对水溶液中连续电沉积出的Fe56-59Ni合金箔的热处理工艺进行了详细的研究.实验结果表明,在氢气气氛中经950℃退火4h又经650℃回火1h的合金衍射峰Ⅰ(200)/Ⅰ(111)的值为最大,磁性能也最好,磁性能达到:最大磁导率(μm)达到0.028234T/A/m,饱和磁感应强度(Bs)1.5T,矫顽力(Hc)15.9155A/m.本文还对镀态的和热处理态的Fe56-59Ni合金进行了表面形貌(SEM)观察和晶体结构(XRD)分析.
参考文献
| [1] | S. D. Leith;S. Ramli .Characterization of NixFe1-x (0.10 < x <0.95) Electrodeposition from a Family of Sulfamate – Chloride Electrolytes[J].Journal of the Electrochemical Society,1999(4):1431-1435. |
| [2] | Romankiw L T .Evolution of the plating through lithographic mask technology[J].Electrochimica Acta,1997,42:2985. |
| [3] | Thomas M. Harris;Jennifer L. (St. Clair) Wilson;Matthew Bleakley .Effect of ethylenediamine on the electrodeposition of Ni-Fe alloys[J].Journal of the Electrochemical Society,1999(4):1461-1464. |
| [4] | N. Zech;D. Landolt .The influence of boric acid and sulfate ions on the hydrogen formation in Ni-Fe plating electrolytes[J].Electrochimica Acta,2000(21):3461-3471. |
| [5] | Vaes J.;Fransaer J. .The Role of Metal Hydroxides in NiFe Deposition[J].Journal of the Electrochemical Society,2000(10):3718-3724. |
| [6] | Tabakovic I;Riemer S;Inturi V;Jallen P Thayer A .[J].Journal of the Electrochemical Society,2000,147(01):219-226. |
| [7] | Ibro Tabakovic;Steve Riemer;Vladyslav Vas'ko .Effect of Magnetic Field on Electrode Reactions and Properties of Electrodeposited NiFe Films[J].Journal of the Electrochemical Society,2003(9):C635-C640. |
| [8] | Grand W C;Talbot J B .Electrodeposition of thin films of Nicket-Iron[J].Journal of the Electrochemical Society,1993,140(03):675-681. |
| [9] | Jung Gi Kim;Kyung Hunn Han;Seok Ho Song;Anne Reilly .Magnetic properties of sputtered soft magnetic Fe-Ni films with an uniaxial anisotropy[J].Thin Solid Films: An International Journal on the Science and Technology of Thin and Thick Films,2003(1/2):54-59. |
| [10] | 郭占成,刘宇星,刘美凤,卢维昌.电沉积Fe、Ni基合金箔的组织形貌及磁性能[J].中国有色金属学报,2004(02):273-279. |
| [11] | R S 特贝尔;D J 克雷克;北京冶金研究所《磁性材料》翻译组.磁性材料[M].北京:科学出版社,1979 |
| [12] | Robertson N.;Hu H.L. .High performance write head using NiFe 45/55[J].IEEE Transactions on Magnetics,1997(5):2818-2820. |
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