":"fc5b09bd-e4b1-49f9-a37a-a52ee138a6b1","originalAuthorName":"张以河"},{"authorName":"刘战伟","id":"2853c2af-8531-4216-a68c-cc9f06af78cc","originalAuthorName":"刘战伟"},{"authorName":"谢惠民","id":"bfe88add-f314-436b-a19a-a6e8ee1a9cba","originalAuthorName":"谢惠民"}],"doi":"","fpage":"119","id":"4f66de05-add2-4786-93e9-44a9936d724b","issue":"1","journal":{"abbrevTitle":"GFZCLKXYGC","coverImgSrc":"journal/img/cover/GFZCLKXYGC.jpg","id":"31","issnPpub":"1000-7555","publisherId":"GFZCLKXYGC","title":"高分子材料科学与工程"},"keywords":[{"id":"67445dac-2fbe-4a1f-8171-772fbcd2ce5c","keyword":"数字散斑相关","originalKeyword":"数字散斑相关"},{"id":"73821277-fe79-4ea1-bb43-b02b90edf3cb","keyword":"热膨胀系数","originalKeyword":"热膨胀系数"},{"id":"fefd986f-e3b9-4fb0-8699-22dbd7084e48","keyword":"聚酰亚胺无机纳米杂化","originalKeyword":"聚酰亚胺无机纳米杂化"}],"language":"zh","publisherId":"gfzclkxygc200601030","title":"数字散斑相关方法测量聚酰亚胺无机纳米杂化材料的热膨胀系数","volume":"22","year":"2006"},{"abstractinfo":"本发明提供了一种聚酰亚胺/无机纳米杂化材料制备方法,首先合成适用于聚酰亚胺的无机纳米粒子改性剂——亚胺环基硅烷;采用溶胶-凝胶法制备无机氧化物纳米粒子,在溶胶一凝胶反应过程中加入改性剂亚胺环基硅烷,得到有机-无机复合体纳米颗粒;将有机-无机复合体纳米颗粒均匀分散于聚酰胺酸溶液中,经过加热处理得到聚酰亚胺/无机纳米杂化材料。本发明的聚酰亚胺/无机纳米杂化材料制备方法解决了纳米粒子分散的难题,在聚酰亚胺/无机纳米杂化材料中纳米粒子分布均匀,不团聚,有利于其各项性能的充分发挥。","authors":[],"doi":"","fpage":"4","id":"1769379d-28a4-4e0c-be29-b2b456dfbfb2","issue":"1","journal":{"abbrevTitle":"GFZCLKXYGC","coverImgSrc":"journal/img/cover/GFZCLKXYGC.jpg","id":"31","issnPpub":"1000-7555","publisherId":"GFZCLKXYGC","title":"高分子材料科学与工程"},"keywords":[{"id":"7d414e4a-edf9-4b32-9558-90d458bd47c4","keyword":"无机纳米粒子","originalKeyword":"无机纳米粒子"},{"id":"e762f231-53b7-4c05-9bc1-5402a20d2277","keyword":"纳米杂化材料","originalKeyword":"纳米杂化材料"},{"id":"16c2d244-ccac-4b90-9706-ef05195b0269","keyword":"聚酰亚胺","originalKeyword":"聚酰亚胺"},{"id":"7820069b-cb4f-4acb-b5a2-78c7379af27b","keyword":"制备方法","originalKeyword":"制备方法"},{"id":"6b010af0-f77d-498c-bf82-fcbbb307d693","keyword":"溶胶-凝胶法","originalKeyword":"溶胶-凝胶法"},{"id":"cf3fd12f-7990-42c0-8f5d-69397662edf3","keyword":"有机-无机","originalKeyword":"有机-无机"},{"id":"1cc44755-5462-4420-8290-596551e90a97","keyword":"均匀分散","originalKeyword":"均匀分散"},{"id":"b3edf15e-9130-4707-917a-5031e0b40292","keyword":"纳米颗粒","originalKeyword":"纳米颗粒"}],"language":"zh","publisherId":"gfzclkxygc201201002","title":"聚酰亚胺/无机纳米杂化材料制备方法","volume":"28","year":"2012"},{"abstractinfo":"无机纳米杂化聚酰亚胺复合薄膜因无机填料在聚合物基体中纳米尺度的分散以及与基体间强的化学结合而具有较常规聚酰亚胺薄膜材料更优异的力学性能、热稳定性能、高绝缘性能及耐电晕性能等.依据国内外聚酰亚胺纳米杂化薄膜材料的最新研究情况,重点综述了SiO2/Al2O3、SiO2/Ti2O3、SiO2、TiO2、Al2O3、SiC、MMT等纳米杂化聚酰亚胺薄膜的研究进展,表明其是一种性能优异、具有广泛应用前途的有机一无机纳米复合材料,但尚存在许多需进一步深入研究的问题.","authors":[{"authorName":"任小龙","id":"2d434b10-7ecf-471e-b6a3-58b0711d2878","originalAuthorName":"任小龙"}],"doi":"10.3969/j.issn.1009-9239.2008.04.009","fpage":"28","id":"a91f2b47-9f2d-41ae-8462-eae794e22700","issue":"4","journal":{"abbrevTitle":"JYCL","coverImgSrc":"journal/img/cover/JYCL.jpg","id":"50","issnPpub":"1009-9239","publisherId":"JYCL","title":"绝缘材料"},"keywords":[{"id":"b520ace3-af93-42f4-8987-d951464d8d03","keyword":"聚酰亚胺薄膜","originalKeyword":"聚酰亚胺薄膜"},{"id":"876c81b0-fedf-4f00-bb6d-6073a142366e","keyword":"有机-无机纳米杂化材料","originalKeyword":"有机-无机纳米杂化材料"},{"id":"c8e2c926-e21c-41ec-92bc-2e9bc557ba41","keyword":"溶胶-凝胶法","originalKeyword":"溶胶-凝胶法"},{"id":"6bcc9453-744f-4b3f-851a-0e6ef40f06ee","keyword":"结构与性能","originalKeyword":"结构与性能"}],"language":"zh","publisherId":"jycltx200804009","title":"无机纳米杂化聚酰亚胺薄膜的研究进展","volume":"41","year":"2008"},{"abstractinfo":"简要介绍聚酰亚胺/纳米无机物杂化材料所用的纳米材料特性、分类、用途及机理,归纳了二者杂化的制备方法、形态结构及热学、电学和力学性能.提出了聚酰亚胺的合成和纳米无机物杂化材料尚需进一步研究的内容.","authors":[{"authorName":"赵军","id":"01feddfd-0fde-4a87-857a-7b29637fd57f","originalAuthorName":"赵军"},{"authorName":"皮丕辉","id":"2b1e20d0-bbf0-4db5-8421-31b6053c2136","originalAuthorName":"皮丕辉"},{"authorName":"杨卓如","id":"cfaad896-5142-4bf5-b3b3-b8604d35c787","originalAuthorName":"杨卓如"}],"doi":"10.3969/j.issn.1009-9239.2008.02.012","fpage":"42","id":"98714a29-bd36-4db5-8ce2-db152a091782","issue":"2","journal":{"abbrevTitle":"JYCL","coverImgSrc":"journal/img/cover/JYCL.jpg","id":"50","issnPpub":"1009-9239","publisherId":"JYCL","title":"绝缘材料"},"keywords":[{"id":"9010d694-3fd4-471a-9d47-253cd06a1232","keyword":"聚酰亚胺","originalKeyword":"聚酰亚胺"},{"id":"5fbf45fd-b9c7-42e5-8e8d-d158444ce2b0","keyword":"纳米无机物","originalKeyword":"纳米无机物"},{"id":"3b6b9913-4503-42b6-bd6c-5a3e106b6146","keyword":"杂化","originalKeyword":"杂化"}],"language":"zh","publisherId":"jycltx200802012","title":"挠性线路板用聚酰亚胺/纳米无机物杂化材料研究进展","volume":"41","year":"2008"},{"abstractinfo":"将无机纳米粒子(TiO2)分散在聚酰胺酸(PAA)前躯体中,经过原位聚合的方法制备出纳米TiO2粒子分散均匀的聚酰亚胺/纳米TiO2复合杂化膜,研究了不同掺杂含量对杂化膜的介电、物理等特性的影响,建立了耐电晕模型.同时通过FTIR研究其亚胺化程度以及用SEM分析纳米粒子在聚酰亚胺基体中的分散状态.结果表明,纳米粒子在PI基体中分散均匀,TiO2的引入对杂化膜的介电常数、介质损耗因数、电气强度和耐电晕性能产生了很大的影响,随着TiO2含量的增加,耐电晕性能得到大幅度的提高,TiO225%含量时介电常数为5.1左右,介质损耗因数在0.03以下,电气强度为110 MV/m,并在实验的基础上初步建立了耐电晕性能的老化机理.因此,在高耐热性绝缘材料中均匀分散一些纳米无机粒子,可以大幅度提高抗高频脉冲尖峰电压和耐电晕等方面的性能.","authors":[{"authorName":"查俊伟","id":"0b45e0e7-13e7-4a91-a628-208b693bf2c0","originalAuthorName":"查俊伟"},{"authorName":"党智敏","id":"c2a02aa0-2614-4419-9011-627c650990ef","originalAuthorName":"党智敏"}],"doi":"10.3969/j.issn.1009-9239.2008.06.002","fpage":"4","id":"707dd69e-18e4-4316-871f-e77fb1ee646b","issue":"6","journal":{"abbrevTitle":"JYCL","coverImgSrc":"journal/img/cover/JYCL.jpg","id":"50","issnPpub":"1009-9239","publisherId":"JYCL","title":"绝缘材料"},"keywords":[{"id":"d9af9eca-6cf6-4663-bcb3-89062114a430","keyword":"耐电晕","originalKeyword":"耐电晕"},{"id":"21daee28-ddc3-4efe-97e8-e4bed19fe2c2","keyword":"聚酰亚胺","originalKeyword":"聚酰亚胺"},{"id":"e30c86de-8f6e-46bc-8152-71384782bfb4","keyword":"纳米杂化膜","originalKeyword":"纳米杂化膜"},{"id":"f9f13c94-aefd-442a-9ee6-5b2d64a6ccc8","keyword":"介电性能","originalKeyword":"介电性能"}],"language":"zh","publisherId":"jycltx200806002","title":"无机纳米/聚酰亚胺复合杂化膜的绝缘特性研究","volume":"41","year":"2008"},{"abstractinfo":"以聚酰胺酸作为基体,通过正硅酸乙酯(TEOS)和异丙醇铝发生水解缩合反应,然后与聚酰胺酸发生溶胶凝胶过程,从而制备出无机纳米掺杂聚酰亚胺薄膜.利用傅里叶红外光谱、热失质量、介电谱及击穿试验对其热性能和电性能进行表征和测试,考察了相应的结构与性能之间的关系.","authors":[{"authorName":"赵斯梅","id":"ff2ce77f-f24b-499c-a7eb-5c785ffab9d5","originalAuthorName":"赵斯梅"}],"doi":"10.3969/j.issn.0253-4312.2007.10.007","fpage":"25","id":"5e67ba08-ab82-4296-9f7d-3a9b5574818c","issue":"10","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业 "},"keywords":[{"id":"43814ce2-b38f-46ce-83be-a94cf537eeae","keyword":"聚酰亚胺","originalKeyword":"聚酰亚胺"},{"id":"468c940a-fef4-46a8-915d-24153bfe6e21","keyword":"无机纳米杂化","originalKeyword":"无机纳米杂化"},{"id":"620fb0d2-bf18-4825-afef-edfe211f28b2","keyword":"薄膜","originalKeyword":"薄膜"}],"language":"zh","publisherId":"tlgy200710007","title":"无机纳米杂化聚酰亚胺薄膜的制备及性能研究","volume":"37","year":"2007"},{"abstractinfo":"采用溶胶-凝胶法制备纳米二氧化硅及氧化铝溶胶,将其掺入聚酰胺酸溶液中,制得聚酰亚胺/二氧化硅-氧化铝杂化薄膜,利用原子力显微镜对杂化薄膜的无机相微观形貌进行表征,用精密阻抗分析仪测试杂化膜介电性能.研究表明:掺入无机组分含量均为4%时,随着掺入二氧化硅所占比例的增大,无机纳米粒子的平均粒径增加,当其与氧化铝质量比为8:1时无机相呈网络状,与聚酰亚胺基体界面模糊;掺入无机组分对杂化薄膜的介电性能产生影响,介电常数ε和介电损耗tgδ随频率增加而减小,在相同频率下随掺入二氧化硅所占比例增大,介电常数ε和介电损耗tgδ增大.","authors":[{"authorName":"刘立柱","id":"690a962a-7555-4e4c-ae2c-77d090fa105d","originalAuthorName":"刘立柱"},{"authorName":"梁冰","id":"e01a86e2-a8ee-41a5-868c-c17d893c8bed","originalAuthorName":"梁冰"},{"authorName":"王伟","id":"d8627d66-60f2-4c42-9eb5-3a97b82414f8","originalAuthorName":"王伟"},{"authorName":"杨阳","id":"f063c320-838b-4d91-8b58-b871077428bb","originalAuthorName":"杨阳"},{"authorName":"雷清泉","id":"4cee4a60-a07e-4e0d-a96c-d056dec784c9","originalAuthorName":"雷清泉"}],"doi":"10.3969/j.issn.1005-0299.2006.03.012","fpage":"265","id":"fab89e19-f299-4286-a322-60c4a8983bc7","issue":"3","journal":{"abbrevTitle":"CLKXYGY","coverImgSrc":"journal/img/cover/CLKXYGY.jpg","id":"14","issnPpub":"1005-0299","publisherId":"CLKXYGY","title":"材料科学与工艺"},"keywords":[{"id":"42d31797-f48d-4296-bd8b-eab760aa62a8","keyword":"聚酰亚胺","originalKeyword":"聚酰亚胺"},{"id":"abd41acc-220a-4e09-ae3d-fe9ee21cf3fe","keyword":"二氧化硅","originalKeyword":"二氧化硅"},{"id":"11139ab4-236a-4a5a-ae4f-4327823b5d7f","keyword":"氧化铝","originalKeyword":"氧化铝"},{"id":"3472bc15-30e4-43ca-a081-1104698ab4e7","keyword":"溶胶-凝胶法","originalKeyword":"溶胶-凝胶法"},{"id":"1c6cd541-c6a9-4513-917b-6765449c3e14","keyword":"杂化薄膜","originalKeyword":"杂化薄膜"},{"id":"7bbdaa1f-8d83-4c3d-b0f1-6aece2ad6bd9","keyword":"介电性能","originalKeyword":"介电性能"}],"language":"zh","publisherId":"clkxygy200603012","title":"杂化聚酰亚胺薄膜无机相形貌和介电性能研究","volume":"14","year":"2006"},{"abstractinfo":"初步探讨了聚酰亚胺薄膜在电场作用下的电学行为,采用溶胶-凝胶工艺制备了聚酰亚胺/二氧化硅纳米杂化薄膜,并对薄膜进行浸水24 h处理,利用原子力显微镜对制备的薄膜进行表面形貌表征,讨论了无机组分SiO2和水对薄膜电性能的影响.结果表明:无机组分的引入及两相间的界面形态将对杂化薄膜的电学性能产生重大的影响;偶联剂的引入使得两相间产生紧密的微相结合,并对电性能产生一定的影响.","authors":[{"authorName":"张明艳","id":"23c626d9-09ab-4581-a2f1-c5a3cf7753e1","originalAuthorName":"张明艳"},{"authorName":"王芳","id":"371f14db-34e4-4d3d-a499-eb23fd723b59","originalAuthorName":"王芳"},{"authorName":"金镇镐","id":"6bd493ef-2fa3-4622-9d37-78347616eb84","originalAuthorName":"金镇镐"},{"authorName":"衷敬和","id":"e11a7dc6-d098-45aa-8020-9a5025a30f89","originalAuthorName":"衷敬和"},{"authorName":"曾恕金","id":"62ca73ab-83ca-45fe-931a-290a8ca2050c","originalAuthorName":"曾恕金"},{"authorName":"范勇","id":"24a7de8b-6236-4666-8f3a-9ac9fa4ada38","originalAuthorName":"范勇"},{"authorName":"雷清泉","id":"0222b843-f5e6-4c5f-8886-9f76e0ca5f5b","originalAuthorName":"雷清泉"}],"doi":"10.3969/j.issn.1005-0299.2004.06.005","fpage":"576","id":"df1a2570-be99-46d7-b684-41dcca5f84a1","issue":"6","journal":{"abbrevTitle":"CLKXYGY","coverImgSrc":"journal/img/cover/CLKXYGY.jpg","id":"14","issnPpub":"1005-0299","publisherId":"CLKXYGY","title":"材料科学与工艺"},"keywords":[{"id":"949d8128-9669-472a-b470-bf613dbcd0fd","keyword":"聚酰亚胺","originalKeyword":"聚酰亚胺"},{"id":"3ad572da-6021-4c60-a884-9ce3aaed47ab","keyword":"纳米杂化薄膜","originalKeyword":"纳米杂化薄膜"},{"id":"0041f2b7-d469-451d-b3d7-251ddd6f3e16","keyword":"偶联剂","originalKeyword":"偶联剂"},{"id":"c85e1770-948e-4ada-b8e7-7f7f11a8a8c5","keyword":"耐电晕","originalKeyword":"耐电晕"}],"language":"zh","publisherId":"clkxygy200406005","title":"无机组分对聚酰亚胺杂化薄膜电性能的影响","volume":"12","year":"2004"},{"abstractinfo":"为了提高聚酰亚胺薄膜的电学性能,将纳米硅/铝氧化物掺杂到聚酰亚胺(PI)基体中,通过固定掺杂总量,调整纳米硅/铝氧化物的相对质量百分含量,制备出一系列的无机纳米杂化聚酰亚胺薄膜.采用SEM(扫描电镜)表征了薄膜的表面形貌,对薄膜电气强度和耐电晕寿命进行了测试.结果表明:无机纳米杂化聚酰亚胺薄膜与纯的聚酰亚胺薄膜相比其电性能大幅度提高.","authors":[{"authorName":"陈慧丹","id":"fe6fa0a6-303c-45bb-a3f4-40a7996f0049","originalAuthorName":"陈慧丹"},{"authorName":"刘晓玉","id":"ade480f3-2e74-4fc0-960e-1d25017a0732","originalAuthorName":"刘晓玉"},{"authorName":"陈昊","id":"474423e2-ff7c-414d-826c-0dbdc706a3e2","originalAuthorName":"陈昊"},{"authorName":"李娟","id":"5c9b74de-23de-4e6a-9d9f-39d9dc0d7415","originalAuthorName":"李娟"},{"authorName":"范勇","id":"efb5e847-d18c-4f4b-8b6f-11d38a46ef37","originalAuthorName":"范勇"}],"doi":"10.3969/j.issn.1009-9239.2008.06.010","fpage":"37","id":"0b6c726a-1780-4a11-b9c8-8651288c44d3","issue":"6","journal":{"abbrevTitle":"JYCL","coverImgSrc":"journal/img/cover/JYCL.jpg","id":"50","issnPpub":"1009-9239","publisherId":"JYCL","title":"绝缘材料"},"keywords":[{"id":"d2195755-6d26-4b7d-b011-d323bb4c2c76","keyword":"聚酰亚胺","originalKeyword":"聚酰亚胺"},{"id":"54db3280-4c5e-49a2-bd4d-7df7b4ee61c4","keyword":"纳米杂化","originalKeyword":"纳米杂化"},{"id":"ca81d3f0-63fa-48eb-afc5-56072386ee50","keyword":"电学性能","originalKeyword":"电学性能"}],"language":"zh","publisherId":"jycltx200806010","title":"纳米硅/铝氧化物杂化聚酰亚胺薄膜电性能研究","volume":"41","year":"2008"},{"abstractinfo":"以均苯四酸二酐、4,4′-二氨基二苯基甲烷和正硅酸乙酯为原料,采用溶胶-凝胶法制备聚酰亚胺/纳米SiO2杂化膜,利用FT-IR、XPS、AFM对杂化膜的制备过程及杂化膜的结构进行了表征.证实聚酰胺酸加热亚胺化较为完全,杂化膜中有SiO2粒子生成,并以纳米尺度均匀地分布于聚酰亚胺中.采用综合热分析仪对杂化膜的热性能进行了分析,结果表明杂化膜的热性能优干聚酰亚胺膜,其热分解温度比聚酰亚胺膜提高了17.8℃.","authors":[{"authorName":"张春红","id":"8c839b06-16ab-43a5-9c7e-ded18da21972","originalAuthorName":"张春红"},{"authorName":"张志谦","id":"2970beee-44b8-48df-a4b8-04bca8d49534","originalAuthorName":"张志谦"},{"authorName":"曹海琳","id":"ab2749d9-f48c-4fa3-99f4-df397dbcfbc7","originalAuthorName":"曹海琳"},{"authorName":"龙军","id":"2a7e161c-f565-4904-9298-8b2f23200f0a","originalAuthorName":"龙军"}],"doi":"10.3969/j.issn.1005-0299.2006.06.021","fpage":"642","id":"c3ca87a7-d43f-48cf-9750-162f4c9987cd","issue":"6","journal":{"abbrevTitle":"CLKXYGY","coverImgSrc":"journal/img/cover/CLKXYGY.jpg","id":"14","issnPpub":"1005-0299","publisherId":"CLKXYGY","title":"材料科学与工艺"},"keywords":[{"id":"2cca8b21-acb2-4570-9788-fb29ba3418f7","keyword":"聚酰亚胺","originalKeyword":"聚酰亚胺"},{"id":"a184370f-0e8d-4916-a8a5-d4aeef14c8c1","keyword":"纳米SiO2","originalKeyword":"纳米SiO2"},{"id":"cfc61d63-921f-4f94-93b8-019f29fb18f2","keyword":"杂化膜","originalKeyword":"杂化膜"},{"id":"6b577577-49bf-4daf-919e-d7685278c316","keyword":"溶胶-凝胶法","originalKeyword":"溶胶-凝胶法"},{"id":"53ebac49-8743-4ab5-871e-5b24d993f03a","keyword":"正硅酸乙酯","originalKeyword":"正硅酸乙酯"}],"language":"zh","publisherId":"clkxygy200606021","title":"聚酰亚胺/纳米SiO2杂化膜的制备和表征","volume":"14","year":"2006"}],"totalpage":4916,"totalrecord":49157}